ChemicalBook > CAS DataBase List > 5-Iodo-3-methyl-2-pyridinamine

5-Iodo-3-methyl-2-pyridinamine

Product Name: 5-Iodo-3-methyl-2-pyridinamine
CAS No.: 166266-19-9
Chemical Name: 5-Iodo-3-methyl-2-pyridinamine
Synonyms: AKOS BB-8252;ASISCHEM X20904;ART-CHEM-BB B025286;2-Amino-5-iodo-3-methyL;2-AMINO-5-IODO-3-PICOLINE;5-IODO-3-METHYLPYRIDIN-2-AMINE;5-IODO-3-METHYL-2-PYRIDINAMINE;2-amino-3-methyl-5-iodopyridine;2-AMINO-5-IODO-3-METHYLPYRIDINE;2-Amino-3-methyl-5-iodipyridine
CBNumber: CB0237884
Molecular Formula: C6H7IN2
Formula Weight: 234.04
MOL File: 166266-19-9.mol

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5-Iodo-3-methyl-2-pyridinamine Property

Melting point:: 110.2-110.5°C
Boiling point:: 303.4±42.0 °C(Predicted)
Density: 1.898±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: soluble in Methanol
form: solid
pka: 5.22±0.49(Predicted)
Appearance: Light yellow to yellow Solid
Sensitive: Light Sensitive
λmax: 296nm(lit.)
InChIKey: WTHKBDPHSGITFJ-UHFFFAOYSA-N
CAS DataBase Reference: 166266-19-9(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 41
Safety Statements: 26-39
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: ADE000317
Product name: 5-Iodo-3-methyl-pyridin-2-ylamine
Purity: Aldrich
Packaging: 1g
Price: $179
Updated: 2025/07/31

TCI Chemical

Product number: A2683
Product name: 2-Amino-5-iodo-3-methylpyridine
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $96
Updated: 2025/07/31

TCI Chemical

Product number: A2683
Product name: 2-Amino-5-iodo-3-methylpyridine
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $288
Updated: 2025/07/31

TRC

Product number: I737193
Product name: 5-Iodo-3-methyl-2-pyridinamine
Packaging: 250mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA08612
Product name: 2-Amino-5-iodo-3-methylpyridine
Packaging: 5G
Price: $236.3
Updated: 2021/12/16

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5-Iodo-3-methyl-2-pyridinamine Chemical Properties,Usage,Production

Synthesis

3430-21-5

166266-19-9

General procedure for the synthesis of 2-amino-3-methyl-5-iodopyridine from 2-amino-3-methyl-5-bromopyridine: 5-bromo-3-methylpyridin-2-amine (2 g, 10.6 mmol), sodium iodide (3.2 g, 21.4 mmol), and copper iodide (0.190 g, 1.06 mmol) were added to dioxane (10 mL), the solution was degassed and tetramethylethane-1,2-diamine (0.803 mL, 1.06 mmol) was added. The mixture was heated at 110 °C overnight. After completion of the reaction, it was cooled to room temperature, water was added and the crude product was extracted with ethyl acetate. The residue was purified by column chromatography to afford 5-iodo-3-methylpyridin-2-amine as a beige solid (2.3 g, 93% yield). Similar to the procedure described in Example 40, 6-fluoro-7-(methylamino)-2,3-dihydrobenzo[e][1,3]oxazin-4-one (0.100 g, 0.51 mmol) was reacted with 5- iodo-3-methylpyridin-2-amine (0.119 g, 0.53 mmol) to give, after reversed-phase HPLC purification, the pure 3- (6-amino pyridin-3-yl) -6-fluoro-7-(methylamino)-2,3-dihydrobenzo[e][1,3]oxazin-4-one (0.020 g, 13% yield). ES-MS (M + H)+ = 303. Following the method of sulfonylurea formation described in Example 5, 3-(6-amino-5-methylpyridin-3-yl)-6-fluoro-7-(methylamino)-2,3-dihydrobenzo[e] [1,3]oxazin-4-one (0.010 g, 0.034 mmol) was coupled with ethyl (5-chlorothiophene-2-sulfonyl)-carbamate (0.048 g, 0.166 mmol) to afford 1-(5-chlorothiophene-2-ylsulfonyl)-3-(5-(6-fluoro-7-(methylamino)-4-oxo-2H-benzo[e][1,3]oxazine -3(4H)-yl)-3-methylpyridin-2-yl)urea (0.016 g, 85% yield).RP-HPLC retention time: 2.7 min; ES-MS (M + H)+ = 526.0; 1H-NMR (DMSO-d6) δ (ppm): 2.2 (s, 3H), 2.8 (s, 3H), 5.6 (s, 2H), 6.2 ( d, 1H), 6.8 (bs, 1H), 7.2 (s, 1H), 7.4 (d, 1H), 7.6 (s, 1H), 7.8 (d, 1H), 8.2 (d, 1H), 9.6 (bs, 1H).

References

[1] Patent: US2006/69093, 2006, A1. Location in patent: Page/Page column 23

5-Iodo-3-methyl-2-pyridinamine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-Iodo-3-methyl-2-pyridinamine manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 5-Iodo-3-methyl-2-pyridinamine 166266-19-9
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 10000KGS
Release date: 2025-05-30

Henan Fengda Chemical Co., Ltd

Product: 5-Iodo-3-methyl-2-pyridinamine 166266-19-9
Price: US $5.00-0.10/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-08

Dideu Industries Group Limited

Product: 5-Iodo-3-methyl-2-pyridinamine 166266-19-9
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-01

166266-19-9, 5-Iodo-3-methyl-2-pyridinamineRelated Search:

(2-AMINO-5-IODO-PYRIDIN-3-YL)-METHANOL 5-Iodo-3-methyl-2-pyridinamine 2-(tert-Butyloxycarbonyl-methylamino)-5-iodo-3-methylpyridine 5-Iodo-3-methyl-2-methylaminopyridine 2-AMINO-5-IODO-PYRIDINE-3-CARBALDEHYDE N-(5-IODO-3-METHYL-PYRIDIN-2-YL)-2,2-DIMETHYL-PROPIONAMIDE 5-IODO-6-METHYL-2-PYRIDINAMINE 2-Amino-5-iodo-4-methylpyridine-3-carbonitrile 1-(6-IODO-3,4-DIHYDRO-2H-[1,8]NAPHTHYRIDIN-1-YL)-2,2-DIMETHYL-PROPAN-1-ONE N-(5-IODO-3-METHYLPYRIDIN-2-YL)-N-METHYL-2,2-DIMETHYLPROPANAMIDE N-(5-IODO-3-METHYL-2-PYRIDINYL)-4-(TRIFLUOROMETHYL)BENZENECARBOXAMIDE RARECHEM AN KD 1064 N-(5-IODO-3-METHYL-2-PYRIDINYL)-2-FURAMIDE RARECHEM AN KA 1064 N-(5-IODO-3-METHYL-2-PYRIDINYL)-2-METHYLBENZENECARBOXAMIDE 4-CHLORO-N-(5-IODO-3-METHYL-2-PYRIDINYL)BENZENECARBOXAMIDE RARECHEM AN KB 1064 2,4-DIBROMO-6-([(5-IODO-3-METHYL-2-PYRIDINYL)AMINO]METHYL)BENZENOL

2-amino-3-methyl-5-iodopyridine

5-Iodo-3-methylpyridin-2-amine, 2-Amino-5-iodo-3-picoline

2-AMINO-3-METHYL-5-IODOPYRIDINE 98%

5-iodo-3-methyl-2-pyridinylamine

(5-iodo-3-methyl-2-pyridyl)amine

5-IODO-3-METHYL-2-PYRIDINAMINE

5-IODO-3-METHYLPYRIDIN-2-AMINE

5-IODO-3-METHYL-PYRIDIN-2-YLAMINE

AKOS BB-8252

ART-CHEM-BB B025286

ASISCHEM X20904

5-iodo-3-methyl-2-pyridinamine (en)

2-AMINO-5-IODO-3-METHYLPYRIDINE

2-AMINO-5-IODO-3-PICOLINE

2-AMINO-5-IODO-3-METHYLPYRIDIN-1-IUM

2-Amino-5-iodo-3-methyL

2-Pyridinamine, 5-iodo-3-methyl-

5-Iodo-3-methyl-2-pyridinamine ISO 9001：2015 REACH

2-Amino-3-methyl-5-iodipyridine

166266-19-9

C6H7N2I

Heterocycle-Pyridine series

amine| alkyl Iodine

Pyridines

Pyridine

Boronic Acid