ChemicalBook > CAS DataBase List > 6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE

6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE

Product Name: 6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE
CAS No.: 120-15-0
Chemical Name: 6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE
Synonyms: Thallin;AKOS BB-9796;TIMTEC-BB SBB002326;SALOR-INT L308625-1EA;Debrisoquine Impurity 11;6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE;Quinoline l,2,3,4-tetrahydro-6-methoxy;Quinoline, 1,2,3,4-tetrahydro-6-methoxy-;6-Methoxy-1,2,3,4-tetrahydroquinoline 99%;methyl 1,2,3,4-tetrahydro-6-quinolyl ether
CBNumber: CB1764400
Molecular Formula: C10H13NO
Formula Weight: 163.22
MOL File: 120-15-0.mol

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6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE Property

Melting point:: 37-41 °C (lit.)
Boiling point:: 290.31°C (rough estimate)
Density: 1.0508 (rough estimate)
refractive index: 1.5718 (estimate)
RTECS: VC2940000
Flash point:: >230 °F
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 5.95±0.20(Predicted)
CAS DataBase Reference: 120-15-0(CAS DataBase Reference)
EPA Substance Registry System: Quinoline, 1,2,3,4-tetrahydro-6-methoxy- (120-15-0)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36/37
WGK Germany: 3
TSCA: Yes
HazardClass: IRRITANT
HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: M268808
Product name: 6-Methoxy-1,2,3,4-tetrahydroquinoline
Packaging: 500mg
Price: $110
Updated: 2021/12/16

Ark Pharm

Product number: P000626393
Product name: 6-Methoxy-1,2,3,4-tetrahydroquinoline
Purity: 95+%
Packaging: 100mg
Price: $12
Updated: 2021/12/16

Ark Pharm

Product number: P000626393
Product name: 6-Methoxy-1,2,3,4-tetrahydroquinoline
Purity: 95+%
Packaging: 250mg
Price: $18
Updated: 2021/12/16

Matrix Scientific

Product number: 033158
Product name: 6-Methoxy-1,2,3,4-tetrahydro-quinoline
Packaging: 500mg
Price: $26
Updated: 2021/12/16

AK Scientific

Product number: J98188
Product name: 6-Methoxy-1,2,3,4-tetrahydroquinoline
Packaging: 1g
Price: $40
Updated: 2021/12/16

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6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE Chemical Properties,Usage,Production

Uses

1,2,3,4-Tetrahydro-6-methoxyquinoline is used as chemical reagents, organic intermediates, fine chemicals, pharmaceutical research and development.

Synthesis

5263-87-6

120-15-0

GENERAL STEPS: 6-methoxyquinoline (1a; 65 mg, 0.5 mmol), Cu(OAc)2 (4.5 mg, 0.025 mmol), B2(OH)4 (135 mg, 1.5 mmol) and acetonitrile (2.0 mL) were added to a 20 mL Schlenk tube. The reaction mixture was stirred at 40 °C for 8 h. The progress of the reaction was monitored by TLC until the reaction was completed. After completion of the reaction, the mixture was cooled to room temperature and concentrated under reduced pressure. Water (10 mL) was added to the concentrated mixture, followed by extraction with ethyl acetate (3 x 10 mL). The organic phases were combined, dried over anhydrous Na2SO4, filtered, and concentrated under reduced pressure. The residue was purified by column chromatography using petroleum ether/ethyl acetate (8:1) as eluent to afford the target product 6-methoxy-1,2,3,4-tetrahydroquinoline (2a: 65 mg, 98% yield) as a brown liquid.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 13, p. 3415 - 3418
[2] Advanced Synthesis and Catalysis, 2017, vol. 359, # 4, p. 677 - 686
[3] Advanced Synthesis and Catalysis, 2017, vol. 359, # 6, p. 933 - 940
[4] Chemistry - A European Journal, 2016, vol. 22, # 48, p. 17151 - 17155
[5] ChemCatChem, 2017, vol. 9, # 13, p. 2496 - 2505

6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE manufacturers

Career Henan Chemical Co

Product: 6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE 120-15-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Kg/T
Release date: 2019-12-19

120-15-0, 6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINERelated Search:

6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride 6-METHOXY-1,2,3,4-TETRAHYDRO-PYRIDO[2,3-B]PYRAZINE 6-METHOXY-1,2,3,4-TETRAHYDRO-ISOQUINOLINE 6-METHOXY-3,4-DIHYDRO-2H-ISOQUINOLIN-1-ONE Quinfamide 6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE 6-Methoxy-3,4-dihydro-1H-quinolin-2-one 8-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE 6-[4-(1-CYCLOHEXYL-1H-TETRAZOL-5-YL) BUTOXY]-2(1H)-QUINOLINONE 6-methoxy-2,3-dihydro-1H-quinolin-4-one 6-ethoxy-1,2,3,4-tetrahydro-2,2,4-trimethylquinoline METHYL 6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE-2-CARBOXYLATE HCL Selprazine 1H,5H-Benzo(ij)quinolizine, 2,3,6,7-tetrahydro-9-(2-(1-piperidinyl)eth oxy)-, dihydrochloride 1-(4,6-DICHLORO-1,3,5-TRIAZIN-2-YL)-6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE AURORA KA-4812 AURORA KA-4073 AURORA KA-4115

SALOR-INT L308625-1EA

TIMTEC-BB SBB002326

Thallin

Quinoline l,2,3,4-tetrahydro-6-methoxy

Quinoline, 1,2,3,4-tetrahydro-6-methoxy-

6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE

AKOS BB-9796

methyl 1,2,3,4-tetrahydro-6-quinolyl ether

6-Methoxy-1,2,3,4-tetrahydroquinoline 99%

N,N-dimethyl-2-[2-[2-methyl-4,6-bis(2-methylpropyl)phenoxy]ethoxy]ethanamine

6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE ISO 9001：2015 REACH

Debrisoquine Impurity 11

120-15-0

Building Blocks

Quinolines

Heterocyclic Building Blocks

Building Blocks

Heterocyclic Building Blocks

Quinolines