CARBONIC ACID DI-2-PYRIDYL ESTER

ChemicalBook > CAS DataBase List > CARBONIC ACID DI-2-PYRIDYL ESTER

CARBONIC ACID DI-2-PYRIDYL ESTER

Product Name: CARBONIC ACID DI-2-PYRIDYL ESTER
CAS No.: 1659-31-0
Chemical Name: CARBONIC ACID DI-2-PYRIDYL ESTER
Synonyms: DI-2-PYRIDYL CARBONATE;Dipyridin-2-yl carbonate;2-Pyridinol carbonate;bis(2-pyridyl) carbonate;Carbonicaciddipyridylester;Di-2-pyridyl Carbonate >2-Pyridinol, 2,2'-carbonate;CARBONIC ACID DI-2-PYRIDYL ESTER;DPC Carbonic acid di-2-pyridyl ester;Carbonic acid di-2-pyridyl ester(DPC)
CBNumber: CB0422460
Molecular Formula: C11H8N2O3
Formula Weight: 216.19
MOL File: 1659-31-0.mol

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CARBONIC ACID DI-2-PYRIDYL ESTER Property

Melting point:: 90 °C
Boiling point:: 351.6±17.0 °C(Predicted)
Density: 1.307
Flash point:: 166.438℃
storage temp.: Inert atmosphere,2-8°C
pka: 0.63±0.12(Predicted)
form: powder to crystal
color: White to Light yellow
InChIKey: GCSAXWHQFYOIFE-UHFFFAOYSA-N
CAS DataBase Reference: 1659-31-0(CAS DataBase Reference)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TCI Chemical

Product number: C1407
Product name: Di-2-pyridyl Carbonate
Purity: >98.0%(T)
Packaging: 1g
Price: $45
Updated: 2024/03/01

TCI Chemical

Product number: C1407
Product name: Di-2-pyridyl Carbonate
Purity: >98.0%(T)
Packaging: 5g
Price: $129
Updated: 2024/03/01

TRC

Product number: D492765
Product name: Di-2-pyridyl Carbonate
Packaging: 2.5g
Price: $120
Updated: 2021/12/16

Ark Pharm

Product number: P000288588
Product name: Dipyridin-2-yl carbonate
Purity: 97%
Packaging: 1g
Price: $10
Updated: 2021/12/16

Matrix Scientific

Product number: 076540
Product name: Dipyridin-2-yl carbonate
Purity: 95+%
Packaging: 1g
Price: $10
Updated: 2021/12/16

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CARBONIC ACID DI-2-PYRIDYL ESTER Chemical Properties,Usage,Production

Chemical Properties

White to faint yellow crystalline powder

Uses

Di-2-pyridyl carbonate is used as a coupling agent in the esterification of carboxylic acids (e.g. 3-Cyclohexenylcarboxylic acid [C988195]). Di-2-pyridyl carbonate is also used as a reagent to synthesize active carbonates (e.g. benzyl 2-pyridyl carbonate) and carbamates (e.g. 3-Pyridyl diethylcarbamate [P992950]).

Preparation

A solution of phosgene (2.5 m in toluene, 2 mL, 5.0 mmol) was diluted with dichloromethane (8 mL) and then a solution of 2-pyridinol 853 (950 mg, 10 mmol) and triethylamine (1.214 g, 10.2 mmol) in dichloromethane (20 mL) was added at 0 ℃. The reaction mixture was stirred at 0℃ for 1 h, then washed with cold 5% NaHCO3 solution (20 mL) and cold saturated brine (20 mL), dried over MgSO4, and filtered. The filtrate was concentrated to dryness to give di-2-pyridyl carbonate, DPC, 725 (972 mg) in 90% yield. It was recrystallized from dichloromethane/petroleum ether (811 mg, 75%); mp 84–86℃. DPC has also been produced as its hydrochloride salt 877, in a more facile procedure on a larger scale, in 97% yield.

CARBONIC ACID DI-2-PYRIDYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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CARBONIC ACID DI-2-PYRIDYL ESTER Suppliers

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View Lastest Price from CARBONIC ACID DI-2-PYRIDYL ESTER manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: Di-2-pyridyl Carbonate 1659-31-0
Price: US $1.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200000KG
Release date: 2020-01-08

Henan Aochuang Chemical Co.,Ltd.

Product: CARBONIC ACID DI-2-PYRIDYL ESTER 1659-31-0
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-09-26

Zhuozhou Wenxi import and Export Co., Ltd

Product: CARBONIC ACID DI-2-PYRIDYL ESTER 1659-31-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

1659-31-0, CARBONIC ACID DI-2-PYRIDYL ESTERRelated Search:

Vinylene carbonate Iodomethyl pivalate BENZYL PHENYL CARBONATE 97 TETRAETHYLENE GLYCOL DI-P-TOSYLATE Diethyl ketomalonate Cyhalothrin Trifluoromethanesulfonic acid Cesium hydroxide 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride CARBONIC ACID DI-2-PYRIDYL ESTER

Carbonic acid di-2-pyridyl esterCarbonic acid di-2-pyridyl ester

Dipyridin-2-yl carbonate

2-Pyridinol carbonate

Di-2-pyridyl carbonate≥ 98%(Titration)

DPC Carbonic acid di-2-pyridyl ester

Carbonicaciddipyridylester

CARBONIC ACID DI-2-PYRIDYL ESTER

DI-2-PYRIDYL CARBONATE

Carbonic acid di-2-pyridyl ester(DPC)

Di-2-pyridyl Carbonate &gt

2-Pyridinol, 2,2'-carbonate

bis(2-pyridyl) carbonate

1659-31-0

C11H8N2O3

Condensation & Active Esterification

Synthetic Organic Chemistry