ChemicalBook > CAS DataBase List > 2,3-DICHLOROANISOLE

2,3-DICHLOROANISOLE

Product Name: 2,3-DICHLOROANISOLE
CAS No.: 1984-59-4
Chemical Name: 2,3-DICHLOROANISOLE
Synonyms: 2,3-DICHLORANISOL;2,3-DICHLOROANISOLE;DICHLOROANISOLE(2,3-);2,3-Dichloroanisole>Miconazole Impurity 11;2,3-Dichloroanisole,96%;2,3-DICHLOROANISOLE, 97+%;2,3-DICHLOROMETHOXYBENZENE;2,3-Dichloroanisole, ≥ 97.0%;2,3-Dichloro-1-methoxybenzene
CBNumber: CB9114018
Molecular Formula: C7H6Cl2O
Formula Weight: 177.03
MOL File: 1984-59-4.mol

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2,3-DICHLOROANISOLE Property

Melting point:: 31-33 °C(lit.)
Boiling point:: 115-116°C 12mm
Density: 1.2970 (rough estimate)
refractive index: 1.5430 (estimate)
Flash point:: >230 °F
storage temp.: Inert atmosphere,Room Temperature
solubility: Chloroform, Methanol
form: Solid
color: Off-White
Water Solubility: Soluble in water (86.9 mg/L).
BRN: 1909166
InChI: InChI=1S/C7H6Cl2O/c1-10-6-4-2-3-5(8)7(6)9/h2-4H,1H3
InChIKey: HFEASCCDHUVYKU-UHFFFAOYSA-N
SMILES: C1(Cl)=CC=CC(OC)=C1Cl
CAS DataBase Reference: 1984-59-4(CAS DataBase Reference)
EPA Substance Registry System: 2,3-Dichloroanisole (1984-59-4)

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Safety

Hazard Codes: Xn
Risk Statements: 36/37/38-20/22
Safety Statements: 22-24/25-37/39-26
WGK Germany: 3
TSCA: Yes
HS Code: 29093090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 156752
Product name: 2,3-Dichloroanisole
Purity: ≥97%
Packaging: 100g
Price: $226.1
Updated: 2025/07/31

TCI Chemical

Product number: D2306
Product name: 2,3-Dichloroanisole
Purity: >97.0%(GC)
Packaging: 25g
Price: $43
Updated: 2025/07/31

TCI Chemical

Product number: D2306
Product name: 2,3-Dichloroanisole
Purity: >97.0%(GC)
Packaging: 500g
Price: $408
Updated: 2025/07/31

TRC

Product number: D431830
Product name: 2,3-Dichloroanisole
Packaging: 25g
Price: $140
Updated: 2021/12/16

Usbiological

Product number: 009137
Product name: 2,3-Dichloroanisole
Packaging: 25g
Price: $425
Updated: 2021/12/16

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2,3-DICHLOROANISOLE Chemical Properties,Usage,Production

Chemical Properties

white to brownish crystalline low melting solid

Agricultural Uses

2,3-Dichloroanisole is a volatile organic compound that has been shown to be an attractant for termites. It is used as a pesticide and agrochemical. 2,3-Dichloroanisole is used as an insecticide against termites and other pests in agriculture. This chemical has been shown to inhibit the sodium channel of the nerve cell membrane, which leads to paralysis of insects. The mechanism of action for this compound is not well understood but it has been suggested that it may act by blocking the reorientation of the sodium ion channels. 2,3-Dichloroanisole can also be used as a metal salt in some thermodynamic reactions.

Synthesis

576-24-9

77-78-1

1984-59-4

General procedure for the synthesis of 2,3-dichloroanisole from 2,3-dichlorophenol and dimethyl sulfate: 2,3-dichlorophenol (20.0 g, 122.7 mmol) was placed in a reaction flask, 120 mL of acetone was added to dissolve it, followed by the addition of potassium carbonate (18.7 g, 135.0 mmol), and magnetically stirred for 0.5 hours. Then dimethyl sulfate (17.0 g, 135.0 mmol) was slowly added dropwise through a dropping funnel and heated to 60°C and refluxed for 3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) (unfolding agent: petroleum ether/ethyl acetate=5:1, Rf=0.8). After completion of the reaction, it was cooled to room temperature, potassium carbonate was removed by filtration with a pump and the filter cake was washed with acetone. After evaporation to remove acetone, ethyl acetate and saturated sodium bicarbonate solution were added sequentially, and the organic phase was washed twice each time with saturated aqueous sodium chloride solution, and then the organic phase was dried with anhydrous sodium sulfate. After filtration, the solvent was evaporated under reduced pressure to give 2,3-dichloroanisole. The product was a colorless oil with a yield of 21.5 g and 99.1%.

References

[1] Patent: CN106916116, 2017, A. Location in patent: Paragraph 0063; 0064; 0065
[2] Recueil des Travaux Chimiques des Pays-Bas, 1918, vol. 37, p. 105

2,3-DICHLOROANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2,3-DICHLOROANISOLE manufacturers

Career Henan Chemical Co

Product: 2,3-DICHLOROANISOLE 1984-59-4
Price: US $8.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10TON
Release date: 2018-12-18

1984-59-4, 2,3-DICHLOROANISOLERelated Search:

1,2,4-TRICHLORODIBENZO-P-DIOXIN 2,3,5,6-TETRACHLOROANISOLE 2,3,4,5-TETRACHLOROANISOLE PENTACHLOROPHENOL DODECANOATE Ethacrynic acid 1,2,3,4,6,7,8,9-OCTACHLORODIBENZO-P-DIOXIN 2,3-DICHLOROANISOLE 1,2,3,4-TETRACHLORODIBENZO-P-DIOXIN L-PYROGLUTAMIC ACID PENTACHLOROPHENYL ESTER R(+)-IAA-94 2,3-DICHLOROPHENOXYACETIC ACID 2,3,6-TRICHLOROANISOLE PENTACHLOROANISOLE 3,5-DICHLOROANISOLE 2,6-DICHLOROANISOLE,2,6-DICHLOROANISOLE 99% 4-Nitro-2,6-dichloroanisole 3,5-DICHLOROANISOLE PESTANAL 2 6-DICHLOROANISOLE PESTANAL

1,2-DICHLORO-3-METHOXYBENZENE

DICHLOROANISOLE(2,3-)

1,2-dichloro-3-methoxy-benzen

2,3-DICHLOROMETHOXYBENZENE

2,3-DICHLOROANISOLE

2,3-DICHLORANISOL

ATRAZIN-2-HYDROXY PESTANAL, 250 MG

2,3-DICHLOROANISOLE, 97+%

2,3-Dichloro-1-methoxybenzene

2,3-Dichloroanisole,96%

2,3-Dichloromethoxybenzene 1,2-Dichloro-3-methoxybenzene

Benzene,1,2-dichloro-3-Methoxy-

2,3-Dichloroanisole&gt

Miconazole Impurity 11

2,3-Dichloroanisole, ≥ 97.0%

C12332300 2,3-Dichloroanisole

2,3-Dichloroanisole, 10 mM in DMSO

1984-59-4

Ethers

Oxygen Compounds

Organic Building Blocks

Building Blocks

Aromatics, Metabolites and Impurities, Pharmaceuticals, Intermediates & Fine Chemicals

Halogenated benzene series

Aromatic Ethers

Anisole

Anisoles, Alkyloxy Compounds & Phenylacetates

Chlorine Compounds