3-CHLORO-2-IODOPHENOL

Product Name: 3-CHLORO-2-IODOPHENOL
CAS No.: 858854-82-7
Chemical Name: 3-CHLORO-2-IODOPHENOL
Synonyms: 3-Choro-2-iodophenol;3-CHLORO-2-IODOPHENOL;Phenol, 3-chloro-2-iodo-
CBNumber: CB0390983
Molecular Formula: C6H4ClIO
Formula Weight: 254.45
MOL File: 858854-82-7.mol

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3-CHLORO-2-IODOPHENOL Property

Melting point:: 56 °C
Boiling point:: 225.6±20.0 °C(Predicted)
Density: 2.087±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 7.55±0.10(Predicted)
Appearance: Off-white to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C382025
Product name: 3-Chloro-2-iodophenol
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Ark Pharm

Product number: AK151227
Product name: 3-Chloro-2-iodophenol
Purity: 97+%
Packaging: 100mg
Price: $28
Updated: 2021/12/16

AK Scientific

Product number: Z0905
Product name: 3-Choro-2-iodophenol
Packaging: 250mg
Price: $124
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0063561
Product name: 3-CHLORO-2-IODOPHENOL
Purity: 95.00%
Packaging: 5MG
Price: $498.18
Updated: 2021/12/16

Alichem

Product number: 858854827
Product name: 3-Chloro-2-iodophenol
Packaging: 1g
Price: $513.32
Updated: 2021/12/16

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3-CHLORO-2-IODOPHENOL Chemical Properties,Usage,Production

Synthesis

863870-77-3

858854-82-7

Step 3: Sodium hydroxide (32.0 g, 800 mmol) was slowly added to a 400 mL ethanol solution containing 3-chloro-2-iodophenyl N,N-diethylcarbamate (57.0 g, 161 mmol) at 25 °C. The reaction mixture was heated to reflux and maintained for 2 hours. Upon completion of the reaction, the ethanol solvent was removed by distillation under reduced pressure. The residue was dissolved in 400 mL of water and subsequently extracted with petroleum ether. The aqueous phase was neutralized with 2N hydrochloric acid solution and extracted with ethyl acetate. All organic phases were combined, washed with saturated brine and dried over anhydrous sodium sulfate. Finally, the organic solvent was removed by distillation under reduced pressure to afford the target product 3-chloro-2-iodophenol (41.0 g, quantitative yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 5.58 (brs, 1H), 6.90 (dd, J = 1.2,8.4 Hz, 1H), 7.06 (dd, J = 1.2,8.0 Hz, 1H), 7.21 (t, J = 8.0 Hz, 1H).

References

[1] Patent: US2017/145005, 2017, A1. Location in patent: Paragraph 0368; 0375; 0376; 0377
[2] Journal of Organic Chemistry, 2005, vol. 70, # 16, p. 6548 - 6551
[3] Journal of Organic Chemistry, 2007, vol. 72, # 14, p. 5113 - 5118
[4] Organic and Biomolecular Chemistry, 2010, vol. 8, # 17, p. 3860 - 3864
[5] Journal of Organic Chemistry, 2011, vol. 76, # 9, p. 3416 - 3437

3-CHLORO-2-IODOPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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3-CHLORO-2-IODOPHENOL Suppliers

China 52 India 1 United Kingdom 1 United States 4 Global 58

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View Lastest Price from 3-CHLORO-2-IODOPHENOL manufacturers

Career Henan Chemical Co

Product: 3-CHLORO-2-IODOPHENOL 858854-82-7
Price: US $2.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: ask
Release date: 2020-01-08

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