ChemicalBook > CAS DataBase List > 2-BROMO-4-CHLORO-6-NITROPHENYLAMINE

2-BROMO-4-CHLORO-6-NITROPHENYLAMINE

Product Name
2-BROMO-4-CHLORO-6-NITROPHENYLAMINE
CAS No.
827-25-8
Chemical Name
2-BROMO-4-CHLORO-6-NITROPHENYLAMINE
Synonyms
2-BROMO-4-CHLORO-6-NITROANILINE;2-Bromo-4-chloro-6-nitrobenzenamine;2-BROMO-4-CHLORO-6-NITROPHENYLAMINE;2-Amino-3-bromo-5-chloronitrobenzene;2-Bromo-4-chloro-6-nitroaniline, 97%;Benzenamine, 2-bromo-4-chloro-6-nitro-;2-BROMO-4-CHLORO-6-NITROPHENYLAMINE ISO 9001:2015 REACH
CBNumber
CB0424570
Molecular Formula
C6H4BrClN2O2
Formula Weight
251.47
MOL File
827-25-8.mol
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2-BROMO-4-CHLORO-6-NITROPHENYLAMINE Property

Melting point:
106 °C
Boiling point:
329.3±37.0 °C(Predicted)
Density 
1.909±0.06 g/cm3(Predicted)
storage temp. 
2-8°C(protect from light)
pka
-3.20±0.25(Predicted)
Appearance
White to yellow Solid
CAS DataBase Reference
827-25-8(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
HS Code 
2921420090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B678828
Product name
2-Bromo-4-chloro-6-nitrophenylamine
Packaging
500mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB149640
Product name
2-Bromo-4-chloro-6-nitroaniline
Packaging
500mg
Price
$60
Updated
2021/12/16
SynQuest Laboratories
Product number
4655-D-X0
Product name
2-Bromo-4-chloro-6-nitroaniline
Packaging
25g
Price
$98
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB149640
Product name
2-Bromo-4-chloro-6-nitroaniline
Packaging
1g
Price
$103
Updated
2021/12/16
Oakwood
Product number
062563
Product name
2-Bromo-4-chloro-6-nitroaniline
Purity
98%
Packaging
1g
Price
$10
Updated
2021/12/16
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2-BROMO-4-CHLORO-6-NITROPHENYLAMINE Chemical Properties,Usage,Production

Synthesis Reference(s)

Tetrahedron Letters, 35, p. 7055, 1994 DOI: 10.1016/0040-4039(94)88224-X

Synthesis

89-63-4

827-25-8

General procedure for the synthesis of 2-nitro-4-chloro-6-bromoaniline from 4-chloro-2-nitroaniline: 4-chloro-2-nitroaniline (5.1 g, 30 mmol) and N-bromosuccinimide (6.2 g, 36 mmol) were dissolved in acetonitrile (50 mL) and the reaction was heated to reflux overnight. After completion of the reaction, the mixture was cooled to room temperature and diluted with ethyl acetate (50 mL). Subsequently, the mixture was washed with saturated aqueous potassium carbonate (100 mL x 2). The organic phase was separated, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford the target compound 2-nitro-4-chloro-6-bromoaniline (109a) as a yellow solid (8.1 g, 100% yield).LCMS analysis showed [M + H]+ of 253.1 H NMR (500 MHz, CDCl3) δ 8.17 (d, J = 2.5 Hz, 1H), 1 H 7.71 (d, J = 2.5 Hz, 1H), 6.64 (s, 2H).

References

[1] Patent: US2013/116262, 2013, A1. Location in patent: Paragraph 0260
[2] Patent: WO2018/13776, 2018, A1. Location in patent: Page/Page column 108
[3] Patent: WO2018/13770, 2018, A1. Location in patent: Page/Page column 80
[4] Patent: WO2018/13774, 2018, A1. Location in patent: Page/Page column 155
[5] Tetrahedron Letters, 1994, vol. 35, # 38, p. 7055 - 7056

2-BROMO-4-CHLORO-6-NITROPHENYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-4-CHLORO-6-NITROPHENYLAMINE Suppliers

Nantong Haochun Biotechnology Co., Ltd
Tel
0513-88562884 15162883737
Email
425424481@qq.com
Country
China
ProdList
65
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58
J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
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76
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44801
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Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Country
China
ProdList
18207
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66
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Fax
021-50795055
Email
sales@accelachem.com
Country
China
ProdList
11035
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Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
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64
China DongFan Chemical Co.,LTD
Tel
86-0571-85151182
Fax
86-0571-85151182
Country
China
ProdList
5691
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66
Shanghai Sunway Pharmaceutical Technology Co., Ltd
Tel
18270980682
Fax
021 51613951
Email
mlcheng@sunwaypharm.cn
Country
China
ProdList
8669
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57
SuZhou ShiYa Biopharmaceuticals, Inc.
Tel
86(512)5235 8471 17715136450
Fax
86(512)5235 6881
Email
sales@shiyabiopharm.com
Country
China
ProdList
4169
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9ding chemical ( Shanghai) Limited
Tel
4009209199
Fax
86-021-52271987
Email
sales@9dingchem.com
Country
China
ProdList
18209
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View Lastest Price from 2-BROMO-4-CHLORO-6-NITROPHENYLAMINE manufacturers

Henan Fengda Chemical Co., Ltd
Product
2-BROMO-4-CHLORO-6-NITROPHENYLAMINE 827-25-8
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-26
Honest Joy Holdings Limited
Product
2-Bromo-4-chloro-6-nitrophenylamine 827-25-8
Price
US $0.00/KG
Min. Order
1KG
Purity
99.5%
Supply Ability
100 tons
Release date
2022-02-20
Zhuozhou Wenxi import and Export Co., Ltd
Product
2-BROMO-4-CHLORO-6-NITROPHENYLAMINE 827-25-8
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-08-11

827-25-8, 2-BROMO-4-CHLORO-6-NITROPHENYLAMINERelated Search:


  • 2-BROMO-4-CHLORO-6-NITROANILINE
  • 2-BROMO-4-CHLORO-6-NITROPHENYLAMINE
  • 2-Bromo-4-chloro-6-nitrobenzenamine
  • 2-Amino-3-bromo-5-chloronitrobenzene
  • Benzenamine, 2-bromo-4-chloro-6-nitro-
  • 2-BROMO-4-CHLORO-6-NITROPHENYLAMINE ISO 9001:2015 REACH
  • 2-Bromo-4-chloro-6-nitroaniline, 97%
  • 827-25-8
  • 927-25-8
  • C6H4BrClN2O2
  • C6H4N2O2BrCl
  • Alkylanilines
  • Anilines, Amides & Amines
  • Bromine Compounds
  • Chlorine Compounds
  • Nitro Compounds