ChemicalBook > CAS DataBase List > 3-(3-BROMO-PHENYL)-PROPAN-1-OL

3-(3-BROMO-PHENYL)-PROPAN-1-OL

Product Name
3-(3-BROMO-PHENYL)-PROPAN-1-OL
CAS No.
65537-54-4
Chemical Name
3-(3-BROMO-PHENYL)-PROPAN-1-OL
Synonyms
BENZENEPROPANOL, 3-BROMO-;3-(3-Bromophenyl)-1-propanol;3-(3-BROMO-PHENYL)-PROPAN-1-OL
CBNumber
CB0807096
Molecular Formula
C9H11BrO
Formula Weight
215.09
MOL File
65537-54-4.mol
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3-(3-BROMO-PHENYL)-PROPAN-1-OL Property

Boiling point:
299.9±15.0 °C(Predicted)
Density 
1.410±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
15.05±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
B698533
Product name
3-(3-Bromophenyl)propan-1-ol
Packaging
500mg
Price
$265
Updated
2021/12/16
ChemScene
Product number
CS-B0313
Product name
3-(3-bromophenyl)propan-1-ol
Packaging
250mg
Price
$53
Updated
2021/12/16
ChemScene
Product number
CS-B0313
Product name
3-(3-bromophenyl)propan-1-ol
Packaging
1g
Price
$190
Updated
2021/12/16
AK Scientific
Product number
V7142
Product name
3-(3-Bromophenyl)propan-1-ol
Packaging
1g
Price
$291
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0351843
Product name
3-(3-BROMOPHENYL)PROPAN-1-OL
Purity
95.00%
Packaging
5MG
Price
$499.66
Updated
2021/12/16
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3-(3-BROMO-PHENYL)-PROPAN-1-OL Chemical Properties,Usage,Production

Synthesis

42287-90-1

65537-54-4

A THF solution (50 mL) of 3-(3-bromophenyl)propionic acid (5 g, 21.83 mmol, 1.00 eq.) was added to a 250 mL three-necked round-bottomed flask under nitrogen protection. The reaction system was cooled to 0 °C and the borane tetrahydrofuran complex solution (1 mol/L, 75 mL, 74.22 mmol, 3.40 eq.) was slowly added dropwise with stirring. After the dropwise addition, the reaction mixture was gradually warmed to room temperature and stirred overnight. After completion of the reaction, the mixture was slowly poured into 150 mL of 1 mol/L HCl solution and extracted with dichloromethane (3 x 200 mL). The organic phases were combined, washed with 300 mL of saturated saline, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography with dichloromethane/methanol (10:1, v/v) as eluent. The target fraction was collected and concentrated under reduced pressure to afford 3-(3-bromophenyl)propan-1-ol (1.3 g, 28% yield) as a colorless oil.1H NMR (DMSO-d6, 400 MHz) δ: 7.41-7.20 (m, 4H), 4.51-4.48 (t, 1H), 3.41-3.34 (m, 2H), 2.67-2.59 (m, 2H), 1.73-1.73 (m, 2H). 2H), 1.73-1.66 (m, 2H).

References

[1] Patent: US2004/10019, 2004, A1. Location in patent: Page 160; 167
[2] Patent: WO2006/101977, 2006, A2. Location in patent: Page/Page column 56
[3] Journal of Organic Chemistry, 2010, vol. 75, # 15, p. 5178 - 5194
[4] Angewandte Chemie - International Edition, 2018, vol. 57, # 15, p. 4058 - 4062
[5] Angew. Chem., 2018, vol. 130, p. 4122 - 4126,5

3-(3-BROMO-PHENYL)-PROPAN-1-OL Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(3-BROMO-PHENYL)-PROPAN-1-OL Suppliers

China 36 Germany 1 India 2 United States 3 Global 42
United States Biological
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Fax
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Email
sales@advtechind.com
Country
United States
ProdList
6075
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Synthonix Inc
Tel
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Fax
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Email
info@synthonix.com
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United States
ProdList
6872
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Combi-Blocks Inc.
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Email
sales@combi-blocks.com
Country
United States
ProdList
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View Lastest Price from 3-(3-BROMO-PHENYL)-PROPAN-1-OL manufacturers

Career Henan Chemical Co
Product
3-(3-BROMO-PHENYL)-PROPAN-1-OL 65537-54-4
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
200kg
Release date
2018-12-25

65537-54-4, 3-(3-BROMO-PHENYL)-PROPAN-1-OLRelated Search:

6-Bromo-2,3-dihydro-4H-chromen-4-one 3,5-Dibromo-L-tyrosine CHEMBRDG-BB 5469887 BOC-3,5-DIBROMO-TYR(OBZL)-OH HA14-1 FMOC-3,5-DIBROMO-TYR-OH BOC-TYR(3,5-BR2)-OH 4-(3-BROMO-PHENYL)-6-METHYL-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER AURORA 1147 N-[6-BROMO-3-(HYDROXYMETHYL)-3,4-DIHYDRO-2H-CHROMEN-4-YL]-N'-(2,4-DICHLOROPHENYL)-N-METHYLUREA SALOR-INT L476528-1EA (6-BROMO-3-OXO-1,3-DIHYDRO-ISOBENZOFURAN-1-YL)-ACETIC ACID 3-(3-BROMO-4-METHOXYPHENYL)PROPANOIC ACID N-[6-BROMO-3-(HYDROXYMETHYL)-3,4-DIHYDRO-2H-CHROMEN-4-YL]-N-METHYL-N'-(4-NITROPHENYL)THIOUREA DL-3,5-DIBROMOTHYRONINE 8-BROMO-1-METHYL-1,3A,4,9B-TETRAHYDRO-3H-CHROMENO[4,3-C]ISOXAZOLE (6-BROMO-3-OXO-2,3-DIHYDRO-1 H-ISOINDOL-1-YL)-ACETIC ACID ETHYL 6-(BROMOMETHYL)-4-(3-BROMOPHENYL)-2-OXO-1,2,3,4-TETRAHYDROPYRIMIDINE-5-CARBOXYLATE

  • 3-(3-Bromophenyl)-1-propanol
  • 3-(3-BROMO-PHENYL)-PROPAN-1-OL
  • BENZENEPROPANOL, 3-BROMO-
  • 65537-54-4