3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE

Product Name: 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
CAS No.: 226260-01-1
Chemical Name: 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
Synonyms: 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE;Benzamide, 3-fluoro-N-methoxy-N-methyl-
CBNumber: CB1151907
Molecular Formula: C9H10FNO2
Formula Weight: 183.18
MOL File: 226260-01-1.mol

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3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE Property

Boiling point:: 300.5±25.0 °C(Predicted)
Density: 1.179±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature

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Safety

HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 1381AB
Product name: 3-Fluoro-N-methoxy-N-methylbenzamide
Packaging: 25g
Price: $181
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0021914
Product name: 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
Purity: 95.00%
Packaging: 5G
Price: $1239.43
Updated: 2021/12/16

Chemenu

Product number: CM251490
Product name: 3-Fluoro-N-methoxy-N-methylbenzamide
Purity: 95%
Packaging: 10g
Price: $234
Updated: 2021/12/16

Alichem

Product number: 226260011
Product name: 3-Fluoro-N-methoxy-N-methylbenzamide
Packaging: 10g
Price: $257.5
Updated: 2021/12/16

Chemenu

Product number: CM251490
Product name: 3-Fluoro-N-methoxy-N-methylbenzamide
Purity: 95%
Packaging: 25g
Price: $468
Updated: 2021/12/16

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3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE Chemical Properties,Usage,Production

Synthesis

6638-79-5

1711-07-5

226260-01-1

Triethylamine (Et3N, 383 g, 3.78 mol) was added to a solution of N,O-dimethylhydroxylamine hydrochloride (138 g, 1.42 mol) in dichloromethane (DCM, 1.5 L) at room temperature (RT). 3-Fluorobenzoyl chloride (150 g, 946 mmol) was added dropwise to the stirred mixture at 0 °C and protected by nitrogen (N2). The reaction solution was stirred at the same temperature for 1 hour, followed by slow warming to room temperature and continued stirring for 10 hours. The reaction mixture was poured into water (~1 L) and extracted with ethyl acetate (EtOAc, 2 x 500 mL). The organic phases were combined, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated. The residue was purified by fast column chromatography (eluent: petroleum ether, PE) to afford N-methyl-N-methoxy-3-fluorobenzamide (1-2) as a white solid (150 g, yield: 86.5%).1H NMR (400 MHz, CDCl3): δ 7.49-7.43 (1H, m), 7.41-7.32 (2H, m), 7.18 -7.10 (1H, m), 3.54 (3H, s), 3.34 (3H, s).

References

[1] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 4, p. 1415 - 1419
[2] Patent: WO2016/145103, 2016, A1. Location in patent: Paragraph 0165
[3] Patent: US6174874, 2001, B1
[4] Patent: US2008/249095, 2008, A1. Location in patent: Page/Page column 44

3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE Suppliers

China 65 India 1 United Kingdom 1 United States 11 Global 78

Adamas Reagent, Ltd.

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Shanghai SuperLan Chemcial Technique Centre

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View Lastest Price from 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE manufacturers

Career Henan Chemical Co

Product: 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 226260-01-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-08

226260-01-1, 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDERelated Search:

N-METHOXY-N-METHYLBENZAMIDE 4-BROMO-2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 4-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 4-cyano-3-fluoro-N-methoxy-N-methylbenzamide 4-CHLORO-2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 2-bromo-4-fluoro-N-methoxy-N-methylbenzamide 3-bromo-4-fluoro-N-methoxy-N-methylbenzamide 4-BROMO-3-FLUORO-N-METHOXY-N-METHYL-BENZAMIDE 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 3,4-DIFLUORO-N-METHOXY-N-METHYLBENZAMIDE

3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE

Benzamide, 3-fluoro-N-methoxy-N-methyl-

226260-01-1