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3,5-DibroMo-biphenyl

Product Name
3,5-DibroMo-biphenyl
CAS No.
16372-96-6
Chemical Name
3,5-DibroMo-biphenyl
Synonyms
PBB 14;3,5-DibroMo-biphenyl;3,5-Dibromo-1,1'-biphenyl;1,1'-Biphenyl, 3,5-dibromo-;3,5-DIBROMO-1-PHENYLBENZENE
CBNumber
CB02570622
Molecular Formula
C12H8Br2
Formula Weight
312
MOL File
16372-96-6.mol
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3,5-DibroMo-biphenyl Property

Melting point:
156-157℃
Boiling point:
208 °C(Press: 15 Torr)
Density 
1.7197 g/cm3(Temp: 25 °C)
refractive index 
1.6541 (589.3 nm 25℃)
storage temp. 
Sealed in dry,Room Temperature
form 
crystalline solid
color 
White
InChI
InChI=1S/C12H8Br2/c13-11-6-10(7-12(14)8-11)9-4-2-1-3-5-9/h1-8H
InChIKey
HIHYAKDOWUFGBK-UHFFFAOYSA-N
SMILES
C1(C2=CC=CC=C2)=CC(Br)=CC(Br)=C1
EPA Substance Registry System
1,1'-Biphenyl, 3,5-dibromo- (16372-96-6)
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Safety

HS Code 
2903998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

AK Scientific
Product number
X7241
Product name
3,5-Dibromo-1,1'-biphenyl
Packaging
25g
Price
$371
Updated
2021/12/16
Chemenu
Product number
CM243418
Product name
3,5-Dibromo-1,1''-biphenyl
Purity
95+%
Packaging
100g
Price
$636
Updated
2021/12/16
Crysdot
Product number
CD41001877
Product name
3,5-Dibromo-1,1'-biphenyl
Purity
97%
Packaging
100g
Price
$673
Updated
2021/12/16
Crysdot
Product number
CD41001877
Product name
3,5-Dibromo-1,1'-biphenyl
Purity
97%
Packaging
500g
Price
$2024
Updated
2021/12/16
Crysdot
Product number
CD41001877
Product name
3,5-Dibromo-1,1'-biphenyl
Purity
97%
Packaging
1000g
Price
$3373
Updated
2021/12/16
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3,5-DibroMo-biphenyl Chemical Properties,Usage,Production

Chemical Properties

Colorless liquid

Synthesis

626-39-1

98-80-6

16372-96-6

A suspension of EtOH-H2O (3 mL, v:v = 1:1) with 1,3,5-tribromobenzene (1.0 mmol), phenylboronic acid (1.2 mmol), potassium carbonate (276 mg, 2.0 mmol), and Pd/HCCP-DABP catalyst (20 mg, 0.3 mol%) was added to the Schlenk tube. The system was evacuated and backfilled three times with nitrogen. The reaction mixture was stirred at 50 °C for 2.5 hours. After completion of the reaction, it was cooled to room temperature and extracted with dichloromethane (CH2Cl2). The organic phases were combined, dried with anhydrous sodium sulfate, concentrated under reduced pressure and purified by silica gel column chromatography to give 1-phenyl-3,5-dibromobenzene. The aqueous phase was filtered through filter paper, the solid was washed with CH2Cl2, and the recovered catalyst could be used in subsequent reactions.

References

[1] Reactive and Functional Polymers, 2017, vol. 110, p. 38 - 46
[2] Patent: KR2016/69021, 2016, A. Location in patent: Paragraph 0155-0157
[3] Journal of the American Chemical Society, 1990, vol. 112, # 22, p. 8024 - 8034
[4] Patent: KR2015/53913, 2015, A. Location in patent: Paragraph 0533-0535
[5] Patent: KR2015/127023, 2015, A. Location in patent: Paragraph 0409; 0560; 0561; 0562; 0563; 0564

3,5-DibroMo-biphenyl Preparation Products And Raw materials

Raw materials

Preparation Products

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3,5-DibroMo-biphenyl Suppliers

China 92 India 1 Japan 1 Lithuania 1 United States 3 Global 98
Aladdin Scientific
Tel
Email
tp@aladdinsci.com
Country
United States
ProdList
57505
Advantage
58
Chemlex Pharmaceuticals LLC
Tel
--
Fax
--
Email
chemlexpharma@yahoo.com
Country
United States
ProdList
238
Advantage
0
Combi-Blocks Inc.
Tel
--
Fax
--
Email
sales@combi-blocks.com
Country
United States
ProdList
6618
Advantage
69
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View Lastest Price from 3,5-DibroMo-biphenyl manufacturers

Hebei Xinsheng New Material Technology Co., LTD.
Product
3,5-DibroMo-biphenyl 16372-96-6
Price
US $35.00-25.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 Ton
Release date
2023-11-07
Career Henan Chemical Co
Product
3,5-DibroMo-biphenyl 16372-96-6
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1ton
Release date
2018-08-06

16372-96-6, 3,5-DibroMo-biphenylRelated Search:

ACETONE-D6 Copper(II) sulfate pentahydrate

  • 3,5-DibroMo-biphenyl
  • 3,5-DIBROMO-1-PHENYLBENZENE
  • PBB 14
  • 1,1'-Biphenyl, 3,5-dibromo-
  • 3,5-Dibromo-1,1'-biphenyl
  • 16372-96-6