ChemicalBook > CAS DataBase List > 2-Chloro-7-Methoxyquinoline

2-Chloro-7-Methoxyquinoline

Product Name
2-Chloro-7-Methoxyquinoline
CAS No.
49609-15-6
Chemical Name
2-Chloro-7-Methoxyquinoline
Synonyms
2-Chloro-7-Methoxyquinoline;QUINOLINE, 2-CHLORO-7-METHOXY-
CBNumber
CB12618060
Molecular Formula
C10H8ClNO
Formula Weight
193.63
MOL File
49609-15-6.mol
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2-Chloro-7-Methoxyquinoline Property

Melting point:
97-98 °C
Boiling point:
145 °C(Press: 0.6 Torr)
Density 
1.267±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
0.65±0.50(Predicted)
Appearance
Off-white to light brown Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C632238
Product name
2-Chloro-7-methoxyquinoline
Packaging
10mg
Price
$45
Updated
2021/12/16
TRC
Product number
C632238
Product name
2-Chloro-7-methoxyquinoline
Packaging
50mg
Price
$130
Updated
2021/12/16
TRC
Product number
C632238
Product name
2-Chloro-7-methoxyquinoline
Packaging
100mg
Price
$200
Updated
2021/12/16
AK Scientific
Product number
6723AB
Product name
2-Chloro-7-methoxyquinoline
Packaging
100mg
Price
$341
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0363643
Product name
2-CHLORO-7-METHOXYQUINOLINE
Purity
95.00%
Packaging
5MG
Price
$501.77
Updated
2021/12/16
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2-Chloro-7-Methoxyquinoline Chemical Properties,Usage,Production

Synthesis

23981-26-2

49609-15-6

General procedure: 300 mg (1.9 mmol) of 7-methoxyquinolin-2(1H)-one was dissolved in 1.1 mL of phosphorus oxychloride (POCl3, 12 mmol) and the reaction was heated to reflux for 3 hours. Upon completion of the reaction, the reaction mixture was slowly poured into ice water, neutralized to neutral with saturated sodium bicarbonate (NaHCO3) solution and subsequently extracted with ethyl acetate. After treatment, the target product 2-chloro-7-methoxyquinoline was obtained in 98% yield. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 8.01 (d, J = 8.5 Hz, 1H), 7.68 (d, J = 8.9 Hz, 1H), 7.35 (d, J = 2.4 Hz, 1H), 7.25 (d, J = 8.3 Hz, 1H), 7.20 (dd, J = 8.9, 2.5 Hz, 1H), and 3.93 (s, 3H).

References

[1] Patent: WO2016/130968, 2016, A1. Location in patent: Page/Page column 183-184
[2] Patent: WO2014/85284, 2014, A1. Location in patent: Paragraph 00222

2-Chloro-7-Methoxyquinoline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Chloro-7-Methoxyquinoline manufacturers

Career Henan Chemical Co
Product
2-Chloro-7-Methoxyquinoline 49609-15-6
Price
US $2.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
100g , 1kg, 5kg , 50kg
Release date
2020-01-07

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  • 49609-15-6