3-CHLORO-2-IODOPHENOL

Product Name: 3-CHLORO-2-IODOPHENOL
CAS No.: 858854-82-7
Chemical Name: 3-CHLORO-2-IODOPHENOL
Synonyms: 3-Choro-2-iodophenol;3-CHLORO-2-IODOPHENOL;Phenol, 3-chloro-2-iodo-
CBNumber: CB0390983
Molecular Formula: C6H4ClIO
Formula Weight: 254.45
MOL File: 858854-82-7.mol

More

Less

3-CHLORO-2-IODOPHENOL Property

Melting point:: 56 °C
Boiling point:: 225.6±20.0 °C(Predicted)
Density: 2.087±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 7.55±0.10(Predicted)
Appearance: Off-white to yellow Solid

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: C382025
Product name: 3-Chloro-2-iodophenol
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Ark Pharm

Product number: AK151227
Product name: 3-Chloro-2-iodophenol
Purity: 97+%
Packaging: 100mg
Price: $28
Updated: 2021/12/16

AK Scientific

Product number: Z0905
Product name: 3-Choro-2-iodophenol
Packaging: 250mg
Price: $124
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0063561
Product name: 3-CHLORO-2-IODOPHENOL
Purity: 95.00%
Packaging: 5MG
Price: $498.18
Updated: 2021/12/16

Ambeed

Product number: A379289
Product name: 3-Chloro-2-iodophenol
Purity: 97%
Packaging: 100mg
Price: $28
Updated: 2021/12/16

More

Less

3-CHLORO-2-IODOPHENOL Chemical Properties,Usage,Production

Synthesis

863870-77-3

858854-82-7

Step 3: Sodium hydroxide (32.0 g, 800 mmol) was slowly added to a 400 mL ethanol solution containing 3-chloro-2-iodophenyl N,N-diethylcarbamate (57.0 g, 161 mmol) at 25 °C. The reaction mixture was heated to reflux and maintained for 2 hours. Upon completion of the reaction, the ethanol solvent was removed by distillation under reduced pressure. The residue was dissolved in 400 mL of water and subsequently extracted with petroleum ether. The aqueous phase was neutralized with 2N hydrochloric acid solution and extracted with ethyl acetate. All organic phases were combined, washed with saturated brine and dried over anhydrous sodium sulfate. Finally, the organic solvent was removed by distillation under reduced pressure to afford the target product 3-chloro-2-iodophenol (41.0 g, quantitative yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 5.58 (brs, 1H), 6.90 (dd, J = 1.2,8.4 Hz, 1H), 7.06 (dd, J = 1.2,8.0 Hz, 1H), 7.21 (t, J = 8.0 Hz, 1H).

References

[1] Patent: US2017/145005, 2017, A1. Location in patent: Paragraph 0368; 0375; 0376; 0377
[2] Journal of Organic Chemistry, 2005, vol. 70, # 16, p. 6548 - 6551
[3] Journal of Organic Chemistry, 2007, vol. 72, # 14, p. 5113 - 5118
[4] Organic and Biomolecular Chemistry, 2010, vol. 8, # 17, p. 3860 - 3864
[5] Journal of Organic Chemistry, 2011, vol. 76, # 9, p. 3416 - 3437

3-CHLORO-2-IODOPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

3-CHLORO-2-IODOPHENOL Suppliers

China 52 India 1 United Kingdom 1 United States 4 Global 58

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

ShangHai AmK Pharmaceutical Technology Co., Ltd.

Tel: 微信 17321281695 18019252918
Fax: 17321281695
Email: sale@amkchem.com
Country: China
ProdList: 15136
Advantage: 55

Tianjin Anhao Biological Technology Co., Ltd.

Tel
Email: sales@ahpharmatech.com
Country: China
ProdList: 5734
Advantage: 55

Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

Tel: 025-66028182 18626450290
Email: yftan@aikonchem.com
Country: China
ProdList: 16679
Advantage: 50

Changzhou Anxuan Chemical, Co., Ltd.

Tel: 13912302692
Fax: 0519-88064678
Email: sales@anxuanchem.com
Country: China
ProdList: 4828
Advantage: 58

SuZhou ShiYa Biopharmaceuticals, Inc.

Tel: 0512-0512-52358471 17715136450
Fax: 05125235 6881
Email: sales@shiyabiopharm.com
Country: China
ProdList: 12127
Advantage: 58

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Suzhou Shanyang Pharmaceutical Technology Co.,

Tel: 0512-63268889 18506119477
Email: 82169840@qq.com
Country: China
ProdList: 592
Advantage: 58

Capot Chemical Co.,Ltd.

Tel: +86-（0）57185586718; +8613336195806
Fax: +86-571-85864795
Email: sales@capot.com
Country: China
ProdList: 29735
Advantage: 60

More

Less

View Lastest Price from 3-CHLORO-2-IODOPHENOL manufacturers

Career Henan Chemical Co

Product: 3-CHLORO-2-IODOPHENOL 858854-82-7
Price: US $2.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: ask
Release date: 2020-01-08

858854-82-7, 3-CHLORO-2-IODOPHENOLRelated Search:

2-Iodophenol 6-IODO-2,4,5-TRICHLOROPHENOL 3-CHLORO-2-IODOPHENOL 3-CHLORO-2-IODOPHENYL N,N-DIETHYLCARBAMATE AKOS B028912 4-BROMO-3-CHLORO-2,6-DIIODOPHENOL

3-CHLORO-2-IODOPHENOL

3-Choro-2-iodophenol

Phenol, 3-chloro-2-iodo-

858854-82-7

pharmacetical