7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one

ChemicalBook > CAS DataBase List > 7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one

7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one

Product Name: 7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one
CAS No.: 5307-99-3
Chemical Name: 7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one
Synonyms: NSC 116987;Dichlorobicycloheptenone;Prostaglandin Impurity 4;7,7-Dichloro[3.2.0]hept-2-en-6-one;7,7-DICHLOROBICYCLO[3.2.0]HEPT-2-ENONE;7,7-DICHLOROBICYCLO[3.2.0]HEPT-2-EN-6-ONE;6,6-dichlorobicyclo[3.2.0]hept-3-en-7-one;7,7-DICHLOROBICYCLO[3.2.0]HEPT-2-ENE-6-ONE;7,7-Dichloro-6-oxobicyclo[3.2.0]hept-2-ene;Bicyclo[3.2.0]hept-2-en-6-one, 7,7-dichloro-
CBNumber: CB0472056
Molecular Formula: C7H6Cl2O
Formula Weight: 177.03
MOL File: 5307-99-3.mol

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7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one Property

Boiling point:: 58-64 °C (0.5 mmHg)
Density: 1.44±0.1 g/cm3(Predicted)
refractive index: 1.5150
Flash point:: 127-128°C/25mm
storage temp.: Refrigerator (+4°C)
form: liquid
color: Clear, dark orange
BRN: 2045059
CAS DataBase Reference: 5307-99-3(CAS DataBase Reference)

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Safety

Hazard Codes: Xi,C
Risk Statements: 36/37/38-34-22
Safety Statements: 26-36/37/39-45
RIDADR: UN 3265 8 / PGIII
WGK Germany: 2
Hazard Note: Irritant
HS Code: 2914290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H314Causes severe skin burns and eye damage

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Alfa Aesar

Product number: A17915
Product name: 7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one, 97%
Packaging: 5g
Price: $47.9
Updated: 2021/12/16

Alfa Aesar

Product number: A17915
Product name: 7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one, 97%
Packaging: 25g
Price: $196
Updated: 2021/12/16

TRC

Product number: D435898
Product name: 7,7-Dichlorobicyclo[3.2.0]Hept-2-En-6-One
Packaging: 500mg
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD145060
Product name: 7,7-Dichloro[3.2.0]hept-2-en-6-one
Packaging: 2g
Price: $120
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD145060
Product name: 7,7-Dichloro[3.2.0]hept-2-en-6-one
Packaging: 1g
Price: $75
Updated: 2021/12/16

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7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one Chemical Properties,Usage,Production

Chemical Properties

clear brown liquid

Synthesis

Under nitrogen protection, to a solution of dichloracetyl chloride (34 g, 0.23 mol) and cyclopentadiene(60 ml, 0.7 mol) in pentane (230 ml), heated to reflux in a three-necked flask with constant pressure funnel and condenser tube, was added dropwise via funnel triethylamine (24 g, 0.24 mol) in pentane (100 ml) with mechanical stirring during 4 hours, and a lot of white triethylamine hydrochloride was produced. After reflux for 2 hours, water (80 ml) was added to dissolve the triethylamine hydrochloride. The reaction mixture was extracted with pentane (2 × 60ml). The combined extracts were filtered and dried over anhydrous Na2SO4, and concentrated in vacuo to give brownish black oil. Fraction of reduced pressure distillation at 83~87 °C/400 Pa was collected to give 7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one (2, 33.5 g) as a colorless oil.

7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one Preparation Products And Raw materials

Raw materials

Preparation Products

HEPTENOPHOS

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View Lastest Price from 7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-one manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 7,7-DICHLOROBICYCLO[3.2.0]HEPT-2-EN-6-ONE 5307-99-3
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

5307-99-3, 7,7-Dichlorobicyclo[3.2.0]hept-2-en-6-oneRelated Search:

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5307-99-3