Tetrahydrofurfuryl bromide

Product Name: Tetrahydrofurfuryl bromide
CAS No.: 1192-30-9
Chemical Name: Tetrahydrofurfuryl bromide
Synonyms: TIMTEC-BB SBB003909;2-(Bromomethyl)oxolane;TETRAHYDROFRUFRYL BROMIDE;α-(Bromomethyl)tetrafuran;TETRAHYDROFURFURYL BROMIDE;2-(bromomethyl)tetrahydro-fura;2-(BROMOMETHYL)TETRAHYDROFURAN;tetrahydro-2-(bromomethyl)-fura;(RS)-Tetrahydrofurfuryl bromide;A-(BROMOMETHYL)TETRA HYDROFURAN
CBNumber: CB0486057
Molecular Formula: C5H9BrO
Formula Weight: 165.03
MOL File: 1192-30-9.mol

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Tetrahydrofurfuryl bromide Property

Boiling point:: 170-171 °C (755 mmHg)
Density: 1.45
refractive index: 1.4853-1.4873
Flash point:: 63 °C
storage temp.: Refrigerator
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Oil
color: Clear Light Yellow
BRN: 102717
InChI: InChI=1S/C5H9BrO/c6-4-5-2-1-3-7-5/h5H,1-4H2
InChIKey: VOHILFSOWRNVJJ-UHFFFAOYSA-N
SMILES: O1CCCC1CBr
CAS DataBase Reference: 1192-30-9(CAS DataBase Reference)
EPA Substance Registry System: Furan, 2-(bromomethyl)tetrahydro- (1192-30-9)

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 36/37/38-22
Safety Statements: 24/25
RIDADR: 1993
RTECS: LU6000000
TSCA: Yes
HS Code: 29321900
Toxicity: mouse,LD50,intravenous,180mg/kg (180mg/kg),U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#03416,

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: CDS001200
Product name: Tetrahydrofurfuryl bromide
Purity: AldrichCPR
Packaging: 1G
Price: $73.1
Updated: 2025/07/31

TCI Chemical

Product number: T1808
Product name: Tetrahydrofurfuryl Bromide
Purity: >95.0%(GC)
Packaging: 25g
Price: $72
Updated: 2025/07/31

TCI Chemical

Product number: T1808
Product name: Tetrahydrofurfuryl Bromide
Purity: >95.0%(GC)
Packaging: 100g
Price: $131
Updated: 2025/07/31

TCI Chemical

Product number: T1808
Product name: Tetrahydrofurfuryl Bromide
Purity: >95.0%(GC)
Packaging: 500g
Price: $315
Updated: 2025/07/31

TRC

Product number: T293570
Product name: (±)-TetrahydrofurfurylBromide
Packaging: 25g
Price: $70
Updated: 2021/12/16

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Tetrahydrofurfuryl bromide Chemical Properties,Usage,Production

Chemical Properties

Colorless to light yellow liqui

Uses

(±)-Tetrahydrofurfuryl Bromide is a general chemical reagent used in the synthesis of tubulin polymerization inhibitors.

Synthesis

In a 500-ml three-necked flask equipped with a stirrer, thermometer, dropping funnel, and calcium chloride tube, place 96 g of redistilled PBr₃ and 50 ml of dry benzene. Add 15 g of dry pyridine dropwise with stirring over 15 minutes.
Cool the flask in an ice-salt bath to -5°C. Then, slowly add a mixture of 102 g of tetrahydrofurfuryl alcohol and 5 g of dry pyridine over 4 hours, maintaining the internal temperature between -5° and -3°C. Stir for an additional hour and allow the mixture to warm to room temperature.
Let the mixture stand for 24-48 hours. Transfer it to a Claisen flask, rinse with a little benzene, and remove the benzene by distillation under reduced pressure (bath temperature ≤90°C). Finally, distill the product under high vacuum (5-10 mm Hg) with the bath temperature up to 150-155°C.
The crude product is redistilled to give pure tetrahydrofurfuryl bromide, boiling at 69-70°C/22 mm Hg. The yield is 90-102 g (53-61%)^[1].

References

[1] Org. Synth. 1943, 23, 88. DOI: 10.15227/orgsyn.023.0088.

Tetrahydrofurfuryl bromide Preparation Products And Raw materials

Raw materials

Tetrahydrofurfuryl alcohol

Preparation Products

TETRAHYDROFURFURYL SODIUM THIOSULFATE alpha-(1-Naphthylmethyl)-2-tetrahydrofuranpropionic acid diethylaminoethyl ester oxalate Ethyl 1-methyl-1H-pyrazole-5-carboxylate (TETRAHYDRO-FURAN-2-YLMETHYL)-HYDRAZINE

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Tetrahydrofurfuryl bromide Suppliers

Belgium 3 China 131 Germany 4 India 6 Japan 4 South Korea 1 Sweden 2 Switzerland 1 Ukraine 1 United Kingdom 16 United States 28 Global 197

Shanghai Kangsente Pharmaceutical Co. LTD

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Energy Chemical

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View Lastest Price from Tetrahydrofurfuryl bromide manufacturers

Shandong Vital Biotechnology Co., Ltd.

Product: Tetrahydrofurfuryl bromide 1192-30-9
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 100tons
Release date: 2025-11-19

Zhuozhou Wenxi import and Export Co., Ltd

Product: Tetrahydrofurfuryl bromide 1192-30-9
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: Tetrahydrofurfuryl bromide 1192-30-9
Price: US $8.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 100kg
Release date: 2019-08-05

1192-30-9, Tetrahydrofurfuryl bromideRelated Search:

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Tetrahydrofurfuryl Bromide=2-(Bromomethyl)tetrahydrofuran

2-(bromomethyl)tetrahydro-fura

tetrahydro-2-(bromomethyl)-fura

TETRAHYDROFRUFRYL BROMIDE

Tetrahydrofurfuryl bromide, pract., 95%

Tetrahydrofurfuryl bromide, tech., 90%

tetrahydro-2-(bromomethyl)-furan

A-(BROMOMETHYL)TETRA HYDROFURAN

(RS)-Tetrahydrofurfuryl bromide

2-(Bromomethyl)oxolane

Tetrahydrofurfuryl bromide, 90%, tech.

TETRAHYDROFURFURYL BROMIDE

TIMTEC-BB SBB003909

2-(BROMOMETHYL)TETRAHYDROFURAN

α-(Bromomethyl)tetrafuran

Tetrahydrofurfuryl broMide, tech., 90% 50GR

Furan,2-(broMoMethyl)tetrahydro-

2-(bromomethyl)oxolane - [B17294]

1192-30-9

C5H9BrO

Furans, Benzofurans & Dihydrobenzofurans

Methyl Halides

Furans

Aromatic Hydrocarbons (substituted) & Derivatives

Furans, Benzofurans & Dihydrobenzofurans

Methyl Halides

Furan&Benzofuran