1,9-DICHLORONONANE
- Product Name
- 1,9-DICHLORONONANE
- CAS No.
- 821-99-8
- Chemical Name
- 1,9-DICHLORONONANE
- Synonyms
- 1,9-Dichlornonan;1,9-Dichlornonane;1,9-dichloro-nonan;1,9-DICHLORONONANE;N-DECYLDIMETHYLAMINE;Nonane,1,9-dichloro-;Nonane, 1,9-dichloro-;1,9-Dichlorononane,99%;NONAMETHYLENE DICHLORIDE;1,9-Dichlorononane, 98%+
- CBNumber
- CB0485171
- Molecular Formula
- C9H18Cl2
- Formula Weight
- 197.15
- MOL File
- 821-99-8.mol
1,9-DICHLORONONANE Property
- Boiling point:
- 258-262 °C(lit.)
- Density
- 1.091 g/mL at 25 °C(lit.)
- refractive index
- n20/D 1.4599(lit.)
- Flash point:
- >230 °F
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Acetone (Slightly), Chloroform (Soluble), DMSO (Slightly), DMSO (Slightly)
- form
- Liquid
- color
- Colorless
- Water Solubility
- Insoluble in water.
- InChI
- InChI=1S/C9H18Cl2/c10-8-6-4-2-1-3-5-7-9-11/h1-9H2
- InChIKey
- JMGRNJZUQCEJDB-UHFFFAOYSA-N
- SMILES
- C(Cl)CCCCCCCCCl
- CAS DataBase Reference
- 821-99-8
- EPA Substance Registry System
- Nonane, 1,9-dichloro- (821-99-8)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- D5116
- Product name
- 1,9-Dichlorononane
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $39
- Updated
- 2025/07/31
- Product number
- D5116
- Product name
- 1,9-Dichlorononane
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $109
- Updated
- 2025/07/31
- Product number
- D434625
- Product name
- 1,9-Dichlorononane
- Packaging
- 250mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 091145
- Product name
- 1,9-Dichlorononane
- Purity
- 95+%
- Packaging
- 10g
- Price
- $49
- Updated
- 2021/12/16
- Product number
- FD139715
- Product name
- 1,9-Dichlorononane
- Packaging
- 5G
- Price
- $63
- Updated
- 2021/12/16
1,9-DICHLORONONANE Chemical Properties,Usage,Production
Chemical Properties
CLEAR YELLOW LIQUID
Uses
It is used as pharmaceutical intermediate. Many organisms use 1,9-dichlorononane as a sole carbon source. Bacteria on incubation of sewage with 1,9-dichlorononane increased its subsequent capacity to dehalogenate.
Synthesis
3937-56-2
821-99-8
General procedure for the synthesis of 1,9-dichlorononane from 1,9-nonanediol: 1,9-nonanediol (5.0 g, 31.2 mmol), dichloromethane (100 mL), and DMF (3 drops) were added to a 500 mL eggplant-shaped vial. Thionyl chloride (11.7 g, 98.3 mmol) was dissolved in dichloromethane (155 mL). The thionyl chloride solution was slowly added dropwise to a cigar shaped flask under ice bath conditions. The reaction mixture was stirred overnight at room temperature. Upon completion of the reaction, the reaction mixture was washed with saturated sodium bicarbonate solution followed by saturated sodium chloride solution. The organic phase was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 1,9-dichlorononane (4.0 g, light yellow oil, 65% yield).
References
[1] Journal of Organic Chemistry USSR (English Translation), 1989, vol. 25, # 4.1, p. 642 - 646
[2] Zhurnal Organicheskoi Khimii, 1989, vol. 25, # 4, p. 716 - 721
[3] Patent: CN107721925, 2018, A. Location in patent: Paragraph 0096; 0097
[4] Journal of the American Chemical Society, 1948, vol. 70, p. 3393
[5] Pharmaceutical Chemistry Journal, 1972, vol. 6, # 5, p. 283 - 286
1,9-DICHLORONONANE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1,9-DICHLORONONANE manufacturers
- Product
- 1,9-DICHLORONONANE 821-99-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-09