2,5-DICHLOROANISOLE
- Product Name
- 2,5-DICHLOROANISOLE
- CAS No.
- 1984-58-3
- Chemical Name
- 2,5-DICHLOROANISOLE
- Synonyms
- Banair;2,5-DICHLOROANISOLE;2,5-DICHLOROANISOLE 99%;2,5-Dichloroanisole,99%;2,5-DICHLOROMETHOXYBENZENE;1,4-dichloro-2-methoxy-benzen;1,4-DICHLORO-2-METHOXYBENZENE;Benzene, 1,4-dichloro-2-methoxy-;2,5-Dichloromethoxybenzene 1,4-Dichloro-2-methoxybenzene;1,4-Dichloro-2-methoxybenzene, 2,5-Dichlorophenyl methyl ether
- CBNumber
- CB1278840
- Molecular Formula
- C7H6Cl2O
- Formula Weight
- 177.03
- MOL File
- 1984-58-3.mol
2,5-DICHLOROANISOLE Property
- Melting point:
- 24°C
- Boiling point:
- 128-132°C 3,5mm
- Density
- 1.33
- refractive index
- 1.5615-1.5635
- Flash point:
- 21°C
- storage temp.
- Inert atmosphere,Room Temperature
- form
- Liquid
- color
- Clear colorless to very slightly yellow
- BRN
- 2327401
- CAS DataBase Reference
- 1984-58-3(CAS DataBase Reference)
- EPA Substance Registry System
- 2,5-Dichloroanisole (1984-58-3)
Safety
- Hazard Codes
- Xn,Xi
- Risk Statements
- 36/37/38-20/22
- Safety Statements
- 37/39-26-23
- RIDADR
- 1993
- Hazard Note
- Irritant
- TSCA
- Yes
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D2605
- Product name
- 2,5-Dichloroanisole
- Packaging
- 5g
- Price
- $91
- Updated
- 2025/07/31
- Product number
- D2605
- Product name
- 2,5-Dichloroanisole
- Packaging
- 25g
- Price
- $281
- Updated
- 2025/07/31
- Product number
- D444960
- Product name
- 1,4-Dichloro-2-methoxybenzene
- Packaging
- 5g
- Price
- $55
- Updated
- 2021/12/16
- Product number
- 2607-5-X1
- Product name
- 2,5-Dichloroanisole
- Packaging
- 25g
- Price
- $64
- Updated
- 2021/12/16
- Product number
- 2607-5-X1
- Product name
- 2,5-Dichloroanisole
- Packaging
- 5G
- Price
- $16
- Updated
- 2021/12/16
2,5-DICHLOROANISOLE Chemical Properties,Usage,Production
Chemical Properties
clear colorless to very slightly yellow liquid
Uses
1,4-Dichloro-2-methoxybenzene is a useful reagent for organic synthesis.
Synthesis
67-56-1
120-82-1
583-78-8
95-77-2
553-82-2
1984-58-3
120-83-2
36404-30-5
1,2,4-Trichlorobenzene (TCB), 50 wt% aqueous NaOH and methanol were added to a pressure reactor at a molar ratio of 1.0:2.4:10. The reactor was sealed and heated to 190°C under stirring conditions and maintained at this temperature for 90 minutes. Continuous stirring was maintained during the reaction. Upon completion of the reaction, the reactor was cooled to room temperature using an ice water bath. The reaction mixture was transferred to a separatory funnel and acidified with 10% H2SO4 to a pH below 1.5. Subsequently, dichloromethane was extracted three times with an aqueous layer. The final yield of 2,5-dichlorophenol was 64.6%. The ratio of regioselectivity (2,5-dichlorophenol to 2,5-dichloroanisole/2,4-dichlorophenol to 2,4-dichloroanisole/3,4-dichlorophenol to 3,4-dichloroanisole) was 71.9:15.5:12.6 as analyzed by gas chromatography (GC).
References
[1] Patent: WO2015/49160, 2015, A1. Location in patent: Page/Page column 11
[2] Patent: WO2015/49360, 2015, A1. Location in patent: Page/Page column 14
2,5-DICHLOROANISOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,5-DICHLOROANISOLE manufacturers
- Product
- 2,5-DICHLOROANISOLE 1984-58-3
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99.%
- Supply Ability
- 10 ton
- Release date
- 2024-08-21
- Product
- 2,5-DICHLOROANISOLE 1984-58-3
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11