3-METHOXYISONICOTINALDEHYDE
- Product Name
- 3-METHOXYISONICOTINALDEHYDE
- CAS No.
- 1849-52-1
- Chemical Name
- 3-METHOXYISONICOTINALDEHYDE
- Synonyms
- 3-METHOXYISONICOTINALDEHYDE;3-methoxypyridine-4-carbaldehyde;3-Methoxy-4-Pyridinecarboxaldehyde;3-Methoxypyridine-4-carboxaldehyde;4-Pyridinecarboxaldehyde, 3-methoxy-
- CBNumber
- CB0460150
- Molecular Formula
- C7H7NO2
- Formula Weight
- 137.14
- MOL File
- 1849-52-1.mol
3-METHOXYISONICOTINALDEHYDE Property
- Melting point:
- 36-37 °C
- Boiling point:
- 80 °C(Press: 1 Torr)
- Density
- 1.159±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- pka
- 2.86±0.10(Predicted)
- Appearance
- Yellow to brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M263440
- Product name
- 3-Methoxyisonicotinaldehyde
- Packaging
- 250mg
- Price
- $620
- Updated
- 2021/12/16
- Product number
- CHM0165989
- Product name
- 3-METHOXYISONICOTINALDEHYDE
- Purity
- 98.00%
- Packaging
- 0.5G
- Price
- $726
- Updated
- 2021/12/16
- Product number
- 119591
- Product name
- 3-Methoxyisonicotinaldehyde
- Purity
- 95+%
- Packaging
- 1g
- Price
- $810
- Updated
- 2021/12/16
- Product number
- 9666AA
- Product name
- 3-Methoxyisonicotinaldehyde
- Packaging
- 1g
- Price
- $477
- Updated
- 2021/12/16
- Product number
- CM127873
- Product name
- 3-methoxyisonicotinaldehyde
- Purity
- 97%
- Packaging
- 5g
- Price
- $1010
- Updated
- 2021/12/16
3-METHOXYISONICOTINALDEHYDE Chemical Properties,Usage,Production
Synthesis
102074-60-2
1849-52-1
General procedure for the synthesis of 3-methoxypyridin-4-aldehyde from (3-methoxypyridin-4-yl)methanol: Manganese dioxide (843 mg) was added to a solution of ethyl acetate (10 mL) in (3-methoxypyridin-4-yl)methanol (270 mg), and the reaction was carried out at reflux for 2 hours. Subsequently, manganese dioxide (167 mg) was added to the reaction system and refluxing was continued for 1 hour. After completion of the reaction, the mixture was cooled to room temperature and filtered to remove insoluble material. The filtrate was distilled under reduced pressure to remove the solvent, and the resulting residue was purified by silica gel column chromatography (eluent ratio: hexane/ethyl acetate = 1:1 → 0:1) to give 3-methoxypyridine-4-aldehyde (190 mg) as a white solid.
References
[1] Patent: WO2007/67511, 2007, A2. Location in patent: Page/Page column 35
[2] Patent: US2016/168139, 2016, A1. Location in patent: Paragraph 0944; 0949; 0950
3-METHOXYISONICOTINALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-METHOXYISONICOTINALDEHYDE Suppliers
- Tel
- +49 5662 408730
- Fax
- +49 5662 4087320
- info@synchem.de
- Country
- Germany
- ProdList
- 4705
- Advantage
- 70
View Lastest Price from 3-METHOXYISONICOTINALDEHYDE manufacturers
- Product
- 3-METHOXYISONICOTINALDEHYDE 1849-52-1
- Price
- US $1.00/KG
- Min. Order
- 1g
- Purity
- 98%
- Supply Ability
- 200kgs
- Release date
- 2020-01-09