2-METHOXYBENZENESULFONYL CHLORIDE
- Product Name
- 2-METHOXYBENZENESULFONYL CHLORIDE
- CAS No.
- 10130-87-7
- Chemical Name
- 2-METHOXYBENZENESULFONYL CHLORIDE
- Synonyms
- AKOS BB-9465;2-Methoxyphenylsulfonyl chloride;o-Methoxybenzenesulfonyl chloride;5-Methoxybenzenesulfonyl chloride;2-METHOXYBENZENESULFONYL CHLORIDE;2-Methoxybenzenesulphonyl chloride;2-Methoxybenzene-1-sulfonyl chloride;2-Methoxybenzenesulfonylchloride,97%;Benzenesulfonyl chloride, 2-methoxy-;M**2-METHOXYBENZENE SULFONYL CHLORIDE
- CBNumber
- CB0219741
- Molecular Formula
- C7H7ClO3S
- Formula Weight
- 206.65
- MOL File
- 10130-87-7.mol
2-METHOXYBENZENESULFONYL CHLORIDE Property
- Melting point:
- 50-54°C
- Boiling point:
- 126-129 °C(Press: 0.3 Torr)
- Density
- 1.376
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- Light brown to brown Solid
- Sensitive
- Moisture Sensitive
- InChI
- InChI=1S/C7H7ClO3S/c1-11-6-4-2-3-5-7(6)12(8,9)10/h2-5H,1H3
- InChIKey
- GYOBZOBUOMDRRN-UHFFFAOYSA-N
- SMILES
- C1(S(Cl)(=O)=O)=CC=CC=C1OC
- CAS DataBase Reference
- 10130-87-7
Safety
- Hazard Codes
- Xi
- Risk Statements
- 34-43
- Safety Statements
- 26-36/37/39-36/37
- RIDADR
- 3261
- HazardClass
- IRRITANT
- HazardClass
- 8
- PackingGroup
- Ⅲ
- HS Code
- 2930909899
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
H318Causes serious eye damage
- Precautionary statements
-
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- M3470
- Product name
- 2-Methoxybenzenesulfonyl Chloride
- Packaging
- 200MG
- Price
- $68
- Updated
- 2025/07/31
- Product number
- M3470
- Product name
- 2-Methoxybenzenesulfonyl Chloride
- Packaging
- 1G
- Price
- $204
- Updated
- 2025/07/31
- Product number
- M265908
- Product name
- 2-MethoxybenzenesulfonylChloride
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 033182
- Product name
- 2-Methoxy-benzenesulfonyl chloride
- Packaging
- 1g
- Price
- $46
- Updated
- 2021/12/16
- Product number
- 088375
- Product name
- 2-Methoxy-benzenesulfonylchloride
- Packaging
- 250mg
- Price
- $36
- Updated
- 2021/12/16
2-METHOXYBENZENESULFONYL CHLORIDE Chemical Properties,Usage,Production
Uses
For synthesis and pharmacological evaluation of sulfonamide derivatives of thiazolidin-4-ones 5-Bromo-2-methoxybenzenesulfonyl chloride is used.
Synthesis
7217-59-6
10130-87-7
General procedure for the synthesis of 2-methoxybenzenesulfonyl chloride from 2-methoxybenzenethiol: To a solution of 2-methoxybenzenethiol (1 eq.) and isopropanol (CAS: 67-63-0) (2 eq.) in methylene chloride (0.15 M) was added batchwise N-bromosuccinimide (CAS: 128-08-5) or N-chlorosuccinimide (CAS: 128-09- 6) (4 or 3.5 equivalents), and the reaction was carried out at room temperature (when using NBS) or at 0 °C (when using NCS). The reaction mixture was stirred at room temperature until the starting material was undetectable by thin layer chromatography (TLC) (about 1 hour). Subsequently, the reaction mixture was diluted with cold saturated NaHCO3 solution and extracted with ethyl acetate (4 times). The organic extracts were combined, dried with Na2SO4 and concentrated in vacuum to give the crude product. Finally, pure 2-methoxybenzenesulfonyl chloride was purified by silica gel column chromatography or radial chromatography using a hexane/ethyl acetate/acetone solvent mixture as eluent to obtain pure 2-methoxybenzenesulfonyl chloride.
References
[1] Tetrahedron Letters, 2017, vol. 58, # 23, p. 2244 - 2247
[2] Green Chemistry, 2017, vol. 19, # 9, p. 2286 - 2295
2-METHOXYBENZENESULFONYL CHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
2-METHOXYBENZENESULFONYL CHLORIDE Suppliers
- Tel
- +1-5166625404;
- Fax
- 1-516-927-0118
- Info@alfa-chemistry.com
- Country
- United States
- ProdList
- 20405
- Advantage
- 58
- Tel
- +1-858-6993322
- Fax
- (+1)-858-876-1948
- info@accelachem.com
- Country
- United States
- ProdList
- 21193
- Advantage
- 58
- Tel
- 8485655694
- sales@alchempharmtech.com
- Country
- United States
- ProdList
- 63687
- Advantage
- 58
- Tel
- tp@aladdinsci.com
- Country
- United States
- ProdList
- 57505
- Advantage
- 58
- Tel
- +1-817863-6948 +1-（817）863-6948
- sales@aceschem.com
- Country
- United States
- ProdList
- 19632
- Advantage
- 58
- Tel
- --
- Fax
- --
- info@synthonix.com
- Country
- United States
- ProdList
- 6872
- Advantage
- 58
- Tel
- --
- Fax
- --
- Country
- United States
- ProdList
- 6773
- Advantage
- 87
- Tel
- --
- Fax
- --
- ryan.reichlyn@ryansci.com
- Country
- United States
- ProdList
- 6439
- Advantage
- 60
- Tel
- --
- Fax
- --
- acd@focussynthesis.com
- Country
- United States
- ProdList
- 2487
- Advantage
- 61
- Tel
- --
- Fax
- --
- sales@matrixscientific.com
- Country
- United States
- ProdList
- 6632
- Advantage
- 80
- Tel
- --
- Fax
- --
- sales@3bsc.com
- Country
- United States
- ProdList
- 6718
- Advantage
- 47
- Tel
- --
- Fax
- --
- rndscichem@gmail.com
- Country
- United States
- ProdList
- 569
- Advantage
- 0
- Tel
- --
- Fax
- --
- info@princetonbio.com
- Country
- United States
- ProdList
- 6934
- Advantage
- 51
- Tel
- --
- Fax
- --
- sales@astginc.com
- Country
- United States
- ProdList
- 2308
- Advantage
- 43
View Lastest Price from 2-METHOXYBENZENESULFONYL CHLORIDE manufacturers
- Product
- 2-Methoxybenzenesulfonyl chloride 10130-87-7
- Price
- US $0.00-0.00/Kg
- Min. Order
- 1KG
- Purity
- 99.0%+
- Supply Ability
- 100 tons
- Release date
- 2020-01-06
- Product
- 2-METHOXYBENZENESULFONYL CHLORIDE 10130-87-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-11