2-AMINO-3-METHYLBENZAMIDE

Product Name: 2-AMINO-3-METHYLBENZAMIDE
CAS No.: 1885-32-1
Chemical Name: 2-AMINO-3-METHYLBENZAMIDE
Synonyms: Benzamide, 2-amino-3-methyl-;Benzamide, 2-amino-3-methyl- (9CI)
CBNumber: CB01009992
Molecular Formula: C8H10N2O
Formula Weight: 150.18
MOL File: 1885-32-1.mol

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2-AMINO-3-METHYLBENZAMIDE Property

Melting point:: 149 °C
Boiling point:: 264.5±28.0 °C(Predicted)
Density: 1.185±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 15.88±0.50(Predicted)
Appearance: Off-white to light yellow Solid

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Safety

HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H317May cause an allergic skin reaction

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A898660
Product name: 2-Amino-3-methylbenzamide
Packaging: 500mg
Price: $285
Updated: 2021/12/16

AK Scientific

Product number: 9821AA
Product name: 2-Amino-3-methylbenzamide
Packaging: 1g
Price: $134
Updated: 2021/12/16

Matrix Scientific

Product number: 128433
Product name: 2-Amino-3-methylbenzamide
Purity: 97%
Packaging: 1g
Price: $332
Updated: 2021/12/16

AK Scientific

Product number: 9821AA
Product name: 2-Amino-3-methylbenzamide
Packaging: 5g
Price: $401
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0117380
Product name: 2-AMINO-3-METHYLBENZAMIDE
Purity: 95.00%
Packaging: 1G
Price: $808.89
Updated: 2021/12/16

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2-AMINO-3-METHYLBENZAMIDE Chemical Properties,Usage,Production

Synthesis

4389-45-1

1885-32-1

Step A: 2-amino-3-methylbenzoic acid (4.0 g, 26.5 mmol) was dissolved in degassed DMF (40 mL) under nitrogen protection. HOBt (4.28 g, 31.7 mmol), DIEA (5.52 mL, 31.7 mmol) and 2N NH3/MeOH solution (19 mL, 37.1 mmol) were added sequentially. The reaction mixture was stirred at room temperature for 16 hours. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure, and the crude product obtained was purified by silica gel column chromatography with an eluent of 10-60% EtOAc/hexane mixed solvent, resulting in 2-amino-3-methylbenzamide (2.52 g, 63% yield) as a white solid. The structure of the product was confirmed by 1H NMR (300 MHz, DMSO-d6): δ 2.07 (s, 3H), 6.40-6.47 (m, 3H), 7.06 (m, 2H), 7.42 (d, 1H), 7.72 (br d, 1H).

References

[1] Organic and Biomolecular Chemistry, 2011, vol. 9, # 17, p. 6089 - 6099
[2] Journal of Medicinal Chemistry, 2017, vol. 60, # 2, p. 814 - 820
[3] Patent: WO2018/46933, 2018, A1. Location in patent: Page/Page column 32-33
[4] Patent: US2012/53174, 2012, A1. Location in patent: Page/Page column 48
[5] Patent: US2016/168140, 2016, A1. Location in patent: Paragraph 1161

2-AMINO-3-METHYLBENZAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-3-METHYLBENZAMIDE Suppliers

China 49 Europe 1 India 1 United States 6 Global 57

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1885-32-1, 2-AMINO-3-METHYLBENZAMIDERelated Search:

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Benzamide, 2-amino-3-methyl- (9CI)

Benzamide, 2-amino-3-methyl-

1885-32-1

AMIDE

AMINEPRIMARY

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