2,3-DICHLOROANISOLE
- Product Name
- 2,3-DICHLOROANISOLE
- CAS No.
- 1984-59-4
- Chemical Name
- 2,3-DICHLOROANISOLE
- Synonyms
- 2,3-DICHLORANISOL;2,3-DICHLOROANISOLE;DICHLOROANISOLE(2,3-);2,3-Dichloroanisole>Miconazole Impurity 11;2,3-Dichloroanisole,96%;2,3-DICHLOROANISOLE, 97+%;2,3-DICHLOROMETHOXYBENZENE;2,3-Dichloroanisole, ≥ 97.0%;2,3-Dichloro-1-methoxybenzene
- CBNumber
- CB9114018
- Molecular Formula
- C7H6Cl2O
- Formula Weight
- 177.03
- MOL File
- 1984-59-4.mol
2,3-DICHLOROANISOLE Property
- Melting point:
- 31-33 °C(lit.)
- Boiling point:
- 115-116°C 12mm
- Density
- 1.2970 (rough estimate)
- refractive index
- 1.5430 (estimate)
- Flash point:
- >230 °F
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- Chloroform, Methanol
- form
- Solid
- color
- Off-White
- Water Solubility
- Soluble in water (86.9 mg/L).
- BRN
- 1909166
- InChI
- InChI=1S/C7H6Cl2O/c1-10-6-4-2-3-5(8)7(6)9/h2-4H,1H3
- InChIKey
- HFEASCCDHUVYKU-UHFFFAOYSA-N
- SMILES
- C1(Cl)=CC=CC(OC)=C1Cl
- CAS DataBase Reference
- 1984-59-4(CAS DataBase Reference)
- EPA Substance Registry System
- 2,3-Dichloroanisole (1984-59-4)
Safety
- Hazard Codes
- Xn
- Risk Statements
- 36/37/38-20/22
- Safety Statements
- 22-24/25-37/39-26
- WGK Germany
- 3
- TSCA
- Yes
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 156752
- Product name
- 2,3-Dichloroanisole
- Purity
- ≥97%
- Packaging
- 100g
- Price
- $226.1
- Updated
- 2025/07/31
- Product number
- D2306
- Product name
- 2,3-Dichloroanisole
- Purity
- >97.0%(GC)
- Packaging
- 25g
- Price
- $43
- Updated
- 2025/07/31
- Product number
- D2306
- Product name
- 2,3-Dichloroanisole
- Purity
- >97.0%(GC)
- Packaging
- 500g
- Price
- $408
- Updated
- 2025/07/31
- Product number
- D431830
- Product name
- 2,3-Dichloroanisole
- Packaging
- 25g
- Price
- $140
- Updated
- 2021/12/16
- Product number
- 009137
- Product name
- 2,3-Dichloroanisole
- Packaging
- 25g
- Price
- $425
- Updated
- 2021/12/16
2,3-DICHLOROANISOLE Chemical Properties,Usage,Production
Chemical Properties
white to brownish crystalline low melting solid
Agricultural Uses
2,3-Dichloroanisole is a volatile organic compound that has been shown to be an attractant for termites. It is used as a pesticide and agrochemical. 2,3-Dichloroanisole is used as an insecticide against termites and other pests in agriculture. This chemical has been shown to inhibit the sodium channel of the nerve cell membrane, which leads to paralysis of insects. The mechanism of action for this compound is not well understood but it has been suggested that it may act by blocking the reorientation of the sodium ion channels. 2,3-Dichloroanisole can also be used as a metal salt in some thermodynamic reactions.
Synthesis
576-24-9
77-78-1
1984-59-4
General procedure for the synthesis of 2,3-dichloroanisole from 2,3-dichlorophenol and dimethyl sulfate: 2,3-dichlorophenol (20.0 g, 122.7 mmol) was placed in a reaction flask, 120 mL of acetone was added to dissolve it, followed by the addition of potassium carbonate (18.7 g, 135.0 mmol), and magnetically stirred for 0.5 hours. Then dimethyl sulfate (17.0 g, 135.0 mmol) was slowly added dropwise through a dropping funnel and heated to 60°C and refluxed for 3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) (unfolding agent: petroleum ether/ethyl acetate=5:1, Rf=0.8). After completion of the reaction, it was cooled to room temperature, potassium carbonate was removed by filtration with a pump and the filter cake was washed with acetone. After evaporation to remove acetone, ethyl acetate and saturated sodium bicarbonate solution were added sequentially, and the organic phase was washed twice each time with saturated aqueous sodium chloride solution, and then the organic phase was dried with anhydrous sodium sulfate. After filtration, the solvent was evaporated under reduced pressure to give 2,3-dichloroanisole. The product was a colorless oil with a yield of 21.5 g and 99.1%.
References
[1] Patent: CN106916116, 2017, A. Location in patent: Paragraph 0063; 0064; 0065
[2] Recueil des Travaux Chimiques des Pays-Bas, 1918, vol. 37, p. 105
2,3-DICHLOROANISOLE Preparation Products And Raw materials
Raw materials
Preparation Products
2,3-DICHLOROANISOLE Suppliers
- Tel
- 0519-85607258 13912342323;
- Fax
- 0519-85607278
- sales@joyouschem.com
- Country
- China
- ProdList
- 294
- Advantage
- 60
- Tel
- 0512-68228771; 13776118946
- Fax
- 0512-68228771
- occasion_peter@126.com
- Country
- China
- ProdList
- 27
- Advantage
- 58
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 4006356688 18621169109
- Fax
- 86-21-61259102
- market03@meryer.com
- Country
- China
- ProdList
- 40228
- Advantage
- 62
- Tel
- 0418-6530555 2855550
- Fax
- +86-418-6502885
- Country
- China
- ProdList
- 338
- Advantage
- 69
- Tel
- 400-6106006
- Fax
- 021-67582001/03/05
- saleschina@alfa-asia.com
- Country
- China
- ProdList
- 30123
- Advantage
- 84
- Tel
- 021-67121386
- Fax
- 021-67121385
- Sales-CN@TCIchemicals.com
- Country
- China
- ProdList
- 24529
- Advantage
- 81
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 0311-89250318 031166536426
- Fax
- 4000311741
- master@sjzsdyn.com
- Country
- China
- ProdList
- 2806
- Advantage
- 65
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
View Lastest Price from 2,3-DICHLOROANISOLE manufacturers
- Product
- 2,3-DICHLOROANISOLE 1984-59-4
- Price
- US $8.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10TON
- Release date
- 2018-12-18