ChemicalBook > CAS DataBase List > 2-AMINO-4-FLUOROBENZONITRILE

2-AMINO-4-FLUOROBENZONITRILE

Uses

Product Name: 2-AMINO-4-FLUOROBENZONITRILE
CAS No.: 80517-22-2
Chemical Name: 2-AMINO-4-FLUOROBENZONITRILE
Synonyms: 4-Fluoroanthranilonitrile;Amino-4-fluorobenzonitrile;2-Amino-4-fluorobenzonitrile;Benzonitrile, 2-amino-4-fluoro-;4-Fluoroanthranilonitrile, 2-Cyano-5-fluoroaniline
CBNumber: CB11263751
Molecular Formula: C7H5FN2
Formula Weight: 136.13
MOL File: 80517-22-2.mol

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2-AMINO-4-FLUOROBENZONITRILE Property

Melting point:: 102.2 °C (decomp)
Boiling point:: 284.7±25.0 °C(Predicted)
Density: 1.25±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: crystals
pka: 0.80±0.10(Predicted)
color: Light purple

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Safety

HazardClass: TOXIC
HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A898183
Product name: 2-Amino-4-fluorobenzonitrile
Packaging: 250mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA67713
Product name: 2-Amino-4-fluorobenzonitrile
Packaging: 25g
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA67713
Product name: 2-Amino-4-fluorobenzonitrile
Packaging: 50g
Price: $120
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0002679
Product name: 2-AMINO-4-FLUOROBENZONITRILE
Purity: 95.00%
Packaging: 1G
Price: $130.2
Updated: 2021/12/16

Matrix Scientific

Product number: 066865
Product name: 2-Amino-4-fluorobenzonitrile
Purity: 98%
Packaging: 25g
Price: $144
Updated: 2021/12/16

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2-AMINO-4-FLUOROBENZONITRILE Chemical Properties,Usage,Production

Uses

2-Amino-4-fluorobenzonitrile is a useful research chemical for organic synthesis and other chemical processes.

Synthesis

3939-09-1

80517-22-2

53312-80-4

Using 2,4-difluorobenzonitrile (2.78 g, 20 mmol) and 3,4,5-trimethoxybenzylamine (3.94 g, 20 mmol) as raw material, the two were mixed and heated at 140 °C for 40 min. After completion of the reaction, the mixture was cooled to room temperature and subsequently dissolved in trifluoroacetic acid (TFA, 20 mL) and stirred at room temperature overnight. Afterwards, the mixture was concentrated using a rotary evaporator and subsequently partitioned between 1N NaOH solution (~100 mL, adjusted to alkaline) and ethyl acetate (100 mL). After separation of the organic layer, the aqueous layer was extracted with additional ethyl acetate (100 mL). All organic layers were combined, washed with brine (50 mL), dried over anhydrous magnesium sulfate (MgSO4) and concentrated to give an oil. Separation of the mixture by column chromatography (eluent: 10% to 40% hexane solution of ethyl acetate) gave two well separated isomeric products. Further concentration gave 4-amino-2-fluorobenzonitrile (1.07 g, 39% yield) as a white solid. The structure of the product was confirmed by LC/MS (m/z = 177.8, corresponding to the determination of [M+H]+ in acetonitrile).

References

[1] Patent: US2008/76813, 2008, A1. Location in patent: Page/Page column 28

2-AMINO-4-FLUOROBENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-AMINO-4-FLUOROBENZONITRILE manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 2-AMINO-4-FLUOROBENZONITRILE 80517-22-2
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2024-11-08

R&D Scientific Inc.

Product: 2-Amino-4-fluorobenzonitrile 80517-22-2
Price: US $580.00/g
Min. Order: 1g
Purity: 98
Supply Ability: 500 Kg
Release date: 2024-02-14

Career Henan Chemical Co

Product: 2-AMINO-4-FLUOROBENZONITRILE 80517-22-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-03

80517-22-2, 2-AMINO-4-FLUOROBENZONITRILERelated Search:

FIPRONIL-DESULFINYL AMINOACETONITRILE 2-Nitrobenzonitrile 2-Chlorobenzonitrile Benzonitrile, 2-amino-4,5-difluoro- (9CI) IFLAB-BB F2108-0005 4-FLUORO-2-ISOCYANATOBENZONITRILE 4-FLUORO-2-NITROBENZONITRILE 4-FLUORO-2-IMIDAZOL-1-YL-BENZONITRILE 2-AMINO-4-FLUOROBENZONITRILE

4-Fluoroanthranilonitrile, 2-Cyano-5-fluoroaniline

Amino-4-fluorobenzonitrile

2-Amino-4-fluorobenzonitrile

Benzonitrile, 2-amino-4-fluoro-

4-Fluoroanthranilonitrile

80517-22-2

Phenyls & Phenyl-Het