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Methyl 2-fluoro-3-methoxybenzoate

Product Name
Methyl 2-fluoro-3-methoxybenzoate
CAS No.
958991-48-5
Chemical Name
Methyl 2-fluoro-3-methoxybenzoate
Synonyms
Methyl 2-fluoro-3-methoxybenzoate;methyl 2-fluoro-3-(methyloxy)benzoate;2-Fluoro-3-methoxybenzoic acid methyl ester;Benzoic acid, 2-fluoro-3-methoxy-, methyl ester;methyl 2-fluoro-3-(methyloxy)benzoate methyl 2-fluoro-3-(methyloxy)benzoate Methyl 2-fluoro-3-(methyloxy)benzoate
CBNumber
CB02565200
Molecular Formula
C9H9FO3
Formula Weight
184.16
MOL File
958991-48-5.mol
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Methyl 2-fluoro-3-methoxybenzoate Property

Boiling point:
260.5±25.0 °C(Predicted)
Density 
1.184±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
Appearance
White to off-white Solid
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Safety

HS Code 
2916310090
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
M305413
Product name
Methyl2-Fluoro-3-methoxybenzoate
Packaging
100mg
Price
$55
Updated
2021/12/16
TRC
Product number
M305413
Product name
Methyl2-Fluoro-3-methoxybenzoate
Packaging
250mg
Price
$100
Updated
2021/12/16
TRC
Product number
M305413
Product name
Methyl2-Fluoro-3-methoxybenzoate
Packaging
500mg
Price
$155
Updated
2021/12/16
AK Scientific
Product number
V9847
Product name
Methyl2-fluoro-3-methoxybenzoate
Packaging
1g
Price
$197
Updated
2021/12/16
Crysdot
Product number
CD12001553
Product name
Methyl2-fluoro-3-methoxybenzoate
Purity
95+%
Packaging
5g
Price
$344
Updated
2021/12/16
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Methyl 2-fluoro-3-methoxybenzoate Chemical Properties,Usage,Production

Synthesis

34472-65-6

137654-20-7

958991-48-5

To a suspension of 2-fluoro-3-methoxybenzoic acid (2.0 g, 11.8 mmol) in dichloromethane (20 mL) and methanol (2 mL) was added slowly and dropwise trimethylmethylsilyl diazomethane (2M ethyl ether solution, 12.3 mmol, 6.2 mL) at 0 °C. The reaction mixture was stirred at 0 °C for 30 min and then the solvent was removed by distillation under reduced pressure. The residue was diluted with ethyl acetate, adsorbed on silica gel and purified by silica gel column chromatography in two batches to give 2.0 g (92% yield) of methyl 2-fluoro-3-methoxybenzoate. The product was characterized by 1H NMR (CDCl3, 400 MHz): δ 7.48-7.44 (m, 1H), 7.15-7.09 (m, 2H), 3.93 (s, 3H), 3.91 (s, 3H).

References

[1] Patent: WO2009/32667, 2009, A1. Location in patent: Page/Page column 166-167

Methyl 2-fluoro-3-methoxybenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 2-fluoro-3-methoxybenzoate Suppliers

Aladdin Scientific
Tel
Email
tp@aladdinsci.com
Country
United States
ProdList
52923
Advantage
58
Aceschem Inc.
Tel
+1-817863-6948 +1-(817)863-6948
Email
sales@aceschem.com
Country
United States
ProdList
19632
Advantage
58
Synthonix Inc
Tel
--
Fax
--
Email
info@synthonix.com
Country
United States
ProdList
6872
Advantage
58
United States Biological
Tel
--
Fax
--
Email
chemicals@usbio.net
Country
United States
ProdList
6214
Advantage
80
Combi-Blocks Inc.
Tel
--
Fax
--
Email
sales@combi-blocks.com
Country
United States
ProdList
6618
Advantage
69
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View Lastest Price from Methyl 2-fluoro-3-methoxybenzoate manufacturers

Career Henan Chemical Co
Product
Methyl 2-fluoro-3-methoxybenzoate 958991-48-5
Price
US $1.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
200kg
Release date
2018-12-25

958991-48-5, Methyl 2-fluoro-3-methoxybenzoateRelated Search:


  • Methyl 2-fluoro-3-methoxybenzoate
  • methyl 2-fluoro-3-(methyloxy)benzoate
  • Benzoic acid, 2-fluoro-3-methoxy-, methyl ester
  • methyl 2-fluoro-3-(methyloxy)benzoate methyl 2-fluoro-3-(methyloxy)benzoate Methyl 2-fluoro-3-(methyloxy)benzoate
  • 2-Fluoro-3-methoxybenzoic acid methyl ester
  • 958991-48-5