2-METHYLNICOTINALDEHYDE
Uses- Product Name
- 2-METHYLNICOTINALDEHYDE
- CAS No.
- 60032-57-7
- Chemical Name
- 2-METHYLNICOTINALDEHYDE
- Synonyms
- 2-METHYLNICOTINALDEHYDE;2-Methylpyridine-3-carbox...;2-Methylpyridine-3-carbaldehyde;2-Methylpyridine-3-carboxaldehyde;2-Methyl-3-Pyridinecarboxaldehyde;3-Pyridinecarboxaldehyde, 2-Methyl-;2-METHYLNICOTINALDEHYDE ISO 9001:2015 REACH
- CBNumber
- CB1494992
- Molecular Formula
- C7H7NO
- Formula Weight
- 121.14
- MOL File
- 60032-57-7.mol
2-METHYLNICOTINALDEHYDE Property
- Melting point:
- 242 °C (decomp)
- Boiling point:
- 94 °C(Press: 12 Torr)
- Density
- 1.106 g/mL at 25 °C
- refractive index
- n20/D1.549
- Flash point:
- 93℃
- storage temp.
- 2-8°C, stored under nitrogen
- form
- liquid
- pka
- 4.15±0.10(Predicted)
- color
- Pale yellow
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-37/38-41
- Safety Statements
- 26-39
- WGK Germany
- 3
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 741183
- Product name
- 2-Methylpyridine-3-carboxaldehyde
- Purity
- 97%
- Packaging
- 500mg
- Price
- $119
- Updated
- 2023/06/20
- Product number
- M323573
- Product name
- 2-Methylnicotinaldehyde
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- M323573
- Product name
- 2-Methylnicotinaldehyde
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 4H32-1-42
- Product name
- 2-Methylpyridine-3-carboxaldehyde
- Packaging
- 1g
- Price
- $225
- Updated
- 2021/12/16
- Product number
- W7274
- Product name
- 2-Methylnicotinaldehyde
- Packaging
- 5g
- Price
- $231
- Updated
- 2021/12/16
2-METHYLNICOTINALDEHYDE Chemical Properties,Usage,Production
Uses
2-Methylnicotinaldehyde is a useful research chemical.
Synthesis
56826-61-0
60032-57-7
General procedure for the synthesis of 2-methylpyridine-3-carbaldehyde from 2-methylpyridine-3-methanol: A mixture of 3-hydroxymethyl-2-methylpyridine (9.0 g, 73.1 mmol) and manganese(IV) dioxide (28.1 g, 322 mmol) in dichloromethane (100 mL) was heated and refluxed for 48 hours. Upon completion of the reaction, the insoluble material was removed by diatomaceous earth filtration and the filter cake was washed with a solvent mixture of methanol/dichloromethane. Subsequently, the solvent in the filtrate was removed by rotary evaporator to give 2-methylpyridine-3-carboxaldehyde (7.5 g, 85% yield) as an oily product. Its nuclear magnetic resonance hydrogen spectrum (NMR) data were as follows: δ 2.78 (s, 3H), 7.43 (dd, 1H), 8.15 (dd, 1H), 8.66 (dd, 1H).
References
[1] Patent: WO2006/106307, 2006, A1. Location in patent: Page/Page column 91
[2] Patent: WO2006/100461, 2006, A1. Location in patent: Page/Page column 83
[3] Chemical and Pharmaceutical Bulletin, 1994, vol. 42, # 9, p. 1841 - 1849
[4] Patent: WO2013/19682, 2013, A1. Location in patent: Page/Page column 101
[5] Patent: WO2013/19626, 2013, A1. Location in patent: Page/Page column 27
2-METHYLNICOTINALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-METHYLNICOTINALDEHYDE manufacturers
- Product
- 2-Methylnicotinaldehyde 60032-57-7
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- Customise
- Release date
- 2025-10-22
- Product
- 2-METHYLNICOTINALDEHYDE 60032-57-7
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-08-30
- Product
- 2-METHYLNICOTINALDEHYDE 60032-57-7
- Price
- US $5.50/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 1kg-100kg
- Release date
- 2020-01-10