5-Fluoro-2-Methoxy-pyridin-3-ylaMine

Product Name: 5-Fluoro-2-Methoxy-pyridin-3-ylaMine
CAS No.: 1211541-93-3
Chemical Name: 5-Fluoro-2-Methoxy-pyridin-3-ylaMine
Synonyms: 5-Fluoro-2-Methoxypyridin-3-aMine;3-Amino-5-fluoro-2-methoxypyridine;3-Pyridinamine, 5-fluoro-2-methoxy-;5-Fluoro-2-Methoxy-pyridin-3-ylaMine
CBNumber: CB12642355
Molecular Formula: C6H7FN2O
Formula Weight: 142.13
MOL File: 1211541-93-3.mol

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5-Fluoro-2-Methoxy-pyridin-3-ylaMine Property

storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: Brown to reddish brown Solid
InChI: InChI=1S/C6H7FN2O/c1-10-6-5(8)2-4(7)3-9-6/h2-3H,8H2,1H3
InChIKey: DXTSVOMMBXIDKL-UHFFFAOYSA-N
SMILES: C1(OC)=NC=C(F)C=C1N

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: PC201061
Product name: 5-Fluoro-2-methoxypyridin-3-amine
Purity: 97%
Packaging: 250mg
Price: $128
Updated: 2021/12/16

Medical Isotopes, Inc.

Product number: 35921
Product name: 5-Fluoro-2-methoxypyridin-3-amine
Purity: 95+%
Packaging: 250mg
Price: $480
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367400
Product name: 5-FLUORO-2-METHOXYPYRIDIN-3-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $495.15
Updated: 2021/12/16

AK Scientific

Product number: 3720AA
Product name: 5-Fluoro-2-methoxypyridin-3-amine
Packaging: 1g
Price: $506
Updated: 2021/12/16

Medical Isotopes, Inc.

Product number: 35921
Product name: 5-Fluoro-2-methoxypyridin-3-amine
Purity: 95+%
Packaging: 1000mg
Price: $750
Updated: 2021/12/16

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5-Fluoro-2-Methoxy-pyridin-3-ylaMine Chemical Properties,Usage,Production

Synthesis

1211534-27-8

1211541-93-3

c) 5-fluoro-2-methoxy-3-nitropyridine (Preparation 5b, 0.300 g, 1.74 mmol) was used as a raw material, which was dissolved in ethanol and 10% palladium carbon catalyst (0.300 g) was added. The reaction mixture was stirred at room temperature and under hydrogen atmosphere. after 5 h, the reaction was completed and the catalyst was removed by Celite filtration. The filter cake was washed with ethanol and the filtrate and washings were combined and concentrated to afford the target product 5-fluoro-2-methoxypyridin-3-amine (0.220 g, 89% yield) as a brown solid. Low resolution mass spectrometry (LRMS) showed m/z: 143 (M+1)+. 1H NMR (300 MHz, CDCl3) data: δ 3.96 (s, 3H), 6.67 (dd, 1H), 7.39 (d, 1H).

References

[1] Patent: EP2527344, 2012, A1. Location in patent: Page/Page column 22-23
[2] Patent: WO2012/160030, 2012, A1. Location in patent: Page/Page column 67
[3] Patent: WO2016/106331, 2016, A1. Location in patent: Paragraph 0201

5-Fluoro-2-Methoxy-pyridin-3-ylaMine Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Fluoro-2-Methoxy-pyridin-3-ylaMine Suppliers

China 41 India 1 United States 2 Global 44

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1211541-93-3