4'-METHOXY-2-METHYL-BIPHENYL

Synthesis

Product Name: 4'-METHOXY-2-METHYL-BIPHENYL
CAS No.: 92495-54-0
Chemical Name: 4'-METHOXY-2-METHYL-BIPHENYL
Synonyms: AKOS BAR-1281;4-o-Tolylanisole;Anisole, p-(o-tolyl)- (7CI);4'-methoxy-2-methylbiphenyl;4'-METHOXY-2-METHYL-BIPHENYL;4-METHOXY-2'-METHYL-1,1'-BIPHENYL;4'-Methoxy-2-methyl-1,1'-biphenyl;1-methoxy-4-(2-methylphenyl)benzene
CBNumber: CB1400391
Molecular Formula: C14H14O
Formula Weight: 198.26
MOL File: 92495-54-0.mol

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4'-METHOXY-2-METHYL-BIPHENYL Property

Melting point:: 97.8-98.6℃
Boiling point:: 140-141.5℃ (13 Torr)
Density: 1.016±0.06 g/cm3(Predicted)

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0150682
Product name: 4'-METHOXY-2-METHYL-BIPHENYL
Purity: 95.00%
Packaging: 5MG
Price: $495.45
Updated: 2021/12/16

Alichem

Product number: 52008943
Product name: 4-Methoxy-2-methylbiphenyl
Packaging: 1g
Price: $1490
Updated: 2021/12/16

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4'-METHOXY-2-METHYL-BIPHENYL Chemical Properties,Usage,Production

Synthesis

Open to the atmosphere, 4-bromoanisole (1.87 g, 10 mmol), o-tolylboronic acid (1.50 g, 11 mmol), KF (spray dried, dried in an oven overnight prior to use, 1.92 g, 33 mmol), and THF (10 mL) were added to a 100-ml round-bottomed Schlenk flflask equipped with a stir bar. The reaction system was flflushed with argon for about 5 min. P(t-Bu)3 (1.9 × 10–4 M stock solution in THF; 2.31 mL, 5.0 × 10–5 mmol) and Pd2(dba)3 (2.16 × 10–5 M stock solution in THF; 2.31 mL, 5.0 × 10–5 mmol) in THF were added sequentially. After 48 h at room temperature, the reaction mixture was diluted with ether or EtOAc, fifiltered through a pad of silica gel with copious washings, and then concentrated. The crude product was then purifified via column chromatography eluting with 5% ether in hexane to yield 1.94 g (98%) of 4-methoxy-2´-methylbiphenyl as a colorless liquid.

4'-METHOXY-2-METHYL-BIPHENYL Preparation Products And Raw materials

Raw materials

Preparation Products

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4'-METHOXY-2-METHYL-BIPHENYL Suppliers

China 11 Germany 2 Russia 1 United States 4 Global 18

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92495-54-0, 4'-METHOXY-2-METHYL-BIPHENYLRelated Search:

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4'-METHOXY-2-METHYL-BIPHENYL

4-METHOXY-2'-METHYL-1,1'-BIPHENYL

AKOS BAR-1281

Anisole, p-(o-tolyl)- (7CI)

4-o-Tolylanisole

1-methoxy-4-(2-methylphenyl)benzene

4'-Methoxy-2-methyl-1,1'-biphenyl

4'-methoxy-2-methylbiphenyl

92495-54-0