ChemicalBook > CAS DataBase List > methyl pyridine-3-acetate

methyl pyridine-3-acetate

Product Name
methyl pyridine-3-acetate
CAS No.
39998-25-9
Chemical Name
methyl pyridine-3-acetate
Synonyms
Methyl 2-(pyridin-3-yl)acetate;EOS-62049;Einecs 254-739-0;METHYL 3-PYRIDYLACETATE;methyl pyridine-3-acetate;Methyl pyridin-3-ylacetate;Methyl 2-(3-Pyridyl)acetate;3-Pyridineacetic acid methyl ester;3-Pyridinylacetic acid methyl ester;Pyridin-3-yl-acetic acid methyl ester
CBNumber
CB1894918
Molecular Formula
C8H9NO2
Formula Weight
151.16
MOL File
39998-25-9.mol
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methyl pyridine-3-acetate Property

Boiling point:
112 °C(Press: 10 Torr)
Density 
1.115±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
4.40±0.11(Predicted)
Appearance
Light yellow to yellow Liquid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
S363855
Product name
METHYL 3-PYRIDYLACETATE
Purity
Aldrich<sup>CPR</sup>
Packaging
1 unit
Price
$113
Updated
2025/07/31
Sigma-Aldrich
Product number
S363855
Product name
METHYL 3-PYRIDYLACETATE
Purity
Aldrich
Packaging
250mg
Price
$110
Updated
2024/03/01
TRC
Product number
M219543
Product name
Methyl2-(Pyridin-3-yl)acetate
Packaging
500mg
Price
$130
Updated
2021/12/16
AK Scientific
Product number
X5277
Product name
Methylpyridine-3-acetate
Packaging
250mg
Price
$82
Updated
2021/12/16
Matrix Scientific
Product number
113966
Product name
Methyl pyridin-3-ylacetate
Purity
97%
Packaging
1g
Price
$371
Updated
2021/12/16
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methyl pyridine-3-acetate Chemical Properties,Usage,Production

Synthesis

67-56-1

6419-36-9

39998-25-9

To synthesize methyl (pyridin-3-yl)acetate, the following procedure was used: in a 1L four-necked flask equipped with a nitrogen introduction tube, thermometer, Dimroth condenser, and a dropping funnel, 25.12 g (0.145 mol) of pyridine-3-acetic acid hydrochloride was added. Subsequently 500mL of anhydrous methanol was added. Stir at room temperature under nitrogen protection until the hydrochloride is completely dissolved. 31.12 g (0.248 mol) of thionyl chloride was slowly added dropwise. After the dropwise addition was completed, the reaction mixture was heated to reflux and the reaction was continued for 2.5 hours. After completion of the reaction, the mixture was cooled to room temperature and methanol was removed by distillation under reduced pressure by rotary evaporator. The residue was neutralized to pH neutral with saturated aqueous sodium bicarbonate. The aqueous phase was extracted with 100 mL of ethyl acetate in three fractions, the organic phases were combined and dried over anhydrous sodium sulfate. After filtration to remove the desiccant, the solvent was removed by distillation under reduced pressure to give 21.29 g (0.141 mol) of methyl (pyridin-3-yl)acetate in 97% yield.

References

[1] Patent: EP2390243, 2011, A1. Location in patent: Page/Page column 26
[2] Tetrahedron Letters, 1993, vol. 34, # 2, p. 331 - 334

methyl pyridine-3-acetate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from methyl pyridine-3-acetate manufacturers

Career Henan Chemical Co
Product
methyl pyridine-3-acetate 39998-25-9
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1000KG
Release date
2020-01-02

39998-25-9, methyl pyridine-3-acetateRelated Search:

methyl 2-amino-2-(5-bromopyridin-3-yl)hexanoate ETHYL 3-PYRIDYLACETATE methyl pyridine-3-acetate (6-CHLORO-PYRIDIN-3-YL)-OXO-ACETIC ACID ETHYL ESTER (2-CHLORO-PYRIDIN-3-YL)-OXO-ACETIC ACID ETHYL ESTER 3-PYRIDINEACETIC ACID, A-OXO, ETHYL ESTER 3-PYRIDINEACETIC ACID, 6-METHYL-,ETHYL ESTER RARECHEM AK ML 0009 ETHYL 2-CYANO-2-PYRIDIN-3-YL-ACETATE 2-CHLOROPYRIDINE-5-ACETIC ACID ETHYL ESTER 2,3,5,6-1H,4H-Tetrahydro-9-(3-pyridyl)quinolizino[9,9a,1-gh]coumarin 3-PYRIDINEACETIC ACID, 4-[[(1,1-DIMETHYLETHOXY)CARBONYL]AMINO]-A-OXO-, ETHYL ESTER RARECHEM AK ML 0008 RARECHEM AK HZ 0055 RARECHEM AM LA 0060 3-Pyridineacetic acid, (5-chloro-3-pyridinyl)methyl ester, monohydroch loride methyl 2-(5-bromopyridin-3-yl)acetate 3-AMINO-2-PYRIDIN-3-YL-PROPIONIC ACID ETHYL ESTER

  • methyl pyridine-3-acetate
  • Pyridin-3-yl-acetic acid methyl ester
  • 3-Pyridineacetic acid methyl ester
  • 3-Pyridinylacetic acid methyl ester
  • Einecs 254-739-0
  • Methyl 2-(pyridin-3-yl)acetate
  • METHYL 3-PYRIDYLACETATE
  • Methyl 2-(3-Pyridyl)acetate
  • Methyl pyridin-3-ylacetate
  • EOS-62049
  • 39998-25-9