Cyclohexanecarbonitrile, 4-hydroxy-

Product Name: Cyclohexanecarbonitrile, 4-hydroxy-
CAS No.: 24056-34-6
Chemical Name: Cyclohexanecarbonitrile, 4-hydroxy-
Synonyms: 4-hydroxycyclohexanecarbonitrile;4-hydroxycyclohexane-1-carbonitrile;Cyclohexanecarbonitrile, 4-hydroxy-
CBNumber: CB12473676
Molecular Formula: C7H11NO
Formula Weight: 125.17
MOL File: 24056-34-6.mol

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Cyclohexanecarbonitrile, 4-hydroxy- Property

Boiling point:: 153-154 °C(Press: 12 Torr)
Density: 1.05±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.69±0.40(Predicted)
Appearance: Colorless to light yellow Oil

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: H954983
Product name: 4-Hydroxycyclohexanecarbonitrile
Packaging: 100mg
Price: $110
Updated: 2021/12/16

ChemScene

Product number: CS-D1577
Product name: 4-Hydroxycyclohexanecarbonitrile
Purity: >97.0%
Packaging: 250mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: W4762
Product name: 4-Hydroxycyclohexanecarbonitrile
Packaging: 100mg
Price: $133
Updated: 2021/12/16

ChemScene

Product number: CS-D1577
Product name: 4-Hydroxycyclohexanecarbonitrile
Purity: >97.0%
Packaging: 1g
Price: $185
Updated: 2021/12/16

Matrix Scientific

Product number: 074528
Product name: 4-Hydroxycyclohexanecarbonitrile
Purity: 95+%
Packaging: 500mg
Price: $255
Updated: 2021/12/16

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Cyclohexanecarbonitrile, 4-hydroxy- Chemical Properties,Usage,Production

Synthesis

34916-10-4

24056-34-6

The general procedure for the synthesis of 4-hydroxycyclohexanecarbonitrile from 4-oxocyclohexanecarbonitrile was as follows: 4-oxocyclohexanecarbonitrile (10 g, 81.20 mmol, 1.00 eq.) and methanol (100 mL) were added to a 250 mL four-necked round-bottomed flask under inert nitrogen protection. Subsequently, sodium borohydride (1.52 g, 40.18 mmol, 0.50 eq.) was slowly added in an ice-water bath at 0 °C. The reaction mixture was stirred at room temperature for 1 hour. Upon completion of the reaction, the reaction was quenched by the addition of 20 mL of aqueous ammonium chloride. The reaction mixture was extracted with ethyl acetate (2 x 100 mL), the organic layers were combined and dried with anhydrous sodium sulfate. Finally, the organic layer was concentrated under reduced pressure to afford 4-hydroxycyclohexanecarbonitrile (10.02 g, 99% yield) as a colorless oil.

References

[1] Patent: US2017/166584, 2017, A1. Location in patent: Paragraph 0887-0889
[2] Annales de Chimie (Cachan, France), 1955, vol. <12> 10, p. 497,531
[3] Bulletin de la Societe Chimique de France, 1954, p. 610,612
[4] Patent: WO2009/156100, 2009, A1. Location in patent: Page/Page column 156

Cyclohexanecarbonitrile, 4-hydroxy- Preparation Products And Raw materials

Raw materials

Preparation Products

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Cyclohexanecarbonitrile, 4-hydroxy- Suppliers

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Cyclohexanecarbonitrile, 4-hydroxy-

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24056-34-6