ChemicalBook > CAS DataBase List > 5-Bromo-2-fluorobenzylamine hydrochloride

5-Bromo-2-fluorobenzylamine hydrochloride

Product Name: 5-Bromo-2-fluorobenzylamine hydrochloride
CAS No.: 99725-13-0
Chemical Name: 5-Bromo-2-fluorobenzylamine hydrochloride
Synonyms: RARECHEM AL BD 0325;5-BROMO-2-FLUOROBENZYL ALCOHOL;(5-BROMO-2-FLUOROPHENYL)METHANOL;Benzenemethanol, 5-bromo-2-fluoro-;5-Bromo-2-fluorobenzylamine hydrochloride;5-Bromo-2-fluorobenzylamine hydrochloride ISO 9001：2015 REACH
CBNumber: CB0218517
Molecular Formula: C7H6BrFO
Formula Weight: 205.02
MOL File: 99725-13-0.mol

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5-Bromo-2-fluorobenzylamine hydrochloride Property

Melting point:: 221-226 °C(lit.)
Boiling point:: 82-87°/0.4mm
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid
CAS DataBase Reference: 99725-13-0(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
Hazard Note: Irritant
HS Code: 2906290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B692118
Product name: 5-Bromo-2-fluorobenzylAlcohol
Packaging: 10g
Price: $130
Updated: 2021/12/16

Apolloscientific

Product number: PC7382
Product name: 5-Bromo-2-fluorobenzylalcohol
Packaging: 25g
Price: $134
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2601-B-12
Product name: 5-Bromo-2-fluorobenzyl alcohol
Packaging: 25g
Price: $175
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB151369
Product name: 5-Bromo-2-fluorobenzylalcohol
Packaging: 1g
Price: $207
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB151369
Product name: 5-Bromo-2-fluorobenzylalcohol
Packaging: 500mg
Price: $120
Updated: 2021/12/16

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5-Bromo-2-fluorobenzylamine hydrochloride Chemical Properties,Usage,Production

Uses

5-Bromo-2-fluorobenzylamine hydrochloride is mainly used as an intermediate in organic synthesis, especially in the fields of medicine and materials science.

Synthesis

93777-26-5

99725-13-0

The general procedure for the synthesis of 5-bromo-2-fluorobenzyl alcohol from 5-bromo-2-fluorobenzaldehyde was as follows: sodium borohydride (8.39 g, 222 mmol) was slowly added to an ethanol (EtOH) solution of 5-bromo-2-fluorobenzaldehyde (30.0 g, 148 mmol) at 0 °C. The reaction mixture was stirred at 0 °C, followed by a gradual warming to room temperature over 15 h. The reaction was carried out at 0 °C. The reaction was carried out at 0 °C. The reaction was carried out at 0 °C. Upon completion of the reaction, the mixture was again cooled to 0 °C and the reaction was quenched with saturated aqueous ammonium chloride (NH4Cl) solution. The reaction mixture was extracted with ethyl acetate (EtOAc) and the organic layer was separated. The organic layer was subsequently washed with brine, dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure to afford 5-bromo-2-fluorobenzyl alcohol (30.3 g, quantitative yield) as a white solid, which can be used in subsequent reactions without further purification. [M-OH]+ 187.

References

[1] Patent: WO2011/159067, 2011, A2. Location in patent: Page/Page column 51
[2] Journal of Medicinal Chemistry, 1999, vol. 42, # 18, p. 3572 - 3587
[3] Patent: US6034093, 2000, A
[4] Patent: US5731315, 1998, A
[5] Patent: WO2004/814, 2003, A1. Location in patent: Page 49

5-Bromo-2-fluorobenzylamine hydrochloride Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-Bromo-2-fluorobenzylamine hydrochloride manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 5-Bromo-2-fluorobenzylamine hydrochloride 99725-13-0
Price: US $9.90/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 5tons
Release date: 2024-12-02

Hangzhou ICH Biofarm Co., Ltd

Product: 5-Bromo-2-fluorobenzyl alcohol 99725-13-0
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 2000kg
Release date: 2023-06-09

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-Bromo-2-fluorobenzylamine hydrochloride 99725-13-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

99725-13-0, 5-Bromo-2-fluorobenzylamine hydrochlorideRelated Search:

DL-ALPHA-METHYLBENZYLAMINE 4-Bromobenzotrifluoride 4-BROMOPHENYLHYDRAZINE HYDROCHLORIDE Ethyl bromodifluoroacetate Topotecan hydrochloride Trimethoprim 4-Fluorobenzylamine Phenoxybenzamine hydrochloride Benzylamine hydrochloride 3-Bromoanisole 1-BROMO-3-(1,3-DIOXOLAN-2-YL)-4-FLUOROBENZENE 5-BROMO-4-CHLORO-2-FLUOROBENZOIC ACID 5-Bromo-2-fluorobenzoic acid 2-AMINO-3,5-DIBROMO-6-FLUOROBENZOIC ACID BROMOTRIFLUOROMETHANE 3-BROMO-5-FLUOROBENZYLAMINE HYDROCHLORIDE,4-BROMO-2-FLUOROBENZYLAMINE HYDROCHLORIDE 2-IODOBENZALDEHYDE 3,5-DIBROMO-2-FLUOROBENZYL ALCOHOL

(5-BROMO-2-FLUOROPHENYL)METHANOL

5-BROMO-2-FLUOROBENZYL ALCOHOL

RARECHEM AL BD 0325

5-Bromo-2-fluorobenzylamine hydrochloride

Benzenemethanol, 5-bromo-2-fluoro-

5-Bromo-2-fluorobenzylamine hydrochloride ISO 9001：2015 REACH

99725-13-0

C7H8BrFNCl

Amine Salts

Building Blocks

Nitrogen Compounds

Organic Building Blocks

Benzhydrols, Benzyl & Special Alcohols

Fluorine Compounds

Anilines, Amides & Amines

Bromine Compounds