3-HYDROXY-2-PHENYLPYRIDINE

Product Name: 3-HYDROXY-2-PHENYLPYRIDINE
CAS No.: 3308-02-9
Chemical Name: 3-HYDROXY-2-PHENYLPYRIDINE
Synonyms: 2-phenyl-3-pyridino;2-PHENYL-3-PYRIDINOL;2-PHENYL-PYRIDIN-3-OL;3-Pyridinol, 2-phenyl-;2-Phenyl-3-hydroxypyridine;3-HYDROXY-2-PHENYLPYRIDINE;1,4-Benzenediamine,2,7-dibromo-;3-HYDROXY-2-PHENYLPYRIDINE ISO 9001：2015 REACH;4-N-(2-bromophenyl)pyrido[4,3-d]pyrimidine-4,7-diamine
CBNumber: CB0460640
Molecular Formula: C11H9NO
Formula Weight: 171.2
MOL File: 3308-02-9.mol

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3-HYDROXY-2-PHENYLPYRIDINE Property

Melting point:: 205 °C
Boiling point:: 320 °C
Density: 1.169±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 8.23±0.10(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 119551
Product name: 2-Phenylpyridin-3-ol
Purity: 95+%
Packaging: 250mg
Price: $468
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0101133
Product name: 3-HYDROXY-2-PHENYLPYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $503.49
Updated: 2021/12/16

AK Scientific

Product number: 3776AB
Product name: 2-Phenylpyridin-3-ol
Packaging: 250mg
Price: $313
Updated: 2021/12/16

Matrix Scientific

Product number: 119551
Product name: 2-Phenylpyridin-3-ol
Purity: 95+%
Packaging: 1g
Price: $1170
Updated: 2021/12/16

J&W Pharmlab

Product number: 69R0248
Product name: 2-Phenyl-pyridin-3-ol
Purity: 98%
Packaging: 5g
Price: $1480
Updated: 2021/12/16

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3-HYDROXY-2-PHENYLPYRIDINE Chemical Properties,Usage,Production

Synthesis Reference(s)

Tetrahedron, 48, p. 8117, 1992 DOI: 10.1016/S0040-4020(01)80481-6

Synthesis

40263-57-8

98-80-6

3308-02-9

To a stirred solution of 2-iodo-3-hydroxypyridine (5.0 g, 22.624 mmol) in benzene (50 ml) was added phenylboronic acid (3.03 g, 24.85 mmol) and 2M Na2CO3 solution (20 mL) sequentially at 25 °C. The reaction system was protected and degassed with argon for 15 min. Tetrakis(triphenylphosphine)palladium (Pd(PPh3)4, 1.3 g, 5 mol%) was then added and degassing continued for 10 minutes. The reaction mixture was heated to reflux for 4 hours. After completion of the reaction, it was cooled to room temperature, water was added and extracted with ethyl acetate (EtOAc). The organic layers were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by solvent milling with methyl tert-butyl ether (MTBE)/dichloromethane (DCM) mixture to give 3-hydroxy-2-phenylpyridine (3.2 g).LCMS detection showed a molecular ion peak of 172 (M + H).

References

[1] Patent: WO2014/186035, 2014, A1. Location in patent: Page/Page column 175; 178; 179

3-HYDROXY-2-PHENYLPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-HYDROXY-2-PHENYLPYRIDINE Suppliers

China 46 Germany 2 India 1 United Kingdom 5 United States 10 Global 64

NovoChemy Ltd.

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Synchem OHG

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Xi'an NewProChem Co.,Ltd.

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JW & Y Pharmlab Co., Ltd.

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Shanghai Carlow Chemicals Co., Ltd.

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Shanghai YuanYe Biotechnology Co., Ltd.

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View Lastest Price from 3-HYDROXY-2-PHENYLPYRIDINE manufacturers

Dideu Industries Group Limited

Product: 3-HYDROXY-2-PHENYLPYRIDINE 3308-02-9
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-09-26

3308-02-9, 3-HYDROXY-2-PHENYLPYRIDINERelated Search:

oxycinchophen 3-HYDROXY-2-PHENYLPYRIDINE Inabenfide 2-HYDROXY-6-PHENYLPYRIDINE-4-CARBOXYLIC ACID 2-HYDROXY-6-PHENYLPYRIDINE 2-Phenylpyridine 2-HYDROXY-4-PHENYLPYRIDINE 2-Amino-3,5-dicyano-6-hydroxy-4-phenylpyridine 3-HYDROXY-5-PHENYLPYRIDINE 3-Cyano-2-hydroxy-6-phenylpyridine 2-HYDROXY-3-PHENYLPYRIDINE 3-HYDROXY-6-PHENYLPYRIDINE 2-Hydroxy-5-phenylpyridine 3,5-Dicyano-2-hydroxy-6-phenylpyridine 3-HYDROXY-4-PHENYLPYRIDINE 4-HYDROXY-6-PHENYLPYRIDINE-2-CARBOXYLIC ACID 4-HYDROXY-2-PHENYLPYRIDINE METHYL 3-CYANO-2-HYDROXY-6-PHENYLPYRIDINE-4-CARBOXYLATE

2-phenyl-3-pyridino

2-Phenyl-3-hydroxypyridine

3-Pyridinol, 2-phenyl-

4-N-(2-bromophenyl)pyrido[4,3-d]pyrimidine-4,7-diamine

3-HYDROXY-2-PHENYLPYRIDINE

2-PHENYL-3-PYRIDINOL

2-PHENYL-PYRIDIN-3-OL

3-HYDROXY-2-PHENYLPYRIDINE ISO 9001：2015 REACH

1,4-Benzenediamine,2,7-dibromo-

3308-02-9

3308-2-9

3308/2/9

Pyridines, Pyrimidines, Purines and Pteredines

pharmacetical