PHENYL-D5-BORONIC ACID
- Product Name
- PHENYL-D5-BORONIC ACID
- CAS No.
- 215527-70-1
- Chemical Name
- PHENYL-D5-BORONIC ACID
- Synonyms
- 2,3,4,5,6-Pentadeuteriumbenzeneboronic Acid;9-bromo-10-(phenyl-d5)anthracene;Phenyl-d?-boronic acid;PHENYL-D5-BORONIC ACID;B-(phenyl-2,3,4,5,6-d5)-;phenyl-d5-boronicacid98atom%d;Deuterated phenylboronic acid;(Perdeuterophenyl)boronic acid;PHENYL-D5-BORONIC ACID(D, 98%);B-(Phenyl-2,3,4,5,6-d5)boronic acid
- CBNumber
- CB0121981
- Molecular Formula
- C6H7BO2
- Formula Weight
- 121.93
- MOL File
- 215527-70-1.mol
PHENYL-D5-BORONIC ACID Property
- Melting point:
- 217-220 °C(lit.)
- solubility
- Chloroform (Slightly), DMSO
- form
- solid
- color
- White
- Stability:
- Hygroscopic
- InChI
- InChI=1S/C6H7BO2/c8-7(9)6-4-2-1-3-5-6/h1-5,8-9H
- InChIKey
- HXITXNWTGFUOAU-RALIUCGRSA-N
- SMILES
- B(C1C([H])=C([H])C([H])=C([H])C=1[H])(O)O
- CAS DataBase Reference
- 215527-70-1
N-Bromosuccinimide Price
- Product number
- 517860
- Product name
- Phenyl-d5-boronic acid
- Purity
- 98 atom % D, 98% (CP)
- Packaging
- 1g
- Price
- $202
- Updated
- 2024/03/01
- Product number
- P319592
- Product name
- PhenylboronicAcid-d5
- Packaging
- 1g
- Price
- $225
- Updated
- 2021/12/16
- Product number
- P319592
- Product name
- PhenylboronicAcid-d5
- Packaging
- 250mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- OR907458
- Product name
- (2,3,4,5,6-Pentadeuteriophenyl)boronicacid
- Purity
- 98%
- Packaging
- 1g
- Price
- $115
- Updated
- 2021/12/16
- Product number
- X0621
- Product name
- Phenyl-d5-boronic acid
- Packaging
- 1g
- Price
- $158
- Updated
- 2021/12/16
PHENYL-D5-BORONIC ACID Chemical Properties,Usage,Production
Uses
Phenylboronic Acid-d5 is the isotope labelled analog of Phenylboronic Acid; a compound used in the organic synthesis of various pharmaceutical goods.
Synthesis
A dry three-neck flask equipped with a rubber septum, an addition funnel equipped with a rubber septum, and a condenser was charged under nitrogen with magnesium turnings. To the addition funnel was added D5-bromobenzene (6.5 mL, 62 mmol) (Aldrich) dissolved in a 1:1 mixture of THF/toluene (31 mL). Grignard reagent formation was observed after about after about 1 mL of the contents of the addition funnel had been added to the magnesium turnings. The remaining bromobenzene solution was added dropwise over a period of about 1 h. After the addition was complete the reaction mixture was heated at 70° C. for 1 h. The reaction mixture was cooled to room temperature and added via a canulating needled to an addition funnel on a second three-neck flask containing a solution of triethylborate (B(OEt)3) (10.5 mL, 62 mmol) in toluene (10 mL) maintained at 0° C. The solution of the freshly prepared Grignard reagent was then added dropwise to the solution of triethylborate over a period of 1 h. The cooling bath was then removed and the reaction mixture was allowed to stir at room temperature for 15 h. The reaction mixture was quenched with 10% H2SO4 (30 mL) and stirred at room temperature for 1 h. The layers were separated and the organic layer was dried over Na2SO4. After removal of the solvent, addition of hexane precipitated the product as an off-white solid, which was collected by filtration and dried to afford Phenyl-d5-boronic acid. Its yield: 3.50 g, 45%.
PHENYL-D5-BORONIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from PHENYL-D5-BORONIC ACID manufacturers
- Product
- Phenyl-D5-boronic acid 215527-70-1
- Price
- US $51.50-956.00/g
- Min. Order
- 5g
- Purity
- 0.98
- Supply Ability
- 10kg
- Release date
- 2023-12-21
- Product
- PHENYL-D5-BORONIC ACID 215527-70-1
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 50000KG/month
- Release date
- 2024-08-09
- Product
- B-(Phenyl-2,3,4,5,6-d5)boronic acid 215527-70-1
- Price
- US $0.00-0.00/G
- Min. Order
- 10G
- Purity
- 0.98
- Supply Ability
- 500kg
- Release date
- 2023-09-25