ChemicalBook > CAS DataBase List > METHYL-2METHYL-6-NITRO-BENZOATE

METHYL-2METHYL-6-NITRO-BENZOATE

Product Name
METHYL-2METHYL-6-NITRO-BENZOATE
CAS No.
61940-22-5
Chemical Name
METHYL-2METHYL-6-NITRO-BENZOATE
Synonyms
METHYL-2METHYL-6-NITRO-BENZOATE;2-Methyl-6-nitrobenzoic Acid Methyl Ester;Benzoic acid, 2-Methyl-6-nitro-, Methyl ester
CBNumber
CB01119075
Molecular Formula
C9H9NO4
Formula Weight
195.17
MOL File
61940-22-5.mol
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METHYL-2METHYL-6-NITRO-BENZOATE Property

Boiling point:
283.4±20.0 °C(Predicted)
Density 
1?+-.0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
DCM, Methanol
form 
Solid
color 
Brown
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Safety

HS Code 
2916310090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M320200
Product name
2-Methyl-6-nitrobenzoicAcidMethylEster
Packaging
1g
Price
$100
Updated
2021/12/16
Apolloscientific
Product number
OR301028
Product name
Methyl2-methyl-6-nitrobenzoate
Packaging
1g
Price
$44
Updated
2021/12/16
SynQuest Laboratories
Product number
4754-1-02
Product name
Methyl 2-methyl-6-nitrobenzoate
Purity
95%
Packaging
1g
Price
$48
Updated
2021/12/16
ChemScene
Product number
CS-W006451
Product name
Methyl2-methyl-6-nitrobenzoate
Purity
≥97.0%
Packaging
5g
Price
$120
Updated
2021/12/16
Apolloscientific
Product number
OR301028
Product name
Methyl2-methyl-6-nitrobenzoate
Packaging
5g
Price
$128
Updated
2021/12/16
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METHYL-2METHYL-6-NITRO-BENZOATE Chemical Properties,Usage,Production

Uses

2-Methyl-6-nitrobenzoic Acid Methyl Ester is an ester derivative of 2-Methyl-nitrobenzoic Acid (M325545), an derivative of Anthranilic Acid (A679220).

Synthesis

13506-76-8

74-88-4

61940-22-5

Step 1) Synthesis of methyl 2-methyl-6-nitrobenzoate (2): 2-methyl-6-nitrobenzoic acid (1; 10 g, 55.2 mmol) was dissolved in 200 mL of methyl ethyl ketone, iodomethane (17.2 mL, 276.0 mmol) and anhydrous potassium carbonate (38.1 g, 276.0 mmol) were added. The reaction mixture was stirred under reflux conditions for 18 hours. Upon completion of the reaction, the mixture was cooled to room temperature and filtered. The filtrate was diluted with ethyl acetate (300 mL), washed sequentially with water (2 x 50 mL) and saturated saline, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to give 10.80 g of methyl 2-methyl-6-nitrobenzoate (2). Mass spectrometry (ESI) analysis: the calculated value of C9H9NO4 was 195.05 and the measured value was 196 [M + H].

References

[1] Chemical Communications, 2005, # 44, p. 5583 - 5585
[2] Chemistry - A European Journal, 2009, vol. 15, # 24, p. 5956 - 5968
[3] Patent: US2011/251395, 2011, A1. Location in patent: Page/Page column 15
[4] Patent: US2005/49253, 2005, A1. Location in patent: Page/Page column 25-26
[5] Patent: US2005/54670, 2005, A1. Location in patent: Page/Page column 27

METHYL-2METHYL-6-NITRO-BENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from METHYL-2METHYL-6-NITRO-BENZOATE manufacturers

Career Henan Chemical Co
Product
METHYL-2METHYL-6-NITRO-BENZOATE 61940-22-5
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
Customized
Release date
2019-12-19

61940-22-5, METHYL-2METHYL-6-NITRO-BENZOATE Related Search:

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  • METHYL-2METHYL-6-NITRO-BENZOATE
  • Benzoic acid, 2-Methyl-6-nitro-, Methyl ester
  • 2-Methyl-6-nitrobenzoic Acid Methyl Ester
  • 61940-22-5