2,7-Dichlorobenzothiazole
- Product Name
- 2,7-Dichlorobenzothiazole
- CAS No.
- 2942-23-6
- Chemical Name
- 2,7-Dichlorobenzothiazole
- Synonyms
- 2,7-Dichlor-benzthiazol;2,7-DICHLORO BENZOTHIAZOLE;2,7-Dichlorobenzo[d]thiazole;Benzothiazole, 2,7-dichloro-;2,7-Dichloro-1,3-benzothiazole;Benzothiazole, 2,7-dichloro- (7CI,8CI,9CI)
- CBNumber
- CB0836593
- Molecular Formula
- C7H3Cl2NS
- Formula Weight
- 204.08
- MOL File
- 2942-23-6.mol
2,7-Dichlorobenzothiazole Property
- Boiling point:
- 286.8±13.0 °C(Predicted)
- Density
- 1.567±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -1.49±0.30(Predicted)
- Appearance
- White to off-white Solid
Safety
- HS Code
- 29342000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D439845
- Product name
- 2,7-Dichlorobenzo[d]thiazole
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- FD151896
- Product name
- 2,7-Dichlorobenzothiazole
- Packaging
- 100mg
- Price
- $103
- Updated
- 2021/12/16
- Product number
- FD151896
- Product name
- 2,7-Dichlorobenzothiazole
- Packaging
- 250mg
- Price
- $205
- Updated
- 2021/12/16
- Product number
- FD151896
- Product name
- 2,7-Dichlorobenzothiazole
- Packaging
- 500mg
- Price
- $360
- Updated
- 2021/12/16
- Product number
- 119731
- Product name
- 2,7-Dichlorobenzo[d]thiazole
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $418
- Updated
- 2021/12/16
2,7-Dichlorobenzothiazole Chemical Properties,Usage,Production
Synthesis
1849-73-6
2942-23-6
General procedure for the synthesis of 2,7-dichlorobenzo[d]thiazole from 7-chlorobenzo[d]thiazole-2(3H)-thione: General method: a mixture of 7-chlorobenzo[d]thiazole-2(3H)-thione (>1 g, 1 eq.) and sulfuryl chloride (10 eq.) was stirred at 20-25 °C for 15 min. Subsequently, water (2 eq.) was added and stirring was continued for 3 hours at 20-25 °C. During the reaction, the sample was removed, quenched with acetonitrile/water (2:1) and analyzed by high performance liquid chromatography (HPLC). Upon completion of the reaction, the mixture was diluted with acetonitrile (5 v/v) and the reaction was quenched by slowly adding water (20 v/v). The product precipitated from the aqueous solution and the solid was collected and washed with distilled water. Finally, the solid was dried under vacuum to give pure 2,7-dichlorobenzo[d]thiazole. For the liquid product 2-chlorobenzo[d]thiazole (13), the reaction mixture was extracted with ethyl acetate and the organic layer was dried and concentrated to give an oily product.
References
[1] Synthesis (Germany), 2018, vol. 50, # 10, p. 2027 - 2032
[2] Journal of Heterocyclic Chemistry, 2005, vol. 42, # 4, p. 727 - 730
[3] Gazzetta Chimica Italiana, 1965, vol. 95, p. 490 - 498
2,7-Dichlorobenzothiazole Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,7-Dichlorobenzothiazole manufacturers
- Product
- 2,7-Dichlorobenzo[d]thiazole 2942-23-6
- Price
- US $3.00-9.00/KG
- Min. Order
- 0.1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2025-06-27
- Product
- 2,7-Dichlor-benzthiazol 2942-23-6
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 100 tons
- Release date
- 2022-01-14