ChemicalBook > CAS DataBase List > 4,4-DIMETHYLCYCLOHEXYLAMINE

4,4-DIMETHYLCYCLOHEXYLAMINE

Product Name: 4,4-DIMETHYLCYCLOHEXYLAMINE
CAS No.: 20615-18-3
Chemical Name: 4,4-DIMETHYLCYCLOHEXYLAMINE
Synonyms: 4,4-DIMETHYLCYCLOHEXYLAMINE;4,4-DIMETHYLCYCLOHEXANAMINE;CyclohexylaMine,4,4-diMethyl-;CyclohexanaMine,4,4-diMethyl-;4,4-diMethylcyclohexan-1-aMine;4-AMINO-1,1-DIMETHYLCYCLOHEXANE
CBNumber: CB0353755
Molecular Formula: C8H17N
Formula Weight: 127.23
MOL File: 20615-18-3.mol

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4,4-DIMETHYLCYCLOHEXYLAMINE Property

storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: D456875
Product name: 4,4-Dimethylcyclohexan-1-amine
Packaging: 250mg
Price: $75
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0377921
Product name: 4,4-DIMETHYLCYCLOHEXANAMINE
Purity: 95.00%
Packaging: 5MG
Price: $495.32
Updated: 2021/12/16

AK Scientific

Product number: 0566AB
Product name: 4,4-Dimethylcyclohexanamine
Packaging: 5g
Price: $971
Updated: 2021/12/16

Crysdot

Product number: CD13018617
Product name: 4,4-Dimethylcyclohexanamine
Purity: 97%
Packaging: 10g
Price: $1376
Updated: 2021/12/16

Ambeed

Product number: A421546
Product name: 4,4-Dimethylcyclohexanamine
Purity: 97%
Packaging: 10g
Price: $1526
Updated: 2021/12/16

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4,4-DIMETHYLCYCLOHEXYLAMINE Chemical Properties,Usage,Production

Synthesis

4701-96-6

20615-18-3

The general procedure for the synthesis of 4,4-dimethylcyclohexylamine from 4,4-dimethylcyclohexanone oxime was as follows: 4,4-dimethylcyclohexanone oxime (10 g, 71 mmol, 1 equiv.) was dissolved in ethanol (100 mL) and Raney Ni catalyst (1 g, 10% w/w) was added. The reaction mixture was stirred under hydrogen atmosphere (50 psi) for 4 hours. Upon completion of the reaction, the catalyst was removed by filtration through a diatomaceous earth pad. Hydrochloric acid (1 M in H2O, 100 mL, 100 mmol, 1.4 eq.) was added to the filtrate and the resulting precipitate was collected by filtration and dissolved in water. The aqueous phase was washed with ether and alkalized to a strong base with potassium hydroxide pellets and subsequently extracted twice with dichloromethane. The organic phases were combined, dried over magnesium sulfate and concentrated in vacuum to afford 4,4-dimethylcyclohexylamine (8 g, 89% yield) as a clear oil, which can be used in the next reaction without further purification.

References

[1] Patent: WO2004/50619, 2004, A1. Location in patent: Page 78-79
[2] Patent: WO2014/37900, 2014, A1. Location in patent: Page/Page column 33
[3] Journal of medicinal chemistry, 1971, vol. 14, # 17, p. 600 - 614
[4] Journal of the Chemical Society [Section] B: Physical Organic, 1971, p. 1047 - 1050

4,4-DIMETHYLCYCLOHEXYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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20615-18-3, 4,4-DIMETHYLCYCLOHEXYLAMINERelated Search:

5-CHOLESTEN-3BETA-[N-PHENYL]AMINE Vincristine sulfate CONESSINE FUNTUMINE BASE 2,3-dimethylcyclohexylamine,mixtureofisomer N,N-Dimethylcyclohexylamine,98+%,N,N-Dimethylcyclohexylamine (DMCHA),N,N-DIMETHYLCYCLOHEXYLAMINE,Dimethylcyclohexylamine 7,7-AZO-3-A,12-A-DIHYDROXYTAUROCHOLANIC ACID, SODIUM SALT (+)-ISOPINOCAMPHEYLAMINE I-SAP (-)-ISOPINOCAMPHEYLAMINE 4,4-DIMETHYLCYCLOHEXYLAMINE HYDROCHLORIDE 2,6-DIMETHYLCYCLOHEXYLAMINE 2-(2-butoxyethoxy)ethyl dihydrogen phosphate, compound with N,N-dimethylcyclohexylamine 2-((4-CHLOROPHENYL)DIAZENYL)-5,5-DIMETHYLCYCLOHEXANE-1,3-DIONE (25β)-3β-Amino-16α,23β-epoxy-16,28-seco-5α-solanidan-23-ol 5-(2-([3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]AMINO)ETHYL)-3,3-SPIRO-2-(5,5-DIMETHYL CYCLOHEXANE-1,3-DIONYL)DIHYDRO-2H-PYRROLO[3,4-D]ISOXAZOLE-4,6-(3H,5H)-DIONE SALOR-INT L202096-1EA 125I-SAP

4-AMINO-1,1-DIMETHYLCYCLOHEXANE

4,4-DIMETHYLCYCLOHEXYLAMINE

4,4-diMethylcyclohexan-1-aMine

CyclohexanaMine,4,4-diMethyl-

CyclohexylaMine,4,4-diMethyl-

4,4-DIMETHYLCYCLOHEXANAMINE

20615-18-3