ChemicalBook > CAS DataBase List > 1H-Indole, 2,6-dimethyl-
1H-Indole, 2,6-dimethyl-
- Product Name
- 1H-Indole, 2,6-dimethyl-
- CAS No.
- 5649-36-5
- Chemical Name
- 1H-Indole, 2,6-dimethyl-
- Synonyms
- 2,6-DiMethyl-1H-Indole;1H-Indole, 2,6-dimethyl-
- CBNumber
- CB11239244
- Molecular Formula
- C10H11N
- Formula Weight
- 145.2
- MOL File
- 5649-36-5.mol
More
Less
1H-Indole, 2,6-dimethyl- Property
- Melting point:
- 82.5°C (estimate)
- Boiling point:
- 273.05°C
- Density
- 1.0641 (estimate)
- refractive index
- 1.6030 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 17.93±0.30(Predicted)
- Appearance
- Off-white to light yellow Solid
More
Less
Safety
- HS Code
- 2933998090
More
Less
N-Bromosuccinimide Price
Biosynth Carbosynth
- Product number
- FD141688
- Product name
- 2,6-Dimethyl-1H-indole
- Packaging
- 50mg
- Price
- $62
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FD141688
- Product name
- 2,6-Dimethyl-1H-indole
- Packaging
- 100mg
- Price
- $108
- Updated
- 2021/12/16
AK Scientific
- Product number
- Z4891
- Product name
- 2,6-Dimethyl-1H-indole
- Packaging
- 250mg
- Price
- $131
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FD141688
- Product name
- 2,6-Dimethyl-1H-indole
- Packaging
- 250mg
- Price
- $215
- Updated
- 2021/12/16
Apolloscientific
- Product number
- OR929350
- Product name
- 2,6-Dimethyl-1H-indole
- Purity
- 95%
- Packaging
- 1g
- Price
- $300
- Updated
- 2021/12/16
More
Less
1H-Indole, 2,6-dimethyl- Chemical Properties,Usage,Production
Synthesis
67-64-1
108-44-1
5649-36-5
General procedure for the synthesis of 2,6-dimethyl-1H-indole (VI) from acetone and 3-methylaniline: in a reaction tube, 3-methylaniline (5.00 g, 0.046 mol), anhydrous copper(II) acetate (18.6 g, 0.093 mol), and palladium(II) acetate (0.208 g, 0.930 mmol) were dissolved in a mixture of acetone (25 mL) and dimethyl sulfoxide (25 mL) in a mixed solution and the reaction was heated at 90 °C for 18 hours. After completion of the reaction, it was cooled to room temperature and the reaction mixture was poured into cold water and extracted with ethyl acetate (2 x 250 mL). The organic layer was separated and washed sequentially with water and brine. The organic layer was dried with anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography (100-200 mesh) with gradient elution of ethyl acetate/hexane to afford the target compound VI (1.0 g, 15% yield).1H NMR (400 MHz, CDCl3): δ 10.70 (s, 1H), 7.23 (d, J = 8.00 Hz, 1H), 7.02 (s, 1H), 6.72 (d J = 7.8 Hz, 1H), 6.01 (s, 1H), 2.34 (s, 6H); MS (ESI, positive mode) m/z 146 ([M+H]+).
References
[1] Patent: WO2015/73528, 2015, A1. Location in patent: Page/Page column 102
1H-Indole, 2,6-dimethyl- Preparation Products And Raw materials
Raw materials
Preparation Products
More
Less
1H-Indole, 2,6-dimethyl- Suppliers
- Tel
- 021-54306202 13764082696
- info@hanhongsci.com
- Country
- China
- ProdList
- 42934
- Advantage
- 64
- Tel
- 027-86697669 13986148687
- Fax
- 86-027-86697669
- sales@tcaschem.com
- Country
- China
- ProdList
- 4127
- Advantage
- 55
- Tel
- 86(512)5235 8471 17715136450
- Fax
- 86(512)5235 6881
- sales@shiyabiopharm.com
- Country
- China
- ProdList
- 4169
- Advantage
- 58
- Tel
- 021-60343070
- Fax
- 021-35122006
- Country
- China
- ProdList
- 12740
- Advantage
- 55
- Tel
- +86 (21) 6715-7650
- Fax
- +86 (21) 6715-7651
- sheepchem@163.com
- Country
- China
- ProdList
- 994
- Advantage
- 60
- Tel
- 027-027-87342388 18086026008
- Fax
- 027-87342388
- sales@kaymke.com
- Country
- China
- ProdList
- 3731
- Advantage
- 55
- Tel
- +86-28-85122536 85324413
- Fax
- +86-28-85326443
- market@astatech.cn
- Country
- China
- ProdList
- 8026
- Advantage
- 55
- Tel
- 021-61995394 18916691159
- chemicalsea@163.com
- Country
- China
- ProdList
- 1972
- Advantage
- 58
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39966
- Advantage
- 60
- Tel
- 021-60345187 13671753212
- Fax
- 021-34702061
- lzz841106@aliyun.com
- Country
- China
- ProdList
- 10263
- Advantage
- 55
- Tel
- 微信 17321281695 18019252918
- Fax
- 17321281695
- sale@amkchem.com
- Country
- China
- ProdList
- 15136
- Advantage
- 55
- Tel
- 021-61478794
- Fax
- 021-61478794
- sales@hcshhai.com
- Country
- China
- ProdList
- 9793
- Advantage
- 50
- Tel
- +86-021-58380978 13482386415
- Fax
- 021-58380978
- info@systeambc.com
- Country
- China
- ProdList
- 896
- Advantage
- 50
- Tel
- +86-021-61654350
- Fax
- +86-021-61654350
- 1245958370@qq.com
- Country
- China
- ProdList
- 2982
- Advantage
- 50
- Tel
- 021-64340559 13651849907;
- Fax
- 021- 64345308
- xinyu_shi@jwypharmlab.com.cn
- Country
- China
- ProdList
- 12000
- Advantage
- 58
- Tel
- 021-34979681; 17701870669
- Fax
- 021-34979681
- 41513101@qq.com
- Country
- China
- ProdList
- 1785
- Advantage
- 55
- Tel
- 21-33526724 18930996265
- Fax
- +86 21 37023730
- info@carlowchem.com
- Country
- China
- ProdList
- 1969
- Advantage
- 50
- Tel
- 13764913901
- Fax
- -
- info@angtibio.com
- Country
- China
- ProdList
- 4981
- Advantage
- 55
- Tel
- 021-61312847; 18021002903
- Fax
- QQ:3008007432
- 3008007409@qq.com
- Country
- China
- ProdList
- 71826
- Advantage
- 60
- Tel
- 02781293128
- orders@biochemsafebuy.com
- Country
- China
- ProdList
- 9923
- Advantage
- 55
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- 025-66162170
- Fax
- 025-66162170
- Country
- China
- ProdList
- 7181
- Advantage
- 55
- Tel
- 021-20432229
- Fax
- QQ2412110556
- 2412110556@qq.com
- Country
- China
- ProdList
- 6017
- Advantage
- 55
- Tel
- 13811826434
- Fax
- -
- lichen13811826434@126.com
- Country
- China
- ProdList
- 663
- Advantage
- 58
- Tel
- 400-711-5280 86-571-81025280
- Fax
- 86-571-85806285
- sales@molcore.com
- Country
- China
- ProdList
- 9967
- Advantage
- 58
- Tel
- 021-021-021-31663258 13795219287
- Fax
- 021-31663258
- donghuanwen@126.com
- Country
- China
- ProdList
- 8816
- Advantage
- 58
- Tel
- 028-65791793 18140026355
- Fax
- QQ568470422
- 568470422@qq.com
- Country
- China
- ProdList
- 9997
- Advantage
- 58
- Tel
- 025-58859352 18068836627
- Fax
- 02557626880
- sales01@aikonchem.com
- Country
- China
- ProdList
- 15083
- Advantage
- 58
- Tel
- 13918479294
- Fax
- -
- xiebenfa@163.com
- Country
- China
- ProdList
- 4092
- Advantage
- 58
- Tel
- 400-8210725 400821072
- Fax
- 021-58955996
- malulu@leyan.com
- Country
- China
- ProdList
- 25000
- Advantage
- 58
- Tel
- 4009004166/18616739031 18616739031
- 3007523370@qq.com
- Country
- China
- ProdList
- 52687
- Advantage
- 58
- Tel
- 021-58581007 18019463053
- Fax
- 021-50966098
- sales@coolpharm.com
- Country
- China
- ProdList
- 12878
- Advantage
- 58
- Tel
- +8613062833949
- fred.wen@crcorporation.cn
- Country
- China
- ProdList
- 8645
- Advantage
- 58
- Tel
- +8618795957998
- karmelhk@126.com
- Country
- CHINA
- ProdList
- 2886
- Advantage
- 58
- Tel
- +8617735180244
- mike_yan@xuanranglobal.com
- Country
- CHINA
- ProdList
- 4017
- Advantage
- 58
- Tel
- 17321241880
- 485229790@qq.com
- Country
- China
- ProdList
- 1750
- Advantage
- 58
- Tel
- 0751-2886766 13927870850
- Fax
- 0751-2886756
- 3001267247@qq.com
- Country
- China
- ProdList
- 9941
- Advantage
- 58
- Tel
- 021-58461859 15821823057
- service@aiviche.com
- Country
- China
- ProdList
- 49312
- Advantage
- 58
- Tel
- +86-0371-86658258 +8613203830695
- Fax
- 0086-371-86658258
- factory@coreychem.com
- Country
- China
- ProdList
- 29798
- Advantage
- 58
- Tel
- +86-0519-85551759 +8613506123987
- Fax
- +0086-519-85557389
- marketing1@neostarunited.com
- Country
- China
- ProdList
- 8830
- Advantage
- 58
- Tel
- 18001895509
- Fax
- QQ2934193566;
- 986383309@qq.com
- Country
- China
- ProdList
- 2680
- Advantage
- 58
- Tel
- 021-58432009 400-005-6266
- Fax
- 021-58436166
- marketing@energy-chemical.com
- Country
- China
- ProdList
- 44918
- Advantage
- 58
- Tel
- 021-51816796-820 13611835272
- Fax
- 021-5161 3951
- sales2@sunwaypharm.com
- Country
- China
- ProdList
- 44119
- Advantage
- 58
- Tel
- 13180081292 13180081292
- contact@wetogethermed.com
- Country
- China
- ProdList
- 7943
- Advantage
- 58
- Tel
- 1483287082 19962651230
- sales@allbiopharm.com
- Country
- China
- ProdList
- 1529
- Advantage
- 58
- Tel
- 021-61109150
- Fax
- 021-61105897
- sales@tcisct.com
- Country
- China
- ProdList
- 29668
- Advantage
- 58
- Tel
- 18721109360
- 306685371@qq.com
- Country
- China
- ProdList
- 1944
- Advantage
- 58
- Tel
- 0751-18902340975/189023400307 18902340307
- Fax
- 0751-2819901
- 3356812514@qq.com
- Country
- China
- ProdList
- 9249
- Advantage
- 58
- Tel
- 4000255188
- Fax
- 025 86918232
- sales_china@pharmablock.com
- Country
- China
- ProdList
- 10000
- Advantage
- 58
- Tel
- 400-6005915
- sales@picasso-e.com
- Country
- China
- ProdList
- 39665
- Advantage
- 58
More
Less
View Lastest Price from 1H-Indole, 2,6-dimethyl- manufacturers
Career Henan Chemical Co
- Product
- 1H-Indole, 2,6-dimethyl- 5649-36-5
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-09
5649-36-5, 1H-Indole, 2,6-dimethyl-Related Search:
4',6-Diamidino-2-phenylindole dihydrochloride
P-AMIDINOPHENYL P-(6-AMIDINO-2-INDOLYL)PHENYL ETHER DIHYDROCHLORIDE
(2,6,7-TRIMETHYL-1H-INDOL-3-YL)-ACETIC ACID
2-PHENYL-1H-INDOLE-6-CARBOXYLIC ACID
DAPI
4-(2,6-DIMETHYL-1H-INDOL-3-YL)-THIAZOL-2-YLAMINE
INDO 1 TETRAPOTASSIUM SALT
RO-32-0432
6-methyl-2-phenyl-1H-indole
INDO 1 PENTAPOTASSIUM SALT
INDO 1-AM
ETHYL 5-HYDROXY-6-(4-METHOXYPHENYL)-1,2-DIMETHYL-1H-INDOLE-3-CARBOXYLATE
VOACORINE
granular blue
2-(2,4,6-TRIMETHYL-1H-INDOL-3-YL)-ETHYLAMINE
(6,7,8,9-TETRAHYDRO-5H-CARBAZOL-2-YL)-ACETIC ACID
ETHYL 5-HYDROXY-1,2-DIMETHYL-6-PHENYL-1H-INDOLE-3-CARBOXYLATE