2-Pyrimidinamine, N-methyl- (9CI)

Product Name: 2-Pyrimidinamine, N-methyl- (9CI)
CAS No.: 931-61-3
Chemical Name: 2-Pyrimidinamine, N-methyl- (9CI)
Synonyms: NSC 102272;N-Methyl-2-pyrimidinamine;2-PyriMidinaMine, N-Methyl-;methyl(pyrimidin-2-yl)amine;2-Pyrimidinamine, N-methyl- (9CI);2-Pyrimidinamine, N-methyl- (9CI) ISO 9001：2015 REACH
CBNumber: CB11081371
Molecular Formula: C5H7N3
Formula Weight: 109.13
MOL File: 931-61-3.mol

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2-Pyrimidinamine, N-methyl- (9CI) Property

Melting point:: 60-62℃
Boiling point:: 216℃
Density: 1.144
Flash point:: 85℃
storage temp.: 2-8°C(protect from light)
form: Solid
pka: 3.90±0.10(Predicted)
Appearance: White to yellow Solid
InChI: InChI=1S/C5H7N3/c1-6-5-7-3-2-4-8-5/h2-4H,1H3,(H,6,7,8)
InChIKey: BQNXHDSGGRTFNX-UHFFFAOYSA-N
SMILES: C1(NC)=NC=CC=N1

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: M103138
Product name: N-methylpyrimidin-2-amine
Packaging: 5mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M103138
Product name: N-methylpyrimidin-2-amine
Packaging: 10mg
Price: $60
Updated: 2021/12/16

ChemScene

Product number: CS-0061723
Product name: N-Methylpyrimidin-2-amine
Packaging: 250mg
Price: $71
Updated: 2021/12/16

AK Scientific

Product number: J55249
Product name: 2-(Methylamino)pyrimidine
Packaging: 100mg
Price: $77
Updated: 2021/12/16

ChemScene

Product number: CS-0061723
Product name: N-Methylpyrimidin-2-amine
Packaging: 1g
Price: $142
Updated: 2021/12/16

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2-Pyrimidinamine, N-methyl- (9CI) Chemical Properties,Usage,Production

Synthesis

1722-12-9

74-89-5

931-61-3

Step 1: Synthesis of N-methylpyrimidin-2-amine To a solution of 2-chloropyrimidine (1 g, 8.7 mmol) in methanol (10 mL) was slowly added a methanolic solution of 2Methylamine (13.2 mL, 26.2 mmol) followed by potassium carbonate (2.5 g, 18 mmol). The reaction flask was sealed and the reaction was stirred at 80 °C overnight. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated by rotary evaporator to remove volatile solvents. The residue was extracted by liquid-liquid partition with distilled water and dichloromethane. The organic layer was separated, dried over anhydrous sodium sulfate, filtered and concentrated to give 2-methylaminopyrimidine (290 mg, 30% yield) as a brown oil.

References

[1] Bulletin of the Chemical Society of Japan, 1998, vol. 71, # 8, p. 1973 - 1991
[2] Journal of Medicinal Chemistry, 2013, vol. 56, # 17, p. 6626 - 6637
[3] Molecules, 2004, vol. 9, # 7, p. 520 - 526
[4] Patent: WO2011/71716, 2011, A1. Location in patent: Page/Page column 99
[5] Journal of the American Chemical Society, 1954, vol. 76, p. 1065,1067

2-Pyrimidinamine, N-methyl- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Pyrimidinamine, N-methyl- (9CI) Suppliers

China 62 Europe 1 India 1 United States 4 Global 68

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View Lastest Price from 2-Pyrimidinamine, N-methyl- (9CI) manufacturers

Dideu Industries Group Limited

Product: 2-Pyrimidinamine, N-methyl- (9CI) 931-61-3
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-12-13

Career Henan Chemical Co

Product: 2-Pyrimidinamine, N-methyl- (9CI) 931-61-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 25kg
Release date: 2019-07-12

931-61-3, 2-Pyrimidinamine, N-methyl- (9CI)Related Search:

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2-Pyrimidinamine, N-methyl- (9CI)

N-Methyl-2-pyrimidinamine

methyl(pyrimidin-2-yl)amine

NSC 102272

2-PyriMidinaMine, N-Methyl-

2-Pyrimidinamine, N-methyl- (9CI) ISO 9001：2015 REACH

931-61-3

PYRIMIDINE