ChemicalBook > CAS DataBase List > 3-CHLORO-2-IODOPHENOL

3-CHLORO-2-IODOPHENOL

Product Name
3-CHLORO-2-IODOPHENOL
CAS No.
858854-82-7
Chemical Name
3-CHLORO-2-IODOPHENOL
Synonyms
3-Choro-2-iodophenol;3-CHLORO-2-IODOPHENOL;Phenol, 3-chloro-2-iodo-
CBNumber
CB0390983
Molecular Formula
C6H4ClIO
Formula Weight
254.45
MOL File
858854-82-7.mol
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3-CHLORO-2-IODOPHENOL Property

Melting point:
56 °C
Boiling point:
225.6±20.0 °C(Predicted)
Density 
2.087±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
7.55±0.10(Predicted)
Appearance
Off-white to yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C382025
Product name
3-Chloro-2-iodophenol
Packaging
100mg
Price
$60
Updated
2021/12/16
Ark Pharm
Product number
AK151227
Product name
3-Chloro-2-iodophenol
Purity
97+%
Packaging
100mg
Price
$28
Updated
2021/12/16
AK Scientific
Product number
Z0905
Product name
3-Choro-2-iodophenol
Packaging
250mg
Price
$124
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0063561
Product name
3-CHLORO-2-IODOPHENOL
Purity
95.00%
Packaging
5MG
Price
$498.18
Updated
2021/12/16
Alichem
Product number
858854827
Product name
3-Chloro-2-iodophenol
Packaging
1g
Price
$513.32
Updated
2021/12/16
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3-CHLORO-2-IODOPHENOL Chemical Properties,Usage,Production

Synthesis

863870-77-3

858854-82-7

Step 3: Sodium hydroxide (32.0 g, 800 mmol) was slowly added to a 400 mL ethanol solution containing 3-chloro-2-iodophenyl N,N-diethylcarbamate (57.0 g, 161 mmol) at 25 °C. The reaction mixture was heated to reflux and maintained for 2 hours. Upon completion of the reaction, the ethanol solvent was removed by distillation under reduced pressure. The residue was dissolved in 400 mL of water and subsequently extracted with petroleum ether. The aqueous phase was neutralized with 2N hydrochloric acid solution and extracted with ethyl acetate. All organic phases were combined, washed with saturated brine and dried over anhydrous sodium sulfate. Finally, the organic solvent was removed by distillation under reduced pressure to afford the target product 3-chloro-2-iodophenol (41.0 g, quantitative yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 5.58 (brs, 1H), 6.90 (dd, J = 1.2,8.4 Hz, 1H), 7.06 (dd, J = 1.2,8.0 Hz, 1H), 7.21 (t, J = 8.0 Hz, 1H).

References

[1] Patent: US2017/145005, 2017, A1. Location in patent: Paragraph 0368; 0375; 0376; 0377
[2] Journal of Organic Chemistry, 2005, vol. 70, # 16, p. 6548 - 6551
[3] Journal of Organic Chemistry, 2007, vol. 72, # 14, p. 5113 - 5118
[4] Organic and Biomolecular Chemistry, 2010, vol. 8, # 17, p. 3860 - 3864
[5] Journal of Organic Chemistry, 2011, vol. 76, # 9, p. 3416 - 3437

3-CHLORO-2-IODOPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-CHLORO-2-IODOPHENOL manufacturers

Career Henan Chemical Co
Product
3-CHLORO-2-IODOPHENOL 858854-82-7
Price
US $2.00/KG
Min. Order
1g
Purity
98%min
Supply Ability
ask
Release date
2020-01-08

858854-82-7, 3-CHLORO-2-IODOPHENOLRelated Search:

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  • 3-CHLORO-2-IODOPHENOL
  • 3-Choro-2-iodophenol
  • Phenol, 3-chloro-2-iodo-
  • 858854-82-7
  • pharmacetical