ChemicalBook > CAS DataBase List > 3-HYDROXY-2-PHENYLPYRIDINE
3-HYDROXY-2-PHENYLPYRIDINE
- Product Name
- 3-HYDROXY-2-PHENYLPYRIDINE
- CAS No.
- 3308-02-9
- Chemical Name
- 3-HYDROXY-2-PHENYLPYRIDINE
- Synonyms
- 2-phenyl-3-pyridino;2-PHENYL-3-PYRIDINOL;2-PHENYL-PYRIDIN-3-OL;3-Pyridinol, 2-phenyl-;2-Phenyl-3-hydroxypyridine;3-HYDROXY-2-PHENYLPYRIDINE;1,4-Benzenediamine,2,7-dibromo-;3-HYDROXY-2-PHENYLPYRIDINE ISO 9001：2015 REACH;4-N-(2-bromophenyl)pyrido[4,3-d]pyrimidine-4,7-diamine
- CBNumber
- CB0460640
- Molecular Formula
- C11H9NO
- Formula Weight
- 171.2
- MOL File
- 3308-02-9.mol
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3-HYDROXY-2-PHENYLPYRIDINE Property
- Melting point:
- 205 °C
- Boiling point:
- 320 °C
- Density
- 1.169±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 8.23±0.10(Predicted)
- Appearance
- Light yellow to yellow Solid
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
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N-Bromosuccinimide Price
Matrix Scientific
- Product number
- 119551
- Product name
- 2-Phenylpyridin-3-ol
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $468
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- CHM0101133
- Product name
- 3-HYDROXY-2-PHENYLPYRIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $503.49
- Updated
- 2021/12/16
AK Scientific
- Product number
- 3776AB
- Product name
- 2-Phenylpyridin-3-ol
- Packaging
- 250mg
- Price
- $313
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 119551
- Product name
- 2-Phenylpyridin-3-ol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $1170
- Updated
- 2021/12/16
J&W Pharmlab
- Product number
- 69R0248
- Product name
- 2-Phenyl-pyridin-3-ol
- Purity
- 98%
- Packaging
- 5g
- Price
- $1480
- Updated
- 2021/12/16
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3-HYDROXY-2-PHENYLPYRIDINE Chemical Properties,Usage,Production
Synthesis Reference(s)
Tetrahedron, 48, p. 8117, 1992 DOI: 10.1016/S0040-4020(01)80481-6
Synthesis
40263-57-8
98-80-6
3308-02-9
To a stirred solution of 2-iodo-3-hydroxypyridine (5.0 g, 22.624 mmol) in benzene (50 ml) was added phenylboronic acid (3.03 g, 24.85 mmol) and 2M Na2CO3 solution (20 mL) sequentially at 25 °C. The reaction system was protected and degassed with argon for 15 min. Tetrakis(triphenylphosphine)palladium (Pd(PPh3)4, 1.3 g, 5 mol%) was then added and degassing continued for 10 minutes. The reaction mixture was heated to reflux for 4 hours. After completion of the reaction, it was cooled to room temperature, water was added and extracted with ethyl acetate (EtOAc). The organic layers were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by solvent milling with methyl tert-butyl ether (MTBE)/dichloromethane (DCM) mixture to give 3-hydroxy-2-phenylpyridine (3.2 g).LCMS detection showed a molecular ion peak of 172 (M + H).
References
[1] Patent: WO2014/186035, 2014, A1. Location in patent: Page/Page column 175; 178; 179
3-HYDROXY-2-PHENYLPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-HYDROXY-2-PHENYLPYRIDINE manufacturers
Dideu Industries Group Limited
- Product
- 3-HYDROXY-2-PHENYLPYRIDINE 3308-02-9
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-09-26
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