ChemicalBook > CAS DataBase List > 3-Iodo-N-phenylcarbazole

3-Iodo-N-phenylcarbazole

Product Name
3-Iodo-N-phenylcarbazole
CAS No.
502161-03-7
Chemical Name
3-Iodo-N-phenylcarbazole
Synonyms
3-iodo-9-phenyl-9H-carbazole;3-Iodo-N-phenyL;3-Iodo-N-phenylcarba;3-iodo-N-phenylcarbazol;3-Iodo-9-phenylcarbazole;3-Iodo-N-phenylcarbazole;3-Iodo-9-phenylcarbazole>3- iodine-9- phenylcarbazole;3-Iodinated-N-phenylcarbazole;9H-Carbazole, 3-iodo-9-phenyl-
CBNumber
CB01073966
Molecular Formula
C18H12IN
Formula Weight
369.2
MOL File
502161-03-7.mol
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3-Iodo-N-phenylcarbazole Property

Melting point:
103.0 to 107.0 °C
Boiling point:
480.6±27.0 °C(Predicted)
Density 
1.55±0.1 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
form 
powder to crystal
color 
White to Light yellow
CAS DataBase Reference
502161-03-7
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical
Product number
I0913
Product name
3-Iodo-9-phenylcarbazole
Purity
>98.0%(GC)
Packaging
1g
Price
$36
Updated
2025/07/31
TCI Chemical
Product number
I0913
Product name
3-Iodo-9-phenylcarbazole
Purity
>98.0%(GC)
Packaging
5g
Price
$50
Updated
2025/07/31
Chem-Impex
Product number
30934
Product name
3-Iodo-9-phenylcarbazole,≥98%(GC)
Purity
≥98%(GC)
Packaging
5G
Price
$61.17
Updated
2021/12/16
AK Scientific
Product number
J97724
Product name
3-Iodo-N-phenylcarbazole
Packaging
5g
Price
$25
Updated
2021/12/16
ChemScene
Product number
CS-W021948
Product name
3-Iodo-N-phenylcarbazole
Purity
98.72%
Packaging
25g
Price
$50
Updated
2021/12/16
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3-Iodo-N-phenylcarbazole Chemical Properties,Usage,Production

Chemical Properties

White crystalline powder

Synthesis

1150-62-5

502161-03-7

General procedure for the synthesis of 3-iodo-9-phenylcarbazole from N-phenylcarbazole: 2.433 g (10 mmol) of intermediate compound A (N-phenylcarbazole) was dissolved in 100 mL of 80% acetic acid solution, followed by the sequential addition of 1.357 g (5.35 mmol) of iodine monomers (I2) and 0.333 g (1.46 mmol) of o-n-octanoic acid ( H5IO6). The reaction mixture was stirred at 80 °C for 2 h under nitrogen protection. After completion of the reaction, the reaction mixture was extracted three times with ether (50 mL). The organic layers were combined and dried with anhydrous magnesium sulfate, followed by evaporation under reduced pressure to remove the solvent. The resulting crude product was purified by silica gel column chromatography to afford 3.23 g of intermediate compound B (3-iodo-9phenylcarbazole) as a white solid in 87% yield.1H NMR (CDCl3, 300 MHz) δ (ppm): 8.43 (d, 1H), 8.05 (d, 1H), 7.62 (dd, 1H), 7.61-7.75 (m, 2H) , 7.51-7.43 (m, 3H), 7.41-7.35 (m, 2H), 7.27 (dd, 1H), 7.14 (d, 1H).

References

[1] Patent: EP1661888, 2006, A1. Location in patent: Page/Page column 11
[2] Patent: US2008/174237, 2008, A1. Location in patent: Page/Page column 13-14
[3] Patent: EP2149555, 2010, A1. Location in patent: Page/Page column 19
[4] Patent: KR101791161, 2017, B1. Location in patent: Paragraph 0116; 0123-0128
[5] Patent: EP2738166, 2014, A1. Location in patent: Paragraph 0162

3-Iodo-N-phenylcarbazole Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Iodo-N-phenylcarbazole Suppliers

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View Lastest Price from 3-Iodo-N-phenylcarbazole manufacturers

Hebei Fengjia New Material Co., Ltd
Product
3-Iodo-N-phenylcarbazole 502161-03-7
Price
US $2.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
10000
Release date
2024-08-08
Hebei Chuanghai Biotechnology Co., Ltd
Product
3-Iodo-N-phenylcarbazole 502161-03-7
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
5tons
Release date
2024-12-04
Shanghai Daken Advanced Materials Co.,Ltd
Product
9H-Carbazole, 3-iodo-9-phenyl- 502161-03-7
Price
US $0.00/KG
Min. Order
1KG
Purity
98.00%
Supply Ability
150KG /month
Release date
2021-11-17

502161-03-7, 3-Iodo-N-phenylcarbazoleRelated Search:

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