ChemicalBook > CAS DataBase List > 2-Chloro-N-methylacetamide

2-Chloro-N-methylacetamide

Product Name: 2-Chloro-N-methylacetamide
CAS No.: 96-30-0
Chemical Name: 2-Chloro-N-methylacetamide
Synonyms: N-Methylchloroacetamide;chloroacetylmethylamide;N-METHYL-2-CHLOROACETAMIDE;96-30-0;usafdo-35;USAF do-35;WLN: G1VM1;OTAVA-BB BB7020410071;2-chloro-n-methyl-acetamid;2-CHLORO-N-METHYLACETAMIDE
CBNumber: CB0341389
Molecular Formula: C3H6ClNO
Formula Weight: 107.54
MOL File: 96-30-0.mol

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2-Chloro-N-methylacetamide Property

Melting point:: 38-40°C
Boiling point:: 112-115°C 20mm
Density: 1.127±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: DMSO (Slightly), Methanol (Slightly)
form: Solid
pka: 14.38±0.46(Predicted)
color: White to Off-White
InChI: InChI=1S/C3H6ClNO/c1-5-3(6)2-4/h2H2,1H3,(H,5,6)
InChIKey: HOZLOOPIXHWKCI-UHFFFAOYSA-N
SMILES: C(NC)(=O)CCl
CAS DataBase Reference: 96-30-0(CAS DataBase Reference)
NIST Chemistry Reference: ClCON(CH3)2(96-30-0)

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Safety

Risk Statements: 36/37/38-43-22
Safety Statements: 26-36/37/39-36/37-24
RTECS: AB5775000
HazardClass: IRRITANT
HS Code: 29241990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: OTV000964
Product name: 2-Chloro-N-methylacetamide
Packaging: 1g
Price: $73.1
Updated: 2025/07/31

TCI Chemical

Product number: C3014
Product name: 2-Chloro-N-methylacetamide
Purity: >98.0%(GC)
Packaging: 5g
Price: $63
Updated: 2025/07/31

TCI Chemical

Product number: C3014
Product name: 2-Chloro-N-methylacetamide
Purity: >98.0%(GC)
Packaging: 25g
Price: $211
Updated: 2025/07/31

TRC

Product number: C368350
Product name: 2-Chloro-N-methylacetamide
Packaging: 1g
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC119482
Product name: 2-Chloro-N-methylacetamide
Packaging: 2g
Price: $50
Updated: 2021/12/16

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2-Chloro-N-methylacetamide Chemical Properties,Usage,Production

Uses

2-Chloro-N-methylacetamide is an intermediate used to prepare piperidinylamino pyrrolopyrimidines as selective Janus kinase inhibitors for the treatment of autoimmune diseases and organ transplant rejection.

Synthesis

To methylamine hydrochloride (896 mg, 13.3 mmol) and Na2C03 (5630 mg, 53 mmol) in water (26 mL) was added 2-chloroacetyl chloride (1500 mg, 13.3 mmol). The mixture was stirred at r.t. for lh and extracted with EtOAc (2x). The combined organic layers were dried over Na2S04 and concentrated to provide 2-Chloro-N-methylacetamide (1200 mg, 84%).

References

[1] Journal of the Chemical Society. Perkin Transactions 2, 2000, # 9, p. 1819 - 1831
[2] Patent: WO2016/210330, 2016, A1. Location in patent: Paragraph 0180-0181
[3] Journal of the Chemical Society. Perkin Transactions 1, 2001, # 1, p. 87 - 93

2-Chloro-N-methylacetamide Preparation Products And Raw materials

Raw materials

Preparation Products

N-METHYL-2-PIPERAZIN-1-YLACETAMIDE

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View Lastest Price from 2-Chloro-N-methylacetamide manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Chloro-N-methylacetamide 96-30-0
Price: US $1.00-4.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200000KG
Release date: 2025-09-05

Shaanxi Dideu New Materials Co. Ltd

Product: 2-Chloro-N-methylacetamide 96-30-0
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10000KGS
Release date: 2025-02-26

Zhuozhou Wenxi import and Export Co., Ltd

Product: 2-Chloro-N-methylacetamide 96-30-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

96-30-0, 2-Chloro-N-methylacetamideRelated Search:

tert-Butyldimethylsilyl chloride Epichlorohydrin N-(HYDROXYMETHYL)ACETAMIDE Chloroacetamide N-Methylacetamide N,N-Dimethylacetamide 2-Chloro-N-[4-chloro-2-(2-chlorobenzoyl)phenyl]acetamide 3,5-DICHLORO-2-PYRIDONE 5-Chlorouracil N,N'-OCTAMETHYLENEBIS(DICHLOROACETAMIDE) 2-Chloro-N-(2,6-dimethylphenyl)acetamide N-(CHLOROACETYL)-2-(TRIFLUOROMETHYL)ANILINE 2,2,2-TRICHLORO-3'-TRIFLUOROMETHYLACETANILIDE Chloromethyl methyl ether Chloroacetic acid N-(CHLOROACETYL)-4-FLUOROANILINE Difluorochloromethane 2-Chloro-N,N-diethylacetamide

OTAVA-BB BB7020410071

N-METHYL-2-CHLOROACETAMIDE

chloroacetylmethylamide

2-CHLORO-N-METHYLACETAMIDE

2-chloro-n-methyl-acetamid

Acetamide, 2-chloro-N-methyl-

alpha-Chloro-N-methylacetamide

N-Methylchloroacetamide

USAF do-35

usafdo-35

2-chloro-N-methyl-ethanamide

2-chloro-N-methylacetamide(SALTDATA: FREE)

2-Chloro-<i>N</i>-methylacetamide

WLN: G1VM1

2-Chloro-N-methylacetamide &gt

2-Chloro-N-methylacetamide,97%

2-Chloro-N-methylacetamide ISO 9001：2015 REACH

96-30-0

Acids and Derivatives