Oxetan-3-yl Methanesulfonate
- Product Name
- Oxetan-3-yl Methanesulfonate
- CAS No.
- 148430-81-3
- Chemical Name
- Oxetan-3-yl Methanesulfonate
- Synonyms
- Oxetan-3-yl Methanesulfonate;3-Oxetanol 3-Methanesulfonate
- CBNumber
- CB12645851
- Molecular Formula
- C4H8O4S
- Formula Weight
- 152.17
- MOL File
- 148430-81-3.mol
Oxetan-3-yl Methanesulfonate Property
- Boiling point:
- 308.9±31.0 °C(Predicted)
- Density
- 1.38±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Safety
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HS Code
- 29309090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- E589565
- Product name
- oxetan-3-ylmethanesulfonate
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 7340CZ
- Product name
- Oxetan-3-ylmethanesulfonate
- Packaging
- 250mg
- Price
- $134
- Updated
- 2021/12/16
- Product number
- 6H64-1-09
- Product name
- Oxetan-3-yl methanesulfonate
- Packaging
- 1g
- Price
- $240
- Updated
- 2021/12/16
- Product number
- CHM0393743
- Product name
- OXETAN-3-YL METHANESULFONATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.9
- Updated
- 2021/12/16
- Product number
- CM200585
- Product name
- Oxetan-3-ylmethanesulfonate
- Purity
- 95%
- Packaging
- 5g
- Price
- $505
- Updated
- 2021/12/16
Oxetan-3-yl Methanesulfonate Chemical Properties,Usage,Production
Synthesis
7748-36-9
124-63-0
148430-81-3
To a solution of oxetan-3-ol (5 g, 67.5 mmol) and triethylamine (14.11 mL, 101 mmol) in dichloromethane (150 mL) was added methanesulfonyl chloride (6.79 mL, 88 mmol) dropwise at 0 °C. The reaction mixture was stirred at room temperature for 3 hours. After completion of the reaction, the solid was removed by filtration and the filtrate was washed sequentially with ice water and saturated saline. The organic phase was dried with anhydrous sodium sulfate and subsequently concentrated under reduced pressure to afford oxetan-3-yl methanesulfonate (11.7 g, 67.5 mmol, 100% yield) as an oil containing 12.2 wt% dichloromethane. The product was characterized by 1H NMR (400 MHz, CDCl3): δ 3.06 (s, 3H), 4.79-4.82 (m, 2H), 4.86-4.90 (m, 2H), 5.52-5.49 (m, 1H).
References
[1] Patent: WO2013/55910, 2013, A1. Location in patent: Page/Page column 124; 125
[2] Patent: TW2017/8221, 2017, A. Location in patent: Page/Page column 98; 99
[3] Patent: WO2015/181186, 2015, A1. Location in patent: Page/Page column 169
[4] Journal of Medicinal Chemistry, 2017, vol. 60, # 23, p. 9769 - 9789
[5] Journal of Medicinal Chemistry, 2018, vol. 61, # 6, p. 2518 - 2532
Oxetan-3-yl Methanesulfonate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Oxetan-3-yl Methanesulfonate manufacturers
- Product
- Oxetan-3-yl Methanesulfonate 148430-81-3
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 95%-99%
- Supply Ability
- 100kg
- Release date
- 2018-12-22