N-(1-Ethylpropyl)-3,4-dimethylaniline

Product Name: N-(1-Ethylpropyl)-3,4-dimethylaniline
CAS No.: 56038-89-2
Chemical Name: N-(1-Ethylpropyl)-3,4-dimethylaniline
Synonyms: N-(1-Ethylpropyl)-3,4-xylidine;N-3-pentyl-3,4-dimethylaniline;3,4-dimethyl-N-pentan-3-yl-aniline;N-(1-ETHYLPROPYL)-3,4-DIMETHYLANILINE;Benzenamine, N-(1-ethylpropyl)-3,4-dimethyl-;Benzenamine, N-(1-ethylpropyl)-4,5-dimethyl-;N-(1-Ethylpropyl)-3,4-diMethylaniline, N-(1-Ethylpropyl)-3,4-xylidine
CBNumber: CB11257251
Molecular Formula: C13H21N
Formula Weight: 191.31
MOL File: 56038-89-2.mol

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N-(1-Ethylpropyl)-3,4-dimethylaniline Property

Boiling point:: 290.2±9.0 °C(Predicted)
Density: 0.920±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
solubility: Chloroform (Sparingly), Methanol (Sparingly)
form: Oil
pka: 6.11±0.33(Predicted)
color: Pale Brown to Brown
EPA Substance Registry System: Benzenamine, N-(1-ethylpropyl)-3,4-dimethyl- (56038-89-2)

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: E938678
Product name: N-(1-Ethylpropyl)-3,4-xylidine
Packaging: 5g
Price: $80
Updated: 2021/12/16

TRC

Product number: E938678
Product name: N-(1-Ethylpropyl)-3,4-xylidine
Packaging: 1g
Price: $50
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD150716
Product name: 3,4-Dimethyl-N-(pentan-3-yl)aniline
Packaging: 50mg
Price: $52
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD150716
Product name: 3,4-Dimethyl-N-(pentan-3-yl)aniline
Packaging: 250mg
Price: $180
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD150716
Product name: 3,4-Dimethyl-N-(pentan-3-yl)aniline
Packaging: 500mg
Price: $315
Updated: 2021/12/16

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N-(1-Ethylpropyl)-3,4-dimethylaniline Chemical Properties,Usage,Production

Uses

N-(1-Ethylpropyl)-3,4-xylidine is a useful compound in the synthesis of dinitro herbicides via one-step dinitration with nitric acid in continuous-flow microreactor.

Synthesis

31599-61-8

616-24-0

56038-89-2

General method: 3,4-dimethyliodobenzene (0.10 mol) was dissolved in xylene (200 mL), bis(triphenylphosphine)dichloropalladium (0.0005 mol) and potassium tert-butoxide (0.20 mol) were added sequentially, and after stirring, 3-aminopentane (0.11 mol) was added. The temperature of the reaction system was raised to 90 °C and the reaction was maintained at this temperature for 6 hours. After completion of the reaction, the mixture was cooled to room temperature and filtered. The filtrate was washed sequentially with 100 mL of 5% aqueous citric acid solution, 100 mL of saturated sodium carbonate solution and 100 mL of saturated sodium chloride solution, and the organic phase was dried with anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure until no bubbles were produced to give 18.4 g of the oily product N-(1-ethylpropyl)-3,4-dimethylaniline. Based on the amount of 3,4-dimethyliodobenzene fed, the product yield was 96.3% and the purity was 96.8% as determined by HPLC.

References

[1] Patent: CN108530303, 2018, A. Location in patent: Paragraph 0025; 0026; 0027; 0028; 0032

N-(1-Ethylpropyl)-3,4-dimethylaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(1-Ethylpropyl)-3,4-dimethylaniline Suppliers

China 49 India 2 Ukraine 3 United Kingdom 1 United States 7 Global 62

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View Lastest Price from N-(1-Ethylpropyl)-3,4-dimethylaniline manufacturers

Career Henan Chemical Co

Product: N-(1-Ethylpropyl)-3,4-dimethylaniline 56038-89-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 85.0-99.8%
Supply Ability: 20 tons
Release date: 2019-12-24

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56038-89-2