ChemicalBook > CAS DataBase List > PHENYL-D5-BORONIC ACID

PHENYL-D5-BORONIC ACID

Product Name
PHENYL-D5-BORONIC ACID
CAS No.
215527-70-1
Chemical Name
PHENYL-D5-BORONIC ACID
Synonyms
2,3,4,5,6-Pentadeuteriumbenzeneboronic Acid;9-bromo-10-(phenyl-d5)anthracene;Phenyl-d?-boronic acid;PHENYL-D5-BORONIC ACID;B-(phenyl-2,3,4,5,6-d5)-;phenyl-d5-boronicacid98atom%d;Deuterated phenylboronic acid;(Perdeuterophenyl)boronic acid;PHENYL-D5-BORONIC ACID(D, 98%);B-(Phenyl-2,3,4,5,6-d5)boronic acid
CBNumber
CB0121981
Molecular Formula
C6H7BO2
Formula Weight
121.93
MOL File
215527-70-1.mol
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PHENYL-D5-BORONIC ACID Property

Melting point:
217-220 °C(lit.)
solubility 
Chloroform (Slightly), DMSO
form 
solid
color 
White
Stability:
Hygroscopic
InChI
InChI=1S/C6H7BO2/c8-7(9)6-4-2-1-3-5-6/h1-5,8-9H
InChIKey
HXITXNWTGFUOAU-RALIUCGRSA-N
SMILES
B(C1C([H])=C([H])C([H])=C([H])C=1[H])(O)O
CAS DataBase Reference
215527-70-1
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Safety

Hazard Codes 
Xn
Risk Statements 
22
Safety Statements 
36
WGK Germany 
3
HS Code 
2931900090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P321Specific treatment (see … on this label).

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
517860
Product name
Phenyl-d5-boronic acid
Purity
98 atom % D, 98% (CP)
Packaging
1g
Price
$202
Updated
2024/03/01
TRC
Product number
P319592
Product name
PhenylboronicAcid-d5
Packaging
1g
Price
$225
Updated
2021/12/16
TRC
Product number
P319592
Product name
PhenylboronicAcid-d5
Packaging
250mg
Price
$85
Updated
2021/12/16
Apolloscientific
Product number
OR907458
Product name
(2,3,4,5,6-Pentadeuteriophenyl)boronicacid
Purity
98%
Packaging
1g
Price
$115
Updated
2021/12/16
AK Scientific
Product number
X0621
Product name
Phenyl-d5-boronic acid
Packaging
1g
Price
$158
Updated
2021/12/16
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PHENYL-D5-BORONIC ACID Chemical Properties,Usage,Production

Uses

Phenylboronic Acid-d5 is the isotope labelled analog of Phenylboronic Acid; a compound used in the organic synthesis of various pharmaceutical goods.

Synthesis

A dry three-neck flask equipped with a rubber septum, an addition funnel equipped with a rubber septum, and a condenser was charged under nitrogen with magnesium turnings. To the addition funnel was added D5-bromobenzene (6.5 mL, 62 mmol) (Aldrich) dissolved in a 1:1 mixture of THF/toluene (31 mL). Grignard reagent formation was observed after about after about 1 mL of the contents of the addition funnel had been added to the magnesium turnings. The remaining bromobenzene solution was added dropwise over a period of about 1 h. After the addition was complete the reaction mixture was heated at 70° C. for 1 h. The reaction mixture was cooled to room temperature and added via a canulating needled to an addition funnel on a second three-neck flask containing a solution of triethylborate (B(OEt)3) (10.5 mL, 62 mmol) in toluene (10 mL) maintained at 0° C. The solution of the freshly prepared Grignard reagent was then added dropwise to the solution of triethylborate over a period of 1 h. The cooling bath was then removed and the reaction mixture was allowed to stir at room temperature for 15 h. The reaction mixture was quenched with 10% H2SO4 (30 mL) and stirred at room temperature for 1 h. The layers were separated and the organic layer was dried over Na2SO4. After removal of the solvent, addition of hexane precipitated the product as an off-white solid, which was collected by filtration and dried to afford Phenyl-d5-boronic acid. Its yield: 3.50 g, 45%.

PHENYL-D5-BORONIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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PHENYL-D5-BORONIC ACID Suppliers

China 157 Germany 2 India 2 Switzerland 1 United States 6 Global 168
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View Lastest Price from PHENYL-D5-BORONIC ACID manufacturers

Shanghai UCHEM Inc.
Product
Phenyl-D5-boronic acid 215527-70-1
Price
US $51.50-956.00/g
Min. Order
5g
Purity
0.98
Supply Ability
10kg
Release date
2023-12-21
Hebei Mojin Biotechnology Co.,Ltd
Product
PHENYL-D5-BORONIC ACID 215527-70-1
Price
US $0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
50000KG/month
Release date
2024-08-09
Kindchem(Nanjing)Co.,Ltd
Product
B-(Phenyl-2,3,4,5,6-d5)boronic acid 215527-70-1
Price
US $0.00-0.00/G
Min. Order
10G
Purity
0.98
Supply Ability
500kg
Release date
2023-09-25

215527-70-1, PHENYL-D5-BORONIC ACIDRelated Search:

TETRAHYDROFURAN-D8 PYRIDINE-D5 Bromobenzene-d5 BENZOIC ACID-D5 IODOMETHANE-D3 Benzene-D6 DICHLOROMETHANE-D2 BORANE-D3 ACETALDEHYDE-D4 TOLUENE-D8 Boric acid PHENYL-D5-BORONIC ACID

  • PHENYL-D5-BORONIC ACID
  • phenyl-d5-boronicacid98atom%d
  • (Perdeuterophenyl)boronic acid
  • B-(Phenyl-2,3,4,5,6-d5)boronic acid
  • 2,3,4,5,6-Pentadeuteriumbenzeneboronic Acid
  • Boronic acid,B-(phenyl-2,3,4,5,6-d5)-
  • 9-bromo-10-(phenyl-d5)anthracene
  • PHENYL-D5-BORONIC ACID(D, 98%)
  • Phenyl-d?-boronic acid
  • Deuterated phenylboronic acid
  • (2,3,4,5,6-pentadeuteriophenyl)boronic acid
  • B-(phenyl-2,3,4,5,6-d5)-
  • 215527-70-1
  • C6D5H2BO2
  • C6D5BOH2
  • C6H2BD5O2
  • Organometallic Reagents
  • Aryl
  • Boronic Acids and Derivatives
  • Boronic Acids
  • Boronic Acids
  • blocks
  • BoronicAcids
  • Aryl
  • Boronic Acids
  • Boronic Acids and Derivatives