ChemicalBook > CAS DataBase List > 1,4-Cyclohexanedione bis(ethylene ketal)
1,4-Cyclohexanedione bis(ethylene ketal)
- Product Name
- 1,4-Cyclohexanedione bis(ethylene ketal)
- CAS No.
- 183-97-1
- Chemical Name
- 1,4-Cyclohexanedione bis(ethylene ketal)
- Synonyms
- 1,4-Cyclohexanedione diethylene ketal;1,4-CYCLOHEXANEDIONE BIS(ETHYLENEKETAL);1,4-CYCLOHEXANEDIONE BISETHYLENE KETAL F;1,4-CYCLOHEXANEDIONE BIS(ETHYLENE ACETAL);1,4-Cyclohexianedione bis(ethylene acetal);1,4-Cyclohexanedione Bis(ethyleneketal) >1,4,9,12-TETRAOXADISPIRO[4.2.4.2]TETRADECANE;2,5-bis(butylamino)cyclohexa-2,5-diene-1,4-dione;1,4,9,12-tetraoxadispiro[4.2.4^{8}.2^{5}]tetradecane;Dispiro[1,3-dioxolane-2,1'-cyclohexane-4',2''-[1,3]dioxolane]
- CBNumber
- CB1668030
- Molecular Formula
- C10H16O4
- Formula Weight
- 200.23
- MOL File
- 183-97-1.mol
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1,4-Cyclohexanedione bis(ethylene ketal) Property
- Melting point:
- 79-80 °C (lit.)
- Boiling point:
- 75-85 °C/0.5 mmHg (lit.)
- Density
- 1.1508 (rough estimate)
- refractive index
- 1.4459 (estimate)
- Flash point:
- 75-85°C/0.5mm
- storage temp.
- Store below +30°C.
- form
- powder to crystal
- color
- White to Almost white
- InChI
- InChI=1S/C10H16O4/c1-2-10(13-7-8-14-10)4-3-9(1)11-5-6-12-9/h1-8H2
- InChIKey
- YSMVSEYPOBXSOK-UHFFFAOYSA-N
- SMILES
- O1C2(CCC3(OCCO3)CC2)OCC1
- CAS DataBase Reference
- 183-97-1(CAS DataBase Reference)
- NIST Chemistry Reference
- 1,4-Cyclohexanedione bis(ethylene ketal)(183-97-1)
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 298743
- Product name
- 1,4-Cyclohexanedione bis(ethylene ketal)
- Purity
- 99%
- Packaging
- 10g
- Price
- $96.8
- Updated
- 2023/06/20
TCI Chemical
- Product number
- C1544
- Product name
- 1,4-Cyclohexanedione Bis(ethyleneketal)
- Purity
- >99.0%(GC)
- Packaging
- 25g
- Price
- $65
- Updated
- 2024/03/01
Alfa Aesar
- Product number
- B20784
- Product name
- 1,4-Cyclohexanedione bis(ethylene acetal), 99%
- Packaging
- 10g
- Price
- $40.65
- Updated
- 2024/03/01
Alfa Aesar
- Product number
- B20784
- Product name
- 1,4-Cyclohexanedione bis(ethylene acetal), 99%
- Packaging
- 50g
- Price
- $118
- Updated
- 2021/12/16
Alfa Aesar
- Product number
- B20784
- Product name
- 1,4-Cyclohexanedione bis(ethylene acetal), 99%
- Packaging
- 250g
- Price
- $467.65
- Updated
- 2024/03/01
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1,4-Cyclohexanedione bis(ethylene ketal) Chemical Properties,Usage,Production
General Description
Hydrolysis of 1,4-cyclohexanedione bis(ethylene ketal) at 250°C has been reported.
Synthesis
After mixing 2243 g (20 mol) of 1,4-cyclohexanedione, 2607 g (42 mol) of ethylene glycol, the resin filtered, and 26 L of toluene, the temperature was raised slowly and refluxed for 11 hours to separate the water. The reaction temperature was lowered to 40° C., the resin was filtered, and the organic phase was concentrated until no liquid flowed. Then add 1257g (21mol) of methylboronic acid and 20L of n-heptane, raise the temperature to 80°C and react for 6 hours, then slowly cool down to 5-10°C in a gradient, filter, rinse the filter cake with n-heptane, and dry to obtain 1,4-Cyclohexanedione bis(ethylene ketal).
1,4-Cyclohexanedione bis(ethylene ketal) Preparation Products And Raw materials
Raw materials
Preparation Products
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1,4-Cyclohexanedione bis(ethylene ketal) Suppliers
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View Lastest Price from 1,4-Cyclohexanedione bis(ethylene ketal) manufacturers
Career Henan Chemical Co
- Product
- 1,4-Cyclohexanedione bis(ethylene ketal) 183-97-1
- Price
- US $5.50/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 1kg-100kg
- Release date
- 2020-01-14
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