6-bromo-3-methoxypyridin-2-amine
- Product Name
- 6-bromo-3-methoxypyridin-2-amine
- CAS No.
- 916737-77-4
- Chemical Name
- 6-bromo-3-methoxypyridin-2-amine
- Synonyms
- 6-bromo-3-methoxypyridin-2-amine;2-AMino-6-broMo-3-Methoxypyridine;2-PyridinaMine, 6-broMo-3-Methoxy-;6-Bromo-3-methoxy-pyridin-2-ylamine;2-Amino-6-bromo-3-methoxypyridine 97%
- CBNumber
- CB12538885
- Molecular Formula
- C6H7BrN2O
- Formula Weight
- 203.04
- MOL File
- 916737-77-4.mol
6-bromo-3-methoxypyridin-2-amine Property
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- Appearance
- White to light brown Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H332Harmful if inhaled
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P322Specific measures (see …on this label).
P330Rinse mouth.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B711208
- Product name
- 6-Bromo-3-methoxypyridin-2-amine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 5448AC
- Product name
- 6-Bromo-3-methoxypyridin-2-amine
- Packaging
- 250mg
- Price
- $107
- Updated
- 2021/12/16
- Product number
- 4H56-9-2R
- Product name
- 2-Amino-6-bromo-3-methoxypyridine
- Packaging
- 250mg
- Price
- $205
- Updated
- 2021/12/16
- Product number
- 4H56-9-2R
- Product name
- 2-Amino-6-bromo-3-methoxypyridine
- Packaging
- 1g
- Price
- $426
- Updated
- 2021/12/16
- Product number
- HCH0367760
- Product name
- 6-BROMO-3-METHOXYPYRIDIN-2-AMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $500.05
- Updated
- 2021/12/16
6-bromo-3-methoxypyridin-2-amine Chemical Properties,Usage,Production
Synthesis
916737-76-3
916737-77-4
Step 2: Preparation of 6-bromo-3-methoxypyridin-2-amine A mixture of 6-bromo-3-methoxy-2-nitropyridine (14.4 g, 61.8 mmol), acetic acid (200 mL), and iron powder (14.0 g, 0.25 mol) was stirred and reacted at 90°C for 1.5 hours. Upon completion of the reaction, the mixture was cooled to room temperature and diluted with ethyl acetate. Subsequently, the mixture was filtered through diatomaceous earth and the filtrate was concentrated under vacuum. Purification by fast column chromatography using dichloromethane as eluent afforded the target compound 6-bromo-3-methoxypyridin-2-amine (10.2 g, 50.2 mmol) as a white solid.1H NMR (400 MHz, DMSO-d6) δ: 3.81 (s, 3H), 4.78 (br.s, 2H), 6.73 (d, J = 7.8 Hz 1H).
References
[1] Patent: WO2014/184234, 2014, A1. Location in patent: Page/Page column 63
[2] Patent: WO2014/6402, 2014, A1. Location in patent: Page/Page column 85
6-bromo-3-methoxypyridin-2-amine Preparation Products And Raw materials
Raw materials
Preparation Products
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