4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE
- Product Name
- 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE
- CAS No.
- 175204-45-2
- Chemical Name
- 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE
- Synonyms
- BUTTPARK 43\57-20;4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE;Pyridine, 4-(bromomethyl)-2,6-dichloro-;4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE, TECH.;4-(Bromomethyl)-2,6-Dichloro-Pyridine 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE, TECH.
- CBNumber
- CB1395480
- Molecular Formula
- C6H4BrCl2N
- Formula Weight
- 240.91
- MOL File
- 175204-45-2.mol
4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE Property
- Boiling point:
- 299.2±35.0 °C(Predicted)
- Density
- 1.770±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- pka
- -3.01±0.10(Predicted)
- form
- Crystalline Powder
- color
- Yellow
Safety
- Hazard Codes
- T
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HS Code
- 29333999
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B808163
- Product name
- 4-(Bromomethyl)-2,6-dichloropyridine
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FB53490
- Product name
- 4-(Bromomethyl)-2,6-dichloropyridine
- Packaging
- 50mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- FB53490
- Product name
- 4-(Bromomethyl)-2,6-dichloropyridine
- Packaging
- 100mg
- Price
- $80
- Updated
- 2021/12/16
- Product number
- OR27145
- Product name
- 4-(Bromomethyl)-2,6-dichloropyridine
- Packaging
- 1g
- Price
- $131
- Updated
- 2021/12/16
- Product number
- 3H32-D-Z6
- Product name
- 4-(Bromomethyl)-2,6-dichloropyridine
- Packaging
- 1g
- Price
- $144
- Updated
- 2021/12/16
4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE Chemical Properties,Usage,Production
Synthesis
101990-69-6
175204-45-2
General procedure for the synthesis of 4-bromomethyl-2,6-dichloropyridine using 2,6-dichloropyridine-4-methanol as starting material: a tetrahydrofuran solution of (2,6-dichloropyridin-4-yl)methanol was mixed with triphenylphosphine and N-bromosuccinimide at 0 °C, maintained at this temperature and the reaction mixture was stirred. After 2 hours of reaction, the reaction mixture was diluted with water and extracted with ethyl acetate (3 x 150 mL). The organic phases were combined and washed with brine (2 x 100 mL) and subsequently dried over anhydrous sodium sulfate. The dried organic phase was filtered and concentrated to give the crude product. The crude product was purified by column chromatography to yield 1.1 g of 4-bromomethyl-2,6-dichloropyridine [0795] as a colorless liquid. Mass spectral analysis showed MS (M + 1)+ = 241.8.
References
[1] Patent: US2017/355708, 2017, A1. Location in patent: Paragraph 0193; 0195
4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE manufacturers
- Product
- 4-(Bromomethyl)-2,6-dichloropyridine 175204-45-2
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2020-01-10