ChemicalBook > CAS DataBase List > 3-Fluoro-4-methylphenol

3-Fluoro-4-methylphenol

Product Name
3-Fluoro-4-methylphenol
CAS No.
452-78-8
Chemical Name
3-Fluoro-4-methylphenol
Synonyms
3-FLUORO-P-CRESOL;3-Fluoro-p-cresol>3-FLUORO-4-METHYLPHENOL;3-Fluoro-p-cresol (OH=1);2-Fluoro-4-hydroxytoluene;Phenol, 3-fluoro-4-methyl-;3-Fluoro-4-methylphenol, JRD,
CBNumber
CB1478242
Molecular Formula
C7H7FO
Formula Weight
126.13
MOL File
452-78-8.mol
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3-Fluoro-4-methylphenol Property

Melting point:
72 °C
Boiling point:
196 °C
Density 
1.17
refractive index 
1.5150
Flash point:
29 °C
storage temp. 
Inert atmosphere,Room Temperature
form 
powder to lump
pka
9.27±0.18(Predicted)
color 
White to Light yellow to Light orange
Odor
Phenol-like
InChI
InChI=1S/C7H7FO/c1-5-2-3-6(9)4-7(5)8/h2-4,9H,1H3
InChIKey
GJOOCAXPERKNMN-UHFFFAOYSA-N
SMILES
C1(O)=CC=C(C)C(F)=C1
CAS DataBase Reference
452-78-8(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
21/22-34-52-36-22
Safety Statements 
26-36/37/39-60-45
RIDADR 
2922
Hazard Note 
Irritant
HazardClass 
8
HS Code 
29081990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H227Combustible liquid

H302Harmful if swallowed

H312Harmful in contact with skin

H314Causes severe skin burns and eye damage

H315Causes skin irritation

H318Causes serious eye damage

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P309IF exposed or if you feel unwell:

P310Immediately call a POISON CENTER or doctor/physician.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical
Product number
F0481
Product name
3-Fluoro-p-cresol
Purity
>98.0%(GC)
Packaging
1g
Price
$32
Updated
2024/03/01
TCI Chemical
Product number
F0481
Product name
3-Fluoro-p-cresol
Purity
>98.0%(GC)
Packaging
5g
Price
$95
Updated
2024/03/01
Alfa Aesar
Product number
H31864
Product name
3-Fluoro-4-methylphenol, 97%
Packaging
1g
Price
$107
Updated
2021/12/16
Alfa Aesar
Product number
H31864
Product name
3-Fluoro-4-methylphenol, 97%
Packaging
5g
Price
$419
Updated
2021/12/16
TRC
Product number
F597145
Product name
3-Fluoro-4-methylphenol
Packaging
100mg
Price
$45
Updated
2021/12/16
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3-Fluoro-4-methylphenol Chemical Properties,Usage,Production

Uses

3-Fluoro-4-methylphenol is a phenolic derivative and can be used as a pharmaceutical intermediate.

Synthesis

3-Fluoro-4-methylaniline (5g, 39.95Immol) was dissolved in 10% sulfuric acid aqueous solution (100ml). Thereafter, the temperature was lowered to 0°C. thereto sodium nitrate (5.5g, 79.902mmol) was added, and the reaction mixture was stirred at same temperature for 30 minutes. Then the reaction mixture was stirred at 50°C for 30 minutes, and the last time, stirred at 80°C for 5 hours. Ice water was added to quench the reaction, and aqueous layer was extracted with ethyl acetate. Combined organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure. The residue was purified by column chromatography (n-hexane:ethyl acetate = 8:1) to give 2.26g (yield: 44.8%, colorless oil) of the target compound. 3-fluoro-4-methylphenol, yield 2.26g, 44.8% 1H NMR(400MHz, CDCl3): 6.98(1, J=8.6Hz, 1H), 6.52(m, 2H), 5.82(br, 1H), 2.12(s, 3H).

3-Fluoro-4-methylphenol Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Fluoro-4-methylphenol Suppliers

Americas 1 China 141 Europe 3 Germany 3 India 4 Italy 1 Japan 2 United Kingdom 17 United States 22 Global 194
Shandong Youfu Pharmaceutical Technology Co., Ltd.
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View Lastest Price from 3-Fluoro-4-methylphenol manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
3-Fluoro-4-methylphenol 452-78-8
Price
US $40.00-20.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200000KG
Release date
2024-08-05
Unipharm pharmaceutical industry Co., Ltd
Product
3-Fluoro-4-methylphenol 452-78-8
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
EX: 100kgs
Release date
2021-03-23
Career Henan Chemical Co
Product
3-FLUORO-4-METHYLPHENOL 452-78-8
Price
US $1.00/KG
Min. Order
1KG
Purity
95%~99%
Supply Ability
1ton
Release date
2019-12-18

452-78-8, 3-Fluoro-4-methylphenolRelated Search:

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  • 2-Fluoro-4-hydroxytoluene
  • 3-FLUORO-4-METHYLPHENOL
  • 3-FLUORO-P-CRESOL
  • 3-Fluoro-p-cresol (OH=1)
  • 3-Fluoro-4-methylphenol, JRD,
  • 3-Fluoro-p-cresol&gt
  • Phenol, 3-fluoro-4-methyl-
  • 452-78-8
  • Fluorine series
  • Aromatic Phenols
  • Phenol&Thiophenol&Mercaptan
  • Fluorine Compounds
  • Phenols