Basic information Safety Supplier Related

2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE

Basic information Safety Supplier Related

2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE Basic information

Product Name:
2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE
Synonyms:
  • N,N-DIMETHYL-2-BROMO-2-CYANOACETAMIDE
  • 2-bromo-2-cyano-n,n-dimethyl-acetamid
  • Bromocyanodimethylacetamide
  • Acetamide, 2-bromo-2-cyano-N,N-dimethyl-
  • 2-BROMO-2-CYANO-N N-DIMETHYLACETAMIDE 90+%
  • 2-(N,N-DIMETHYLCARBAMOYL)-2-BROMOACETONITRILE
  • 2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE
  • Einecs 239-441-0
CAS:
15430-62-3
MF:
C5H7BrN2O
MW:
191.03
EINECS:
239-441-0
Product Categories:
  • Bromination
  • Halogenation
  • Synthetic Organic Chemistry
Mol File:
15430-62-3.mol
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2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE Chemical Properties

Melting point:
57°C
Boiling point:
135 °C / 3mmHg
Density 
1.560±0.06 g/cm3(Predicted)
solubility 
sol ethanol, benzene, chloroform, ethyl acetate, and THF; insol petroleum ether and hexane; slightly sol hot ether, isopropyl alcohol, and H2O
pka
-0.65±0.70(Predicted)
EPA Substance Registry System
Acetamide, 2-bromo-2-cyano-N,N-dimethyl- (15430-62-3)
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Safety Information

Hazard Codes 
Xn
Risk Statements 
36/37/38-36-22
Safety Statements 
26-36/37/39
HS Code 
2926907090
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2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDE Usage And Synthesis

Uses

2-Bromo-2-cyano-n,n-dimethylacetamide is a monobrominating agent that is selective for the α-carbon of enolizable ketones.

Preparation

Via bromination of 2-cyano-N,N-dimethylacetamide with Br2 in AcOH/Ac2O at 8- 10 °C.

storage

The reagent is fairly stable at rt. For long storage, keep at 0-10 °C,  shielded from light. This reagent should be handled in a fume hood.

2-BROMO-2-CYANO-N,N-DIMETHYLACETAMIDESupplier

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