ChemicalBook > CAS DataBase List > N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE

N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE

Product Name: N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE
CAS No.: 25892-08-4
Chemical Name: N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE
Synonyms: N-(2,6-Difluoro-3-nitrophenyl);N-(2,6-Difluoro-3-nitrophenyl)acetaMid;N-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE;N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE;Acetamide, N-(2,6-difluoro-3-nitrophenyl)-;N1-(2,6-difluoro-3-nitrophenyl)acetamide 95+%
CBNumber: CB1252600
Molecular Formula: C8H6F2N2O3
Formula Weight: 216.14
MOL File: 25892-08-4.mol

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N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE Property

Melting point:: 148 °C
Boiling point:: 352.7±42.0 °C(Predicted)
Density: 1.513±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 12.03±0.70(Predicted)
Appearance: Off-white to light yellow Solid

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Safety

HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D451180
Product name: N-(2,6-Difluoro-3-nitrophenyl)acetamide
Packaging: 500mg
Price: $130
Updated: 2021/12/16

Matrix Scientific

Product number: 074736
Product name: N-(2,6-Difluoro-3-nitrophenyl)acetamide
Purity: 95+%
Packaging: 1g
Price: $268
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD105530
Product name: N-(2,6-difluoro-3-nitrophenyl)acetamide
Packaging: 1g
Price: $300
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD105530
Product name: N-(2,6-difluoro-3-nitrophenyl)acetamide
Packaging: 2g
Price: $500
Updated: 2021/12/16

AK Scientific

Product number: W4923
Product name: N-(2,6-Difluoro-3-nitro-phenyl)-acetamide
Packaging: 10g
Price: $617
Updated: 2021/12/16

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N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE Chemical Properties,Usage,Production

Synthesis

3896-29-5

25892-08-4

1. cool sulfuric acid (53.3 mL, 760 mmol) in an ice-water bath and slowly add nitric acid (25.6 mL, 610 mmol), keeping the temperature below 10°C. 2. add N-(2,6-difluorophenyl)acetamide (13.0 g, 76.0 mmol) to the mixed acid solution. 2. N-(2,6-difluorophenyl)acetamide (13.0 g, 76.0 mmol) was added to the above mixed acid solution in batches, ensuring that the reaction temperature was maintained at room temperature. 3. The reaction mixture was stirred at room temperature for 18 hours to carry out the nitration reaction. 4. Upon completion of the reaction, the mixture was slowly poured into ice water to precipitate a yellow solid. 5. The precipitate was collected by filtration and the solid residue was washed well with cold water. 6. The product was dried over air to give 2,6-difluoro-3-nitro-acetanilide (11.2 g, 51.8 mmol, 68% yield) as a yellow solid. 7. The product was analyzed by LCMS (1:1). 7. The product was characterized by LCMS (ESI, cationic mode): calculated C8H6F2N2O3 [M+H]+ 216.0, measured 217.2. 8. 1H NMR (ESI, cationic mode) was performed on the product. 8. 1H NMR (300 MHz, DMSO-d6) δ ppm: 10.04 (br s, 1H, NH), 8.02-8.28 (m, 1H, ArH), 7.44 (td, J = 9.1, 1.8 Hz, 1H, ArH), 2.11 (s, 3H, CH3).

References

[1] Journal of Chemical Research, 2004, # 10, p. 699 - 701
[2] Bioorganic and Medicinal Chemistry, 2016, vol. 24, # 10, p. 2215 - 2234
[3] Patent: WO2012/85127, 2012, A1. Location in patent: Page/Page column 39
[4] Patent: WO2012/101238, 2012, A1. Location in patent: Page/Page column 38
[5] Patent: US2012/322803, 2012, A1. Location in patent: Page/Page column 17

N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE manufacturers

Career Henan Chemical Co

Product: N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDE 25892-08-4
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

25892-08-4, N1-(2,6-DIFLUORO-3-NITROPHENYL)ACETAMIDERelated Search:

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25892-08-4

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