ChemicalBook > CAS DataBase List > Methyl 2-fluoro-3-methoxybenzoate
Methyl 2-fluoro-3-methoxybenzoate
- Product Name
- Methyl 2-fluoro-3-methoxybenzoate
- CAS No.
- 958991-48-5
- Chemical Name
- Methyl 2-fluoro-3-methoxybenzoate
- Synonyms
- Methyl 2-fluoro-3-methoxybenzoate;methyl 2-fluoro-3-(methyloxy)benzoate;2-Fluoro-3-methoxybenzoic acid methyl ester;Benzoic acid, 2-fluoro-3-methoxy-, methyl ester;methyl 2-fluoro-3-(methyloxy)benzoate methyl 2-fluoro-3-(methyloxy)benzoate Methyl 2-fluoro-3-(methyloxy)benzoate
- CBNumber
- CB02565200
- Molecular Formula
- C9H9FO3
- Formula Weight
- 184.16
- MOL File
- 958991-48-5.mol
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Methyl 2-fluoro-3-methoxybenzoate Property
- Boiling point:
- 260.5±25.0 °C(Predicted)
- Density
- 1.184±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Solid
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Safety
- HS Code
- 2916310090
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N-Bromosuccinimide Price
TRC
- Product number
- M305413
- Product name
- Methyl2-Fluoro-3-methoxybenzoate
- Packaging
- 100mg
- Price
- $55
- Updated
- 2021/12/16
TRC
- Product number
- M305413
- Product name
- Methyl2-Fluoro-3-methoxybenzoate
- Packaging
- 250mg
- Price
- $100
- Updated
- 2021/12/16
TRC
- Product number
- M305413
- Product name
- Methyl2-Fluoro-3-methoxybenzoate
- Packaging
- 500mg
- Price
- $155
- Updated
- 2021/12/16
AK Scientific
- Product number
- V9847
- Product name
- Methyl2-fluoro-3-methoxybenzoate
- Packaging
- 1g
- Price
- $197
- Updated
- 2021/12/16
Ambeed
- Product number
- A156498
- Product name
- Methyl2-fluoro-3-methoxybenzoate
- Purity
- 97%
- Packaging
- 100mg
- Price
- $29
- Updated
- 2021/12/16
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Methyl 2-fluoro-3-methoxybenzoate Chemical Properties,Usage,Production
Synthesis
34472-65-6
137654-20-7
958991-48-5
To a suspension of 2-fluoro-3-methoxybenzoic acid (2.0 g, 11.8 mmol) in dichloromethane (20 mL) and methanol (2 mL) was added slowly and dropwise trimethylmethylsilyl diazomethane (2M ethyl ether solution, 12.3 mmol, 6.2 mL) at 0 °C. The reaction mixture was stirred at 0 °C for 30 min and then the solvent was removed by distillation under reduced pressure. The residue was diluted with ethyl acetate, adsorbed on silica gel and purified by silica gel column chromatography in two batches to give 2.0 g (92% yield) of methyl 2-fluoro-3-methoxybenzoate. The product was characterized by 1H NMR (CDCl3, 400 MHz): δ 7.48-7.44 (m, 1H), 7.15-7.09 (m, 2H), 3.93 (s, 3H), 3.91 (s, 3H).
References
[1] Patent: WO2009/32667, 2009, A1. Location in patent: Page/Page column 166-167
Methyl 2-fluoro-3-methoxybenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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Methyl 2-fluoro-3-methoxybenzoate Suppliers
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View Lastest Price from Methyl 2-fluoro-3-methoxybenzoate manufacturers
Career Henan Chemical Co
- Product
- Methyl 2-fluoro-3-methoxybenzoate 958991-48-5
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 200kg
- Release date
- 2018-12-25