ChemicalBook > CAS DataBase List > 3,4-Pyridinediamine,5-methyl-(9CI)

3,4-Pyridinediamine,5-methyl-(9CI)

Product Name: 3,4-Pyridinediamine,5-methyl-(9CI)
CAS No.: 13958-86-6
Chemical Name: 3,4-Pyridinediamine,5-methyl-(9CI)
Synonyms: 5-Methylpyridin-3,4-diaMine;5-Methylpyridine-3,4-diaMine;3,4-Diamino-5-methylpyridine;5-Methyl-3,4-pyridinediamine;3,4-Pyridinediamine, 5-methyl-;3,4-Pyridinediamine,5-methyl-(9CI)
CBNumber: CB11271563
Molecular Formula: C6H9N3
Formula Weight: 123.16
MOL File: 13958-86-6.mol

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3,4-Pyridinediamine,5-methyl-(9CI) Property

Melting point:: 149 °C
Boiling point:: 363.1±37.0 °C(Predicted)
Density: 1.190
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 9.40±0.24(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M340613
Product name: 5-Methylpyridine-3,4-diamine
Packaging: 100mg
Price: $90
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0390941
Product name: 5-METHYLPYRIDINE-3,4-DIAMINE
Purity: 95.00%
Packaging: 5MG
Price: $498.75
Updated: 2021/12/16

Matrix Scientific

Product number: 081262
Product name: 5-Methylpyridine-3,4-diamine
Purity: 95%
Packaging: 500mg
Price: $365
Updated: 2021/12/16

AK Scientific

Product number: Y7493
Product name: 5-Methylpyridine-3,4-diamine
Packaging: 10g
Price: $1004
Updated: 2021/12/16

Matrix Scientific

Product number: 081262
Product name: 5-Methylpyridine-3,4-diamine
Purity: 95%
Packaging: 1g
Price: $561
Updated: 2021/12/16

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3,4-Pyridinediamine,5-methyl-(9CI) Chemical Properties,Usage,Production

Synthesis

18227-67-3

13958-86-6

The general procedure for the synthesis of 5-methyl-3,4-diaminopyridine from 4-amino-5-methyl-3-nitropyridine was as follows: a mixture of 4-amino-5-methyl-3-nitropyridine (1.198 g), iron powder (1.748 g), ethanol (52 mL), and hydrochloric acid (13 mL) was heated and refluxed for 3 hours. After completion of the reaction, the mixture was cooled to room temperature and ethanol was removed by distillation. The resulting suspension was diluted to 50 mL with water and the pH was adjusted to 13 by slow addition of 2N NaOH solution. extraction was carried out with ethyl acetate (3 x 70 mL), the organic phases were combined and dried with anhydrous sodium sulfate. Finally, the solvent was evaporated to give 0.579 g (60% yield) of 5-methyl-3,4-diaminopyridine.

References

[1] Patent: WO2005/63744, 2005, A2. Location in patent: Page/Page column 232

3,4-Pyridinediamine,5-methyl-(9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3,4-Pyridinediamine,5-methyl-(9CI) manufacturers

Career Henan Chemical Co

Product: 3,4-Pyridinediamine,5-methyl-(9CI) 13958-86-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-26

Nanjing jinheyou Trading Co., Ltd.

Product: 3,4-Pyridinediamine,5-methyl-(9CI) 13958-86-6
Price: US $0.00/g
Min. Order: 1g
Purity: 95%min
Supply Ability: 30kgs/month
Release date: 2019-11-14

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