ChemicalBook > CAS DataBase List > 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER

5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER

Application

Product Name: 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER
CAS No.: 773873-77-1
Chemical Name: 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER
Synonyms: RARECHEM AL BF 0374;Methyl 5-BroMoindole-3-carboxylate;METHYL 5-BROMO-1H-INDOLE-3-CARBOXYLATE;1H-Indole-3-carboxylicacid,5-broMo-,Methylester;5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER;5-Bromo-1H-Indole-3-Carboxylic Acid Methyl Ester, 10 mM in DMSO
CBNumber: CB1191525
Molecular Formula: C10H8BrNO2
Formula Weight: 254.08
MOL File: 773873-77-1.mol

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5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER Property

Melting point:: 212-214 °C
Boiling point:: 386.2±22.0 °C(Predicted)
Density: 1.629±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.46±0.30(Predicted)
Appearance: White to off-white Solid
CAS DataBase Reference: 773873-77-1

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M295663
Product name: Methyl5-Bromoindole-3-carboxylate
Packaging: 250mg
Price: $55
Updated: 2021/12/16

Apolloscientific

Product number: OR962104
Product name: Methyl5-bromo-1H-indole-3-carboxylate
Purity: 98%
Packaging: 5g
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: J51148
Product name: Methyl5-bromo-1H-indole-3-carboxylate
Packaging: 5g
Price: $80
Updated: 2021/12/16

Matrix Scientific

Product number: 073274
Product name: Methyl 5-bromo-1H-indole-3-carboxylate
Purity: 95+%
Packaging: 1g
Price: $82
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB56545
Product name: 5-Bromo-1H-indole-3-carboxylic acid methyl ester
Packaging: 500mg
Price: $95
Updated: 2021/12/16

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5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER Chemical Properties,Usage,Production

Application

Methyl 5-bromoindole-3-carboxylic acid can be used as an organic synthesis intermediate. It can be prepared in two steps from 5-bromo-1H-indole as a reactant, or it can be obtained by one-step esterification of 5-bromo-1H-indole-3-carboxylic acid.

Synthesis

67-56-1

10406-06-1

773873-77-1

GENERAL METHOD: 4.0 g of 5-bromo-1H-indole-3-carboxylic acid was dissolved in 40 times the volume (400 mL) of methanol and a catalytic amount of concentrated sulfuric acid was slowly added. The reaction mixture was heated to reflux for 5 hours, followed by slow cooling to room temperature. Ice-cold water was added to the cooled mixture and the yellow solid was collected by filtration. The solid was recrystallized from ethanol to give methyl 5-bromo-indole-3-carboxylate (12b) as a yellow solid in 62% yield. The product characterization data were as follows: melting point: 210-212 °C; IR (KBr, cm-1): 3213, 3114, 2929, 1745; 1H NMR (400 MHz, CDCl3): δ 3.93 (3H, s, -OCH3), 7.28 (1H, d, J = 8.8 Hz, Ar-H), 7.35 (1H, m, Ar-H ), 7.91 (1H, d, J = 2.8 Hz, Ar-H), 8.32 (1H, s, Ar-H), 8.67 (1H, s, -NH); 13C NMR (400 MHz, CDCl3 + DMSO-d6): δ 49.93, 105.91, 112.88, 113.75, 122.40, 124.26, 126.65, 131.89, 134.33, 164.13; HRMS (m/z): calculated value C10H9NO2Br [M]+: 253.98112, measured value: 253.98102.

References

[1] Chemical Papers, 2018, vol. 72, # 6, p. 1369 - 1378

5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER Preparation Products And Raw materials

Raw materials

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View Lastest Price from 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER manufacturers

Career Henan Chemical Co

Product: 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER 773873-77-1
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-08

Career Henan Chemical Co

Product: 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER 773873-77-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-08

773873-77-1, 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTERRelated Search:

5-Bromoindole-2-carboxylic acid methyl ester 5-BROMOISOINDOLINE 2-BROMO-4-CYANOTHIOPHENE 5-BROMOISOQUINOLIN-1-AMINE 5-Bromoindole 5-BROMOPHTHALAZINE 4-(4-Bromo-phenyl)-pyridine 5-Bromothiazole-4-carboxylic acid 5-BROMOTRYPTAMINE HYDROCHLORIDE 5-Bromoindole-2-carboxylic acid 5-Bromoindole trimer RARECHEM AL BI 0374 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID 5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER 6-BROMO-1H-INDOLE-2-CARBOXYLIC ACID METHYL ESTER 7-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER 3-Bromo-1H-indole-2-carboxylic acid methyl ester 2-Bromo-3-cyclohexyl-indole-6-carboxylic Acid Methyl Ester

1H-Indole-3-carboxylicacid,5-broMo-,Methylester

Methyl 5-BroMoindole-3-carboxylate

5-BROMO-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER

METHYL 5-BROMO-1H-INDOLE-3-CARBOXYLATE

RARECHEM AL BF 0374

5-Bromo-1H-Indole-3-Carboxylic Acid Methyl Ester, 10 mM in DMSO

773873-77-1