ChemicalBook > CAS DataBase List > 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE

3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE

Product Name
3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
CAS No.
226260-01-1
Chemical Name
3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
Synonyms
3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE;Benzamide, 3-fluoro-N-methoxy-N-methyl-
CBNumber
CB1151907
Molecular Formula
C9H10FNO2
Formula Weight
183.18
MOL File
226260-01-1.mol
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3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE Property

Boiling point:
300.5±25.0 °C(Predicted)
Density 
1.179±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
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Safety

HS Code 
2924297099
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
1381AB
Product name
3-Fluoro-N-methoxy-N-methylbenzamide
Packaging
25g
Price
$181
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0021914
Product name
3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
Purity
95.00%
Packaging
5G
Price
$1239.43
Updated
2021/12/16
Chemenu
Product number
CM251490
Product name
3-Fluoro-N-methoxy-N-methylbenzamide
Purity
95%
Packaging
10g
Price
$234
Updated
2021/12/16
Alichem
Product number
226260011
Product name
3-Fluoro-N-methoxy-N-methylbenzamide
Packaging
10g
Price
$257.5
Updated
2021/12/16
Chemenu
Product number
CM251490
Product name
3-Fluoro-N-methoxy-N-methylbenzamide
Purity
95%
Packaging
25g
Price
$468
Updated
2021/12/16
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3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE Chemical Properties,Usage,Production

Synthesis

6638-79-5

1711-07-5

226260-01-1

Triethylamine (Et3N, 383 g, 3.78 mol) was added to a solution of N,O-dimethylhydroxylamine hydrochloride (138 g, 1.42 mol) in dichloromethane (DCM, 1.5 L) at room temperature (RT). 3-Fluorobenzoyl chloride (150 g, 946 mmol) was added dropwise to the stirred mixture at 0 °C and protected by nitrogen (N2). The reaction solution was stirred at the same temperature for 1 hour, followed by slow warming to room temperature and continued stirring for 10 hours. The reaction mixture was poured into water (~1 L) and extracted with ethyl acetate (EtOAc, 2 x 500 mL). The organic phases were combined, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated. The residue was purified by fast column chromatography (eluent: petroleum ether, PE) to afford N-methyl-N-methoxy-3-fluorobenzamide (1-2) as a white solid (150 g, yield: 86.5%).1H NMR (400 MHz, CDCl3): δ 7.49-7.43 (1H, m), 7.41-7.32 (2H, m), 7.18 -7.10 (1H, m), 3.54 (3H, s), 3.34 (3H, s).

References

[1] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 4, p. 1415 - 1419
[2] Patent: WO2016/145103, 2016, A1. Location in patent: Paragraph 0165
[3] Patent: US6174874, 2001, B1
[4] Patent: US2008/249095, 2008, A1. Location in patent: Page/Page column 44

3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE Suppliers

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View Lastest Price from 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE manufacturers

Career Henan Chemical Co
Product
3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 226260-01-1
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-08

226260-01-1, 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDERelated Search:

N-METHOXY-N-METHYLBENZAMIDE 4-BROMO-2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 4-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 4-cyano-3-fluoro-N-methoxy-N-methylbenzamide 4-CHLORO-2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 2-bromo-4-fluoro-N-methoxy-N-methylbenzamide 3-bromo-4-fluoro-N-methoxy-N-methylbenzamide 4-BROMO-3-FLUORO-N-METHOXY-N-METHYL-BENZAMIDE 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 3,4-DIFLUORO-N-METHOXY-N-METHYLBENZAMIDE

  • 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
  • Benzamide, 3-fluoro-N-methoxy-N-methyl-
  • 226260-01-1